CN103668098B - A kind of method improving use in magnetron sputtering coating target utilization rate - Google Patents

A kind of method improving use in magnetron sputtering coating target utilization rate Download PDF

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Publication number
CN103668098B
CN103668098B CN201410001386.8A CN201410001386A CN103668098B CN 103668098 B CN103668098 B CN 103668098B CN 201410001386 A CN201410001386 A CN 201410001386A CN 103668098 B CN103668098 B CN 103668098B
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target
line
residual
spliced
width
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CN103668098A (en
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姚能健
黄威智
方家芳
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Guangyang new material technology (Kunshan) Co.,Ltd.
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KUNSHAN QUANYAGUAN ENVIRONMENTAL PROTECTION TECHNOLOGY Co Ltd
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Abstract

The invention discloses a kind of method improving use in magnetron sputtering coating target utilization rate, including following step: (1), according to the sputtering runway of residual target, uses wire cutting machine line to cut residual target in the erosion curved surface of described residual target, obtains multi-disc spliced target;The choosing method of line of cut is: select width vertical line, and the angle of described line of cut and width vertical line is between 0~30 °, and described width vertical line uses bosom and vertical with the width of residual target at residual target;(2) each described spliced target is cleaned;(3) spliced target after cleaning is stitched together, and by spliced target and backboard seam, after seam, installation carries out sputter coating again.The utilization rate of use in magnetron sputtering coating target is improved to 40% by the present invention, meanwhile, reduces production cost, decreases the wasting of resources, present invention is particularly suitable for precious metal and oxide target material.

Description

A kind of method improving use in magnetron sputtering coating target utilization rate
Technical field
The present invention relates to a kind of method improving use in magnetron sputtering coating target utilization rate, belong to target Material technical field.
Background technology
At present, use in magnetron sputtering coating target is varied, for composition, has simple substance target, Also there is alloys target.Wherein alloys target has silver alloy, billon, platinum alloy, nickel alloy, aluminum to close Gold, tin indium oxide, niobium oxide etc..For shape, there are flat target and rotary target.Magnetic control In use there is uneven erosion phenomenon in sputter coating target, so the utilization of target Rate is generally low, flat target about 20%, rotary target about 60%.
It is known that the production cost of alloy target material is higher than common simple substance target, noble metal list Matter target can be recycled by remelting, and alloys target and oxide target material due to its complicated component because of The cost of this remelting recycling is the highest, there is also the risk of uneven components simultaneously.And rotary target In the case of length is less than 1 meter, its cost is about the target cost with sample ingredient and length 3 times, when rotary target length is further added by, cost will be multiplied.
Summary of the invention
The deficiency existed for prior art, it is an object of the present invention to provide a kind of the most sharp by residual target With, the method improving use in magnetron sputtering coating target utilization rate, reduce production cost, reduce The wasting of resources.
To achieve these goals, the present invention is to realize by the following technical solutions:
A kind of method improving use in magnetron sputtering coating target utilization rate, including following step:
(1) according to the sputtering runway of residual target, in the erosion curved surface of residual target, wire cutting machine is used Line cuts residual target, obtains multi-disc spliced target;
The choosing method of line of cut is: select width vertical line, line of cut and width vertical line Angle is between 0~30 °, and width vertical line uses bosom and the width with residual target at residual target Direction is vertical;
(2) each spliced target is cleaned;
(3) spliced target after cleaning is stitched together, and by spliced target and the back of the body Plate seam, after seam, installation carries out sputter coating again.
Also include before step (1) that residual target releases seam step.
In step (1), the width of the monolithic spliced target after line cutting is divided by sputtering runway Width is equal to 0.2~1.2, and the residual target length before its length is cut with line is identical.
In step (3), during splicing, the gap between each spliced target is 0~2mm;
The seam surface of backboard is provided with the backboard solder layer of low melting point, the seam of spliced target Surface is sequentially provided with the target solder layer of plasma spraying boundary layer and low melting point from inside to outside, the back of the body Plate solder layer connects with target solder layer soft soldering;
Backboard solder layer is 0.05~2mm with the gross thickness of target solder layer.
The material that backboard uses is copper or titanium.
The utilization rate of use in magnetron sputtering coating target is improved to 40% by the present invention, reduces meanwhile Production cost, decreases the wasting of resources, present invention is particularly suitable for precious metal and oxide Target.
Accompanying drawing explanation
Fig. 1 is the new target (sectional area is 725mm2) of one embodiment of the invention;
Fig. 2 is the most residual target (sectional area is 559mm2) of one embodiment of the invention;
Fig. 3 is residual target recycling target (sectional area is 559mm2) of one embodiment of the invention;
Fig. 4 is the residual target of secondary (sectional area is 423mm2) of one embodiment of the invention;
Fig. 5 is the most residual target runway figure;
Fig. 6 is the erosion cambered cross-section figure of the most residual target;
Fig. 7 is the target spliced map (a, b, c, d, e are spliced target) after seam completes;
Fig. 8 is the profile of Fig. 7.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be prone to bright with effect White understanding, below in conjunction with detailed description of the invention, is expanded on further the present invention.
A kind of method improving use in magnetron sputtering coating target utilization rate, especially precious metal and The residual target of valuable oxide, including following step:
(1) residual target releases seam (i.e. removing backboard), but part target is not required to release seam.
(2) in Fig. 5 and embodiment illustrated in fig. 6, measure and make at corresponding magnetron sputtering board With sputtering runway and the erosion curve of residual target;Different magnetron sputtering boards, its sputtering runway and Erosion curve is the most different;Fig. 2 (obtains the most residual target of Fig. 2 by the new target of Fig. 1) after being used Just differing with sputtering runway and the erosion curve of Fig. 6, its target utilization rate is respectively 23% With 19%.
In the embodiment shown in fig. 6, using wire cutting machine line to cut residual target, line cutting end at the whole story must Must be in erosion curve, typically using width interval, innermost left and right 15%, (line cutting is residual During target two terminal circle arc runway, can not be in erosion curve), when certain one end is not or not this interval Time interior, the utilization rate of target will be reduced to less than 30%;The angle of line cutting must be less than 15 °, After line cutting angle is more than 15 °, line cuts end A and can shorten, then line cuts end can The part reused will reduce, and target utilization rate also can reduce, and meeting butt welding is merged and connects Cause difficulty;The width of the monolithic spliced target after line cutting is equal to divided by the width of sputtering runway 0.2~1.2, the general and former target of length L is the longest.
(3) the residual target after cleaning line is cut is carried out with sandblasting or grinding.
(4) in Fig. 7 and embodiment illustrated in fig. 8, target and backboard seam, during seam Splicing sheet number is relevant with sputtering runway;Gap between the residual target of Fig. 3 is 0~2mm, solder layer Thickness 0.05~2mm.Installation uses, and the cross section using rear target is similar with Fig. 4, Fig. 4 In target utilization rate reached 42%.
The ultimate principle of the present invention and principal character and the present invention excellent has more than been shown and described Point.Skilled person will appreciate that of the industry, the present invention is not restricted to the described embodiments, on State the principle that the present invention is simply described described in embodiment and description, without departing from the present invention On the premise of spirit and scope, the present invention also has various changes and modifications, and these change and change Enter to both fall within scope of the claimed invention.Claimed scope is by appended power Profit claim and equivalent thereof define.

