CN103673590A - Honeycomb type SCR denitration catalyst calcining furnace and method for drying SCR denitration catalyst - Google Patents
Honeycomb type SCR denitration catalyst calcining furnace and method for drying SCR denitration catalyst Download PDFInfo
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- CN103673590A CN103673590A CN201310650096.1A CN201310650096A CN103673590A CN 103673590 A CN103673590 A CN 103673590A CN 201310650096 A CN201310650096 A CN 201310650096A CN 103673590 A CN103673590 A CN 103673590A
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Abstract
The invention discloses a honeycomb type SCR denitration catalyst calcining furnace and a method for drying an SCR denitration catalyst. The honeycomb type SCR denitration catalyst calcining furnace comprises a furnace body, a conveying device and a heating device. The conveying device comprises a feeding platform, a conveying platform and a discharging platform. The conveying device further comprises a net belt operating on the feeding platform, the conveying platform and the discharging platform in a revolving mode. The heating device is an infrared quartz heating pipe arranged inside the furnace body. The tail end of the furnace body is provided with a cooling area which is provided with a heat exchanging pipe. The heat exchanging pipe is connected with a heat pumping draught fan. The two sides of the net belt are provided with automatic skew adjustment devices comprising guiding wheels. The drying method comprises the warming section I, the sintering section I, the warming section II, the sintering section II and the cooling section. The calcining furnace is economical, durable, good in heat preservation effect and high in automation degree and saves energy consumption, the number of the fractured sintered products is small, and the quality of the products is high.
Description
Technical field
The invention belongs to SCR denitrating catalyst production field, be specifically related to a kind of calcining furnace and drying means thereof for the production of honeycomb fashion SCR denitrating catalyst.
Background technology
Due to mankind's activity and economic fast development, China's environment is seriously damaged, and extreme climate showed increased causes serious threat to people's life and property, to country, causes heavy losses, has hindered the sustainable development of national economy simultaneously.Country has also paid huge cost in order to administer environment.
The current discharged nitrous oxides total amount of China surpasses 1,800 ten thousand tons, if do not take effective control measure, 5 years Chinese nitrogen oxide emissions of Future Ten will continue to increase, and to the year two thousand twenty, may reach more than 3,000 ten thousand tons.China is coal-fired big country, and coal-burning power plant is the primary emission source of nitrogen oxide, accounts for 40% of total amount, will become the first batch of control object of country.
Honeycomb ceramics SCR denitrating catalyst Main Function is by the NO in discharging waste gas
xconvert nitrogen and steam to, to reach environmental emission standard.
SCR device is mainly comprised of two large main bodys: remove agent preparation system and reactor body.By spray into reactant NH in reactor
3, NOx is reduced to nitrogen.Because this reduction reaction is comparatively responsive to temperature, therefore need add catalyst active with intensified response, meet the temperature requirement of reaction.
Honeycomb fashion SCR denitrating catalyst main component generally comprises nano-TiO
2, V
2o
5and WO
3.These three kinds of shared catalyst ratios of composition surpass 95 ﹪, and TiO
2proportion is generally 80%~85%.In order to meet production technology needs, guarantee easy extrusion modling, also needing in addition to increase the mixture additives such as some viscose glues and glass fibre increases pug intensity and mobility, adjusts its physical property.Due to these compositions stir mixing rear mobility and plasticity poor, moulding difficulty is larger.Again because the water holding capacity of product is poor, atmospheric crack very easily after moulding is therefore also higher to the production engineering specifications of dry kiln.During simultaneously due to this product calcining, can give off a large amount of NH
3, SO
3deng corrosive gas and compound hydrogen sulfate ammonia thereof, after calcining also easily because of cooling too fast cracking.
Therefore, this production requires also higher to calcining furnace.If the production technology assurance to this product is bad, may there is failed situation in dry kiln and calcining kiln.
