CN103709839A - Gilding liquid cement and preparation method thereof as well as application of titanium dioxide in gilding liquid cement - Google Patents
Gilding liquid cement and preparation method thereof as well as application of titanium dioxide in gilding liquid cement Download PDFInfo
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Abstract
The invention relates to the technical field of gilding liquid cement, and particularly relates to gilding liquid cement and a preparation method thereof as well as an application of titanium dioxide in the gilding liquid cement. The gilding liquid cement comprises the following components of resin, titanium dioxide and an organic solvent. The preparation method of the gilding liquid cement comprises the following steps: 1, adding a formula amount of titanium dioxide to resin, evenly stirring to obtain a mixture; 2, grinding the mixture; and 3, adding the formula amount of organic solvent to the ground mixture, evenly stirring to obtain the gilding liquid cement. The titanium dioxide is applied to the gilding liquid cement, so that the alcohol resistance of the gilding liquid cement can be greatly improved, meanwhile, the coating production condition of the gilding liquid cement is stable, the gilding effect of the gilding liquid cement is not changed, the later processing stability of the gilding product is good, meanwhile, the firmness of a gilding film and the flatness of the section can be improved, the gilding liquid cement is better in levelling property when being coated, and the coating is fine in grains.
Description
Technical field
The present invention relates to gold stamping glue technical field, be specifically related to a kind of gold stamping glue and preparation method thereof and titanium dioxide in the application of gold stamping glue.
Background technology
Laser gold blocking printing is widely used in packages printing industry, and laser gold blocking print product has been widely used in the occasions such as cosmetic package, senior Packaging box, high-grade cigarette packing box, overlay film and drug packaging.
The gold stamping glue that laser gold blocking printshop is used requires very high to alcohol resistance.Gold stamping print product is in being applied to the production process of cosmetic package; often there will be spirituosity to drop on gilding film or hand is put on the situation on gilding film after being stained with alcohol; cause alcohol to corrode gilding film; thereby the laser gold blocking place that makes gilding film loses laser effect and metal sense; thereby have a strong impact on the quality of product, improved condemnation factor and production cost.
In prior art, for different application products, be mainly by adjusting the method for the proportion of various kinds of resin in gold stamping glue so that the alcohol resistance of gold stamping glue reaches requirement.Yet, this method needs to meet the alcohol resistance requirement of gold stamping glue, but, the method easily causes the correlated performances such as gilding film firmness and tangent plane planeness to change, thereby make hot stamping effects be difficult to control, and the method also can make the coating process conditions such as thermoprint speed, blocking temperature, drying temperature change, make again to explore suitable coating process condition, thereby make technique loaded down with trivial details and consuming time, greatly reduce production efficiency.
In addition, prior art is also by carrying out being coated with to increase the thickness of gilding film for twice with the erosion of reduction alcohol.But the method has reduced production efficiency, increased production cost simultaneously.
Summary of the invention
One of object of the present invention is for the deficiencies in the prior art, provides a kind of alcohol resistance energy good gold stamping glue.
Two of object of the present invention is for the deficiencies in the prior art, and the preparation method of the gold stamping glue that a kind of production cost is low is provided.
Three of object of the present invention is for the deficiencies in the prior art, and the application of titanium dioxide at gold stamping glue is provided.
One of to achieve these goals, the present invention adopts following technical scheme:
A gold stamping glue, comprises the component of following weight percent:
Resin 35% ~ 45%
Titanium dioxide 1% ~ 3%
Organic solvent 54% ~ 64%.
Preferably, a kind of gold stamping glue, comprises the component of following weight percent:
Resin 45%
Titanium dioxide 3%
Organic solvent 52%.
Described resin is oleoresin, and described oleoresin is any one or any one the above mixture in polyolefin resin, aldehyde ketone resin, polyvinyl acetate resin, chlorinated polypropylene or silicone resin.
Described resin is water-base resin, and described water-base resin is any one or any one the above mixture in acrylic resin, resol or urethane resin.
Described resin is the mixture of oleoresin and water-base resin, and the blending ratio of described oleoresin and described water-base resin is 7 ~ 9:1 ~ 3.
Described oleoresin is polyolefin resin, and described water-base resin is acrylic resin.
Described organic solvent is ethyl acetate and/or propyl carbinol.
To achieve these goals two, the present invention adopts following technical scheme:
The preparation method of a kind of gold stamping glue described above, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds;
Step 3, the organic solvent toward adding formula ratio in the mixture after grinding, obtains gold stamping glue after stirring.
In technique scheme, in described step 2, mixture is ground, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m.
To achieve these goals three, the present invention adopts following technical scheme:
Titanium dioxide is for improving the application of the alcohol resistance energy of gold stamping glue described above.