Claims (3)

1. the method improving use in magnetron sputtering coating target utilization rate, it is characterised in that Including following step:
(1) according to the sputtering runway of residual target, line is used to cut in the erosion curved surface of described residual target Cutting mill line cuts residual target, obtains multi-disc spliced target;
The choosing method of line of cut is: selecting width vertical line, described line of cut is vertical with width The angle of line is 15 °, and described width vertical line uses bosom and the width with residual target at residual target Degree direction is vertical;
The width of the monolithic spliced target after the cutting of described line is equal to divided by the width of sputtering runway 0.2~1.2, the residual target length before its length is cut with line is identical;
(2) each described spliced target is cleaned;
(3) spliced target after cleaning is stitched together, and by spliced target and the back of the body Plate seam, after seam, installation carries out sputter coating again;During splicing, each described spliced target it Between gap be 0~2mm;The seam surface of described backboard is provided with the backboard solder layer of low melting point, The seam surface of spliced target is sequentially provided with plasma spraying boundary layer and low from inside to outside The target solder layer of fusing point, described backboard solder layer connects with target solder layer soft soldering;Described backboard Solder layer is 0.05~2mm with the gross thickness of target solder layer.
The side of raising use in magnetron sputtering coating target utilization rate the most according to claim 1 Method, it is characterised in that
Also include before step (1) that residual target releases seam step.
The side of raising use in magnetron sputtering coating target utilization rate the most according to claim 1 Method, it is characterised in that
The material that described backboard uses is copper or titanium.
CN201410001386.8A 2014-01-02 2014-01-02 A kind of method improving use in magnetron sputtering coating target utilization rate Active CN103668098B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107032630A (en) * 2017-04-26 2017-08-11 张家港市铭斯特光电科技有限公司 A kind of method for glass magnetron sputtering plating

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106676485A (en) * 2017-01-04 2017-05-17 青岛蓝光晶科新材料有限公司 Production method for runway type silicon target material
CN111690903A (en) * 2020-05-22 2020-09-22 江西兴泰科技有限公司 Target material secondary utilization method

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2072086U (en) * 1990-06-09 1991-02-27 杨兆方 Cathode target for magnetron sputtering
US20090045051A1 (en) * 2007-08-13 2009-02-19 Stephane Ferrasse Target designs and related methods for coupled target assemblies, methods of production and uses thereof
CN101586228A (en) * 2009-02-05 2009-11-25 田小智 Method for improving utilization ratio of planar targets in magnetron sputtering coating system
CN101879640A (en) * 2009-05-06 2010-11-10 光洋应用材料科技股份有限公司 Ceramic sputtering target assembly and seaming method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2072086U (en) * 1990-06-09 1991-02-27 杨兆方 Cathode target for magnetron sputtering
US20090045051A1 (en) * 2007-08-13 2009-02-19 Stephane Ferrasse Target designs and related methods for coupled target assemblies, methods of production and uses thereof
CN101586228A (en) * 2009-02-05 2009-11-25 田小智 Method for improving utilization ratio of planar targets in magnetron sputtering coating system
CN101879640A (en) * 2009-05-06 2010-11-10 光洋应用材料科技股份有限公司 Ceramic sputtering target assembly and seaming method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107032630A (en) * 2017-04-26 2017-08-11 张家港市铭斯特光电科技有限公司 A kind of method for glass magnetron sputtering plating

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Address after: 215300 No. 135 CHENFENG East Road, Yushan Town, Kunshan City, Suzhou City, Jiangsu Province

Patentee after: Guangyang new material technology (Kunshan) Co.,Ltd.

Address before: 215300 No. 135 CHENFENG East Road, Wusongjiang Industrial Park, Kunshan City, Suzhou City, Jiangsu Province

Patentee before: KUNSHAN MULTIRESOURCE TECHNOLOGY Inc.