Because existing honeycomb fashion SCR denitrating catalyst technology is mainly from external introduction, calcining furnace equipment is main Introduced From Abroad tradition calcining furnace also, as Japan and U.S.'s electrical heating guipure kiln calcining furnace, German combustion gas shuttle kiln calcining furnace.These mesh-belt kiln calcining furnaces mainly adopt electric power as heating source, heater element is traditional resistor silk, the erosion of corrosivity resistance when these resistance wires are easily received calcining, be not durable, insulation material is light fire brick, and being mainly manifested in electrical heating is that electric energy energy transform into heat energy efficiency is lower by radiant heat transfer, and heat insulation effect is poor, fuel cost is high.Not only equipment price is higher, and energy consumption is also larger simultaneously, does not meet current energy-conserving and environment-protective Developing mainstream.Combustion gas shuttle kiln calcining furnace mainly adopts heated by natural gas, and due to service intermittent characteristic, production stability is not high, hand labor intensity is large, in combustion gas, also can take away amount of heat, and energy consumption is higher, and also automatic continuous production is carried out in inconvenience simultaneously.
In addition, mesh-belt kiln calcining furnace is provided with the guipure that transports idiosome, and deviation easily appears in this guipure in the process of transporting, and causes transporting and cannot complete, and needs break-off to correct guipure.
Summary of the invention
The invention provides a kind of honeycomb fashion SCR denitrating catalyst calcining furnace.This calcining furnace economy and durability, high insulating effect, saves energy consumption, and product quality is high, and automaticity is high.The present invention also provides a kind of drying means of SCR denitrating catalyst, uses the method dry, and product cracking is few, and quality is high.
In order to solve the problems of the technologies described above, the present invention is achieved through the following technical solutions: a kind of honeycomb fashion SCR denitrating catalyst calcining furnace, comprise body of heater, conveyer, heater, described conveyer comprises feeding platform, delivery platform, discharging platform, described conveyer is also included in described feeding platform, delivery platform, the guipure of discharging platform upper rotary operation, described heater is the Far-infrared quartz heating tube being arranged in body of heater, described body of heater end is provided with cooled region, described cooled region is provided with heat exchanger tube, described heat exchanger tube with take out air-heater and be connected, described guipure both sides are provided with automatic deviation rectifying device, described automatic deviation rectifying device comprises directive wheel.Due in calcination process, honeycomb fashion SCR denitrating catalyst idiosome can give off a large amount of NH
3, SO
3deng corrosive gas, traditional resistance wire is exposed in these gases and can be corroded, and affects service life, and Far-infrared quartz heating tube can be by these gas attacks, very durable.Meanwhile, the restriction of described directive wheel, can make described guipure can not be partial in running.The described air-heater of taking out is extracted air in described cooled region out via heat exchanger tube, make this section of temperature slow decreasing, and the honeycomb fashion SCR denitrating catalyst base substrate that makes high temperature can not cause temperature decrease in air and causes product cracking because of being directly exposed to suddenly.
As preferably, described furnace body inside is provided with insulation material, and described insulation material is full fiber folded piece.Adopt full fiber folded piece to make liner and can reduce accumulation of heat, improve programming rate, strengthen heat insulation effect, energy-saving and cost-reducing.
As preferably, the heater element in described Far-infrared quartz heating tube is resistance wire.Resistance wire is placed in and in Far-infrared quartz heating tube, has avoided contacting of resistance wire and corrosive gas.
As preferably, described body of heater length is 47 ~ 58 meters, 0.9 ~ 1.8 meter of described body of heater inner width, and the quantity of described Far-infrared quartz heating tube is 117 ~ 234.Furnace profile is wide, and useful load is large, can further expand the scale of production.
As preferably, described Far-infrared quartz heating tube is connected with temperature controller, is also provided with Temperature Detector in described body of heater.Temperature Detector can be collected temperature signal, and temperature controller can be according to the voltage of resistance wire in this Signal Regulation Far-infrared quartz heating tube, and then changes firing rate.
As preferably, described Far-infrared quartz heating tube is divided into 12 ~ 15 groups and is connected with temperature controller respectively, and the quantity of described Temperature Detector is 9 ~ 12.Temperature controller divides 12~15 groups to carry out temperature and automatically control, and the firing temperature curve of product is more level and smooth, and temperature is controlled more stable, improves the product quality of honeycomb fashion SCR denitrating catalyst.