The invention has the beneficial effects as follows:
(1) a kind of gold stamping glue provided by the invention, owing to having added titanium dioxide as gold stamping glue component, can improve the alcohol resistance of this gold stamping glue greatly, thereby can protect gilding film to be not easy to be corroded by alcoholic solvent in the process of producing.
(2) a kind of gold stamping glue provided by the invention, owing to having added titanium dioxide as gold stamping glue component, can improve coating adhesion and wear resisting property after gold stamping glue thermoprint.
(3) a kind of gold stamping glue provided by the invention, owing to having added titanium dioxide as gold stamping glue component, when improving gold stamping glue alcohol resistance energy, make the coating working condition of gold stamping glue stable, and can not change the hot stamping effects of gold stamping glue, make the good stability of the post-production of gold stamping product, can improve gilding film firmness and tangent plane planeness simultaneously.
(4) a kind of gold stamping glue provided by the invention, owing to having added titanium dioxide as gold stamping glue component,
(5) preparation method of a kind of gold stamping glue provided by the invention, has technique simple, and prepared gold stamping glue can improve the production efficiency of laser gold blocking printing, and can reduce the production cost of laser gold blocking printing.
(6) titanium dioxide provided by the invention is applied at gold stamping glue, has application method simple, can improve the production efficiency of laser gold blocking printing, and can reduce the production cost of laser gold blocking printing.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated.
embodiment 1.
A gold stamping glue, comprises the component of following weight: polyolefin resin 45 kg, titanium dioxide 3 kg, ethyl acetate 30 kg, propyl carbinol 22 kg.
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in polyolefin resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, ethyl acetate and propyl carbinol toward adding formula ratio in the mixture after grinding, obtain gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 2.
A gold stamping glue, comprises the component of following weight: aldehyde ketone resin 35 kg, titanium dioxide 1 kg, ethyl acetate 39 kg, propyl carbinol 25 kg.
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in aldehyde ketone resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, ethyl acetate and propyl carbinol toward adding formula ratio in the mixture after grinding, obtain gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 3.
A gold stamping glue, comprises the component of following weight: polyvinyl acetate resin 40 kg, titanium dioxide 2 kg, ethyl acetate 35 kg, propyl carbinol 23 kg.
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in polyvinyl acetate resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, ethyl acetate and propyl carbinol toward adding formula ratio in the mixture after grinding, obtain gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 4.
A gold stamping glue, comprises the component of following weight: chlorinated polypropylene 27 kg, silicone resin 10 kg, titanium dioxide 1.5 kg, ethyl acetate 40 kg, propyl carbinol 21.5 kg.
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in chlorinated polypropylene and silicone resin premixture, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, ethyl acetate and propyl carbinol toward adding formula ratio in the mixture after grinding, obtain gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 5.
A gold stamping glue, comprises the component of following weight: acrylic resin 43 kg, titanium dioxide 2.5 kg, ethyl acetate 54.5 kg.
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in acrylic resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, the ethyl acetate toward adding formula ratio in the mixture after grinding, obtains gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 6.
A gold stamping glue, comprises the component of following weight: resol 41 kg, titanium dioxide 1.2 kg, propyl carbinol 57.8 kg.
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in resol, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, the propyl carbinol toward adding formula ratio in the mixture after grinding, obtains gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 7.
A gold stamping glue, comprises the component of following weight: resol 18 kg, urethane resin 20 kg, titanium dioxide 2.8 kg, ethyl acetate 20 kg, propyl carbinol 39.2 kg.
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in the premixture of resol and urethane resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, ethyl acetate and propyl carbinol toward adding formula ratio in the mixture after grinding, obtain gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 8.
A gold stamping glue, comprises the component of following weight: polyolefin resin 16 kg,, aldehyde ketone resin 20 kg, titanium dioxide 1.7 kg, ethyl acetate 32.3 kg, propyl carbinol 30 kg.
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in the premixture of polyolefin resin and aldehyde ketone resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, ethyl acetate and propyl carbinol toward adding formula ratio in the mixture after grinding, obtain gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 9.
A gold stamping glue, comprises the component of following weight: aldehyde ketone resin 12 kg, polyvinyl acetate resin 10 kg, chlorinated polypropylene 20 kg, titanium dioxide 2.3 kg, ethyl acetate 55.7 kg.
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in the premixture of aldehyde ketone resin, polyvinyl acetate resin and chlorinated polypropylene, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, the ethyl acetate toward adding formula ratio in the mixture after grinding, obtains gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 10.
A gold stamping glue, comprises the component of following weight: acrylic resin 20 kg, resol 10 kg, urethane resin 14 kg, titanium dioxide 2.9 kg, propyl carbinol 53.1 kg.