The drying means of SCR denitrating catalyst, comprises the following steps: the section that 1) heats up I, for SCR denitrating catalyst base substrate is heated to 180~210 ℃; 2) section of burning till I, for burning till SCR denitrating catalyst base substrate at 180~210 ℃; 3) an intensification section II, for being warming up to 485~620 ℃ by SCR denitrating catalyst base substrate; 4) section of burning till II, for burning till SCR denitrating catalyst base substrate at 485~620 ℃; 5) cooling section, for being cooled to 75~40 ℃ by the SCR denitrating catalyst after burning till.
Adopt above temperature programming, the drying and sintering method of cooling, the SCR denitrating catalyst product sintering into cracking is few, and quality is high, has improved raw material availability, has improved production efficiency, energy-saving and cost-reducing.
As preferably, completing the once sintered cycle is 33 ± 3 hours.Cycle is short.
Compared with prior art, the present invention has following beneficial effect: 1. the present invention adopts Far-infrared quartz heating tube heating, and resistance wire heater element is arranged on quartz ampoule inside, extends resistance wire service life.
2. the present invention is provided with the directive wheel that plays automatic deviation rectifying function in guipure both sides, can make described guipure can not be partial in running, has improved operating efficiency.
3. the present invention adopts the indirect type of cooling to carry out Slow cooling to product, guarantees that product is not easy to crack, improves the product quality of honeycomb fashion SCR denitrating catalyst.
4. the present invention adopts full fiber folded piece to reduce accumulation of heat as liner, improves programming rate, strengthens heat insulation effect, energy-saving and cost-reducing.
5. the present invention adopts controllable silicon to divide 12~15 groups to carry out temperature and automatically control, and the firing temperature curve of product is more level and smooth, and temperature is controlled more stable, improves the product quality of honeycomb fashion SCR denitrating catalyst.
6. burner hearth of the furnace body section of the present invention is wide, and useful load is large, has expanded production specification scale.
7. the SCR denitrating catalyst product cracking that drying and sintering of the present invention becomes is few, and quality is high, has improved raw material availability, has improved production efficiency, energy-saving and cost-reducing.
Accompanying drawing explanation
Fig. 1 is schematic diagram of the present invention.
Fig. 2 is the schematic diagram of body of heater inside in the present invention.
Fig. 3 is the schematic diagram of discharging platform in the present invention.
The specific embodiment
Below in conjunction with accompanying drawing and the specific embodiment, the present invention is described in further detail: see accompanying drawing, a kind of honeycomb fashion SCR denitrating catalyst calcining furnace, comprise body of heater 1, conveyer, heater, described conveyer comprises feeding platform 2, delivery platform 4, discharging platform 3, described conveyer is also included in described feeding platform 2, delivery platform 4, the guipure 31 of discharging platform 3 upper rotary operations, described heater is the Far-infrared quartz heating tube 6 being arranged in body of heater 1, described body of heater 1 end is provided with cooled region, described cooled region is provided with heat exchanger tube 5, described heat exchanger tube 5 with take out air-heater 8 and be connected, described guipure 31 both sides are provided with automatic deviation rectifying device, described automatic deviation rectifying device comprises directive wheel 32.Described body of heater 1 inner side is provided with insulation material, and described insulation material is full fiber folded piece 7.Heater element in described Far-infrared quartz heating tube 6 is resistance wire.In present embodiment, described body of heater 1 length is 47 meters, 0.9 meter of described body of heater 1 inner width, and the quantity of described Far-infrared quartz heating tube 6 is 117.Described Far-infrared quartz heating tube 6 is connected with temperature controller, in described body of heater 1, is also provided with Temperature Detector.Described Far-infrared quartz heating tube 6 is divided into 12 groups and is connected with temperature controller respectively, and the quantity of described Temperature Detector is 9.
During drying and sintering SCR denitrating catalyst, comprise the following steps: during work, feeding platform 2 is for being longitudinally placed on honeycomb fashion SCR denitrating catalyst base substrate the guipure of feeding platform 2, product bottom is lined with asbestos fibre, and product is automatically entered in honeycomb fashion SCR denitrating catalyst calcining furnace and carried out sintering by guipure.Feeding platform 2 consists of frame, passive swift, tensioner cylinder, upper supporting roller and snub pulley.Discharging platform 3 for by cooled product discharge to discharging platform 3.Discharging platform 3 is by frame, active encapsulate swift, tensioner cylinder, guide pulley, transmission variable-frequency motor, gearbox, upper supporting roller, snub pulley, limit alarm device and speed measuring device.Transmission variable-frequency motor, gearbox and initiatively encapsulate swift employing double strand chain transmission.In guipure 31 runnings, guipure both sides are directed to wheel 32 and limit, and guipure 31 can not be offset.