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in the premixture of acrylic resin, resol and urethane resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, the propyl carbinol toward adding formula ratio in the mixture after grinding, obtains gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 11.
A gold stamping glue, comprises the component of following weight: polyolefin resin 35.2 kg, acrylic resin 8.8 kg, titanium dioxide 2.9 kg, propyl carbinol 53.1 kg.In the present embodiment, oleoresin (polyolefin resin) is 8:2 with the blending ratio of water-base resin (acrylic resin).
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in the premixture of polyolefin resin and acrylic resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, the propyl carbinol toward adding formula ratio in the mixture after grinding, obtains gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 12.
A gold stamping glue, comprises the component of following weight: polyolefin resin: 39.375 kg, acrylic resin 5.625 kg, titanium dioxide 3 kg, ethyl acetate 30 kg, propyl carbinol 22 kg.In the present embodiment, oleoresin (polyolefin resin) is 7:1 with the blending ratio of water-base resin (acrylic resin).
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in the premixture of polyolefin resin and acrylic resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, the propyl carbinol toward adding formula ratio in the mixture after grinding, obtains gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
embodiment 13.
A gold stamping glue, comprises the component of following weight: polyolefin resin 26.25 kg, acrylic resin 8.75 kg, titanium dioxide 1 kg, ethyl acetate 39 kg, propyl carbinol 25 kg.In the present embodiment, oleoresin (polyolefin resin) is 9:3 with the blending ratio of water-base resin (acrylic resin).
The preparation method of above-mentioned gold stamping glue, it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in the premixture of polyolefin resin and acrylic resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m;
Step 3, the propyl carbinol toward adding formula ratio in the mixture after grinding, obtains gold stamping glue after stirring.
Titanium dioxide is applied to prepare above-mentioned gold stamping glue, can greatly improve the alcohol resistance energy of above-mentioned gold stamping glue.In addition, titanium dioxide can also improve coating adhesion and the wear resisting property after this gold stamping glue thermoprint.
Above-mentioned gold stamping glue is applied to laser gold blocking printing, prepared laser gold blocking for print product ethanol (mass percent concentration is 95%) soak after 10 minutes, use this laser gold blocking print product gilding film surface of 2000# sand papering, it is good that the firmness of gilding film and laser effect all keep again.
Finally should be noted that; above embodiment is only in order to illustrate technical scheme of the present invention; but not limiting the scope of the invention; although the present invention has been done to explain with reference to preferred embodiment; those of ordinary skill in the art is to be understood that; can modify or be equal to replacement technical scheme of the present invention, and not depart from essence and the scope of technical solution of the present invention.
Claims (10)
1. a gold stamping glue, is characterized in that: the component that comprises following weight percent:
Resin 35% ~ 45%
Titanium dioxide 1% ~ 3%
Organic solvent 54% ~ 64%.
2. a kind of gold stamping glue according to claim 1, is characterized in that: the component that comprises following weight percent:
Resin 45%
Titanium dioxide 3%
Organic solvent 52%.
3. a kind of gold stamping glue according to claim 1, it is characterized in that: described resin is oleoresin, described oleoresin is any one or any one the above mixture in polyolefin resin, aldehyde ketone resin, polyvinyl acetate resin, chlorinated polypropylene or silicone resin.
4. a kind of gold stamping glue according to claim 1, is characterized in that: described resin is water-base resin, and described water-base resin is any one or any one the above mixture in acrylic resin, resol or urethane resin.
5. a kind of gold stamping glue according to claim 1, is characterized in that: described resin is the mixture of oleoresin and water-base resin, and the blending ratio of described oleoresin and described water-base resin is 7 ~ 9:1 ~ 3.
6. a kind of gold stamping glue according to claim 5, is characterized in that: described oleoresin is polyolefin resin, and described water-base resin is acrylic resin.
7. a kind of gold stamping glue according to claim 1, is characterized in that: described organic solvent is ethyl acetate and/or propyl carbinol.
8. the preparation method of a kind of gold stamping glue described in claim 1 to 7 any one, is characterized in that: it comprises the following steps:
Step 1, joins the titanium dioxide of formula ratio in resin, stirs, and obtains mixture;
Step 2, the mixture that step 1 is obtained grinds;
Step 3, the organic solvent toward adding formula ratio in the mixture after grinding, obtains gold stamping glue after stirring.
9. the preparation method of a kind of gold stamping glue according to claim 8, is characterized in that: in described step 2, mixture is ground, until the particle diameter of the titanium dioxide in mixture is less than 0.36 μ m.
Titanium dioxide for improve the gold stamping glue described in claim 1 to 9 any one alcohol resistance can application.
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