SCR denitrating catalyst base substrate enters after body of heater 1, can pass through with the next stage: for SCR denitrating catalyst base substrate being heated to the intensification section I of 180 ℃; Be used for SCR denitrating catalyst base substrate the 180 ℃ of section of burning till of burning till I; For SCR denitrating catalyst base substrate is warming up to the intensification section II of 485 ℃; Be used for SCR denitrating catalyst base substrate the 485 ℃ of section of burning till of burning till II; For the SCR denitrating catalyst base substrate after burning till is cooled to the cooling section of 75 ℃ indirectly.30 hours sintering periods.Wherein, described in cooling section process, taking out air-heater 8 extracts air in described cooled region out via heat exchanger tube 5, make this section of temperature slow decreasing, the honeycomb fashion SCR denitrating catalyst base substrate that makes high temperature can not cause temperature decrease in air and causes product cracking because of being directly exposed to suddenly.
The SCR denitrating catalyst product cracking that drying and sintering becomes is few, and quality is high, has improved raw material availability, has improved production efficiency, energy-saving and cost-reducing.
Another embodiment of the invention is: a kind of honeycomb fashion SCR denitrating catalyst calcining furnace, comprise body of heater 1, conveyer, heater, described conveyer comprises feeding platform 2, delivery platform 4, discharging platform 3, described conveyer is also included in described feeding platform 2, delivery platform 4, the guipure 31 of discharging platform 3 upper rotary operations, described heater is the Far-infrared quartz heating tube 6 being arranged in body of heater 1, described body of heater 1 end is provided with cooled region, described cooled region is provided with heat exchanger tube 5, described heat exchanger tube 5 with take out air-heater 8 and be connected, described guipure 31 both sides are provided with automatic deviation rectifying device, described automatic deviation rectifying device comprises directive wheel 32.Described body of heater 1 inner side is provided with insulation material, and described insulation material is full fiber folded piece 7.Heater element in described Far-infrared quartz heating tube 6 is resistance wire.In present embodiment, described body of heater 1 length is 58 meters, 1.8 meters of described body of heater 1 inner widths, and the quantity of described Far-infrared quartz heating tube 6 is 234.Described Far-infrared quartz heating tube 6 is connected with temperature controller, in described body of heater 1, is also provided with Temperature Detector.Described Far-infrared quartz heating tube 6 is divided into 15 groups and is connected with temperature controller respectively, and the quantity of described Temperature Detector is 12.
During work, feeding platform 2 is for being longitudinally placed on honeycomb fashion SCR denitrating catalyst base substrate the guipure of feeding platform 2, and product bottom is lined with asbestos fibre, and product is automatically entered in honeycomb fashion SCR denitrating catalyst calcining furnace and carried out sintering by guipure.Feeding platform 2 consists of frame, passive swift, tensioner cylinder, upper supporting roller and snub pulley.Discharging platform 3 for by cooled product discharge to discharging platform 3.Discharging platform 3 is by frame, active encapsulate swift, tensioner cylinder, guide pulley, transmission variable-frequency motor, gearbox, upper supporting roller, snub pulley, limit alarm device and speed measuring device.Transmission variable-frequency motor, gearbox and initiatively encapsulate swift employing double strand chain transmission.In guipure 31 runnings, guipure both sides are directed to wheel 32 and limit, and guipure 31 can not be offset.
SCR denitrating catalyst base substrate enters after body of heater 1, can pass through with the next stage: for SCR denitrating catalyst base substrate being heated to the intensification section I of 210 ℃; Be used for SCR denitrating catalyst base substrate the 210 ℃ of section of burning till of burning till I; For SCR denitrating catalyst base substrate is rapidly heated to the intensification section II of 620 ℃; Be used for SCR denitrating catalyst base substrate the 620 ℃ of section of burning till of burning till II; For the SCR denitrating catalyst base substrate after burning till is cooled to the cooling section of 40 ℃ indirectly.36 hours sintering periods.Wherein, described in cooling section process, taking out air-heater 8 extracts air in described cooled region out via heat exchanger tube 5, make this section of temperature slow decreasing, the honeycomb fashion SCR denitrating catalyst base substrate that makes high temperature can not cause temperature decrease in air and causes product cracking because of being directly exposed to suddenly.
The SCR denitrating catalyst product cracking that drying and sintering becomes is few, and quality is high, has improved raw material availability, has improved production efficiency, energy-saving and cost-reducing.
Claims (8)
1. a honeycomb fashion SCR denitrating catalyst calcining furnace, comprise body of heater (1), conveyer, heater, described conveyer comprises feeding platform (2), delivery platform (4), discharging platform (3), described conveyer is also included in described feeding platform (2), delivery platform (4), the guipure (31) of discharging platform (3) upper rotary operation, it is characterized in that, described heater is for being arranged at the Far-infrared quartz heating tube (6) in body of heater (1), described body of heater (1) end is provided with cooled region, described cooled region is provided with heat exchanger tube (5), described heat exchanger tube (5) with take out air-heater (8) and be connected, described guipure (31) both sides are provided with automatic deviation rectifying device, described automatic deviation rectifying device comprises directive wheel (32).
2. a kind of honeycomb fashion SCR denitrating catalyst calcining furnace according to claim 1, is characterized in that, described body of heater (1) inner side is provided with insulation material, and described insulation material is full fiber folded piece (7).
3. a kind of honeycomb fashion SCR denitrating catalyst calcining furnace according to claim 2, is characterized in that, the heater element in described Far-infrared quartz heating tube (6) is resistance wire.
4. a kind of honeycomb fashion SCR denitrating catalyst calcining furnace according to claim 3, it is characterized in that, described body of heater (1) length is 47 ~ 58 meters, 0.9 ~ 1.8 meter of described body of heater (1) inner width, and the quantity of described Far-infrared quartz heating tube (6) is 117 ~ 234.
5. according to a kind of honeycomb fashion SCR denitrating catalyst calcining furnace described in claim 1 ~ 4 any one, it is characterized in that, described Far-infrared quartz heating tube (6) is connected with temperature controller, and described body of heater is also provided with Temperature Detector in (1).
6. a kind of honeycomb fashion SCR denitrating catalyst calcining furnace according to claim 5, is characterized in that, described Far-infrared quartz heating tube (6) is divided into 12 ~ 15 groups and is connected with temperature controller respectively, and the quantity of described Temperature Detector is 9 ~ 12.
7. the drying means of SCR denitrating catalyst as claimed in claim 1, is characterized in that, comprises the following steps: the section that 1) heats up I, for SCR denitrating catalyst base substrate is heated to 180~210 ℃; 2) section of burning till I, for burning till SCR denitrating catalyst base substrate at 180~210 ℃; 3) an intensification section II, for being warming up to 485~620 ℃ by SCR denitrating catalyst base substrate; 4) section of burning till II, for burning till SCR denitrating catalyst base substrate at 485~620 ℃; 5) cooling section, for being cooled to 75~40 ℃ by the SCR denitrating catalyst after burning till.
8. the drying means of SCR denitrating catalyst according to claim 7, is characterized in that, completing the once sintered cycle is 33 ± 3 hours.
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CN104315843A (en) * | 2014-10-28 | 2015-01-28 | 黄冈市华窑中瑞窑炉有限公司 | Vertical recycling, drying and calcining furnace for SCR (selective catalytic reduction) denitration catalysts |
CN104764320A (en) * | 2015-02-12 | 2015-07-08 | 浙江三龙催化剂有限公司 | Industrial tunnel kiln for roasting denitration catalyst |
CN105170197A (en) * | 2015-10-09 | 2015-12-23 | 山东奥福环保科技股份有限公司 | Catalyst calcinating method and calcinating equipment |
CN108645207A (en) * | 2018-05-18 | 2018-10-12 | 江苏浩日朗环保科技有限公司 | Electrical kiln for cellular catalyst roasting |
CN113405332A (en) * | 2021-08-19 | 2021-09-17 | 徐州紫聚石化设备有限公司 | Low temperature SCR denitration catalyst shaping drying device |
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Application publication date: 20140326 |