CN103655821B - Chinese medicine preparation of a kind of beneficial gas establishing-Yang and Tianjing Busuiye medicinal and preparation method thereof - Google Patents
Chinese medicine preparation of a kind of beneficial gas establishing-Yang and Tianjing Busuiye medicinal and preparation method thereof Download PDFInfo
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Abstract
The present invention relates to the field of Chinese medicines, relate in particular to Chinese medicine preparation of a kind of beneficial gas establishing-Yang and Tianjing Busuiye medicinal and preparation method thereof. The present invention takes following technical scheme: its raw material by following components by weight percent is prepared from: ginseng 90-140 part; Morinda officinalis 40-80 part; Pilose antler 15-25 part; Saline cistanche 50-70 part; Hippocampus 50-70 part; Bark of eucommia 50-70 part; Stone swallow 50-70 part; Barrenwort 100-140 part; Cloves 15-25 part; Impetuous 15-25 part; Gekko 15-25 part; Fructus Corni 100-130 part; Frutus cnidii 100-135 part; Oyster 100-135 part; Radix Astragali 900-1050 part; Earthworm 40-60 part; Chinese cassia tree 40-60 part; Fruit of Chinese magnoliavine 40-65 part. Adopt as above the present invention of technical scheme, there is following beneficial effect: beneficial gas establishing-Yang, Tianjing Busuiye medicinal, for the insufficiency of the kidney yang, having a dizzy spell due to deficiency of YIN-essence,impairment of YIN-essence, shortness of breath and fatigue, the diseases such as seminal emission. Find that there is fabulous result for the treatment of through clinical testing.
Description
Technical field
The present invention relates to the field of Chinese medicines, relate in particular to Chinese medicine preparation and the preparation side thereof of a kind of beneficial gas establishing-Yang and Tianjing Busuiye medicinalMethod.
Background technology
Along with modern's life pressure increases, increasing people is in sub-health state, current various beneficial gas body-buildingLiquid is more and more, but various result for the treatment of differs, and respectively has quality.
Western medicine is due to highly purified molecule cluster, and concentrated absorption is unavoidably in evil case, to all poisonous pairs of the heart, brain, liver, kidneyEffect.
Summary of the invention
The object of invention: for Chinese medicine preparation of a kind of beneficial gas establishing-Yang and Tianjing Busuiye medicinal and preparation method thereof is provided.
In order to reach as above object, the present invention takes following technical scheme: the preparation of its raw material by following components by weight percent andBecome: ginseng 90-140 part; Morinda officinalis 40-80 part; Pilose antler 15-25 part; Saline cistanche 50-70 part; Hippocampus 50-70 part; Bark of eucommia 50-70Part; Stone swallow 50-70 part; Barrenwort 100-140 part; Cloves 15-25 part; Impetuous 15-25 part; Gekko 15-25 part; Fructus Corni100-130 part; Frutus cnidii 100-135 part; Oyster 100-135 part; Radix Astragali 900-1050 part; Earthworm 40-60 part; Chinese cassia tree 40-60Part; Fruit of Chinese magnoliavine 40-65 part.
The further technical scheme of the present invention is, its raw material by following components by weight percent is prepared from: 120 parts of ginsengs; Bar60 parts, halberd sky; 20 parts, pilose antler; 60 parts of saline cistanches; 60 parts of hippocampus; 60 parts of the barks of eucommia; 60 parts, stone swallow; 120 parts of barrenwort; 20 parts of cloves;Impetuous 20 parts; 20 parts of gekkos; 120 parts of Fructus Cornis; 120 parts of frutus cnidiis; 120 parts of oysters; 1000 parts of the Radixs Astragali; 60 parts of earthworms; Meat60 parts, osmanthus; 60 parts, the fruit of Chinese magnoliavine.
The method of preparation preparation as above, is characterized in that: comprise following steps:
● just system: ginseng, Chinese cassia tree, cloves, the bark of eucommia are dried, and are ground into powder, cross 60 mesh sieves, mix with frutus cnidii;
● extraction and concentration: add 80% alcohol reflux and extract twice, add for the first time alcohol 4 volumes and doubly measure, extract 8 hours, theSecondary adds alcohol 2 volumes doubly to be measured, and extracts 6 hours, merges extract, filter, and decompression filtrate recycling ethanol, and be concentrated into relative densityMedicinal extract at 1.30～1.34,80 DEG C;
● decoct and concentrate: the dregs of a decoction and saline cistanche, Morinda officinalis, oyster, stone swallow, the fruit of Chinese magnoliavine, the seed of garden balsam, barrenwort, mountain ZhuCornel, Radix Astragali boiling three times, 10 volumes that add water for the first time are doubly measured, and decoct 2 hours, and 8 volumes that add water for the second time are doubly measured, and decoct 2Hour, 6 volumes that add water for the third time are doubly measured, decoct 1 hour, collecting decoction, filter, filtrate be concentrated into relative density 1.30～Medicinal extract at 1.34,80 DEG C; By pilose antler, hippocampus, gekko, earthworm oven dry, pulverizing, boiling twice, 8 volumes for the first time add waterDoubly amount, 6 volumes that add water for the second time are doubly measured, and decoct respectively 2 hours, collecting decoction, filters, filtrate be concentrated into relative density 1.30～Medicinal extract at 1.34,80 DEG C;
● regulate pH and concentrated: the dregs of a decoction add water, add hydrochloric acid and regulate pH value to 4.5～5.0, little in 100 DEG C of ordinary-pressure hydrolysis 24Time, filtering, filtrate adds 10% sodium hydroxide solution and regulates pH value to 6.5～7.0, filters, and filtrate decompression is concentrated into relative densityMedicinal extract at 1.30～1.34,80 DEG C.
The further technical scheme of the present invention is, also comprises the step of granulation, merges medicinal extract, mixes, and adds starch, mix,Dry, pulverize into fine powder, with sucrose, add ethanol granulation, be drying to obtain.
Adopt as above the present invention of technical scheme, there is following beneficial effect: beneficial gas establishing-Yang, Tianjing Busuiye medicinal, for kidney yangDeficiency, having a dizzy spell due to deficiency of YIN-essence,impairment of YIN-essence, shortness of breath and fatigue, the diseases such as seminal emission. Find that there is fabulous treatment effect through clinical testingReally.
Detailed description of the invention
Below embodiments of the invention are described, embodiment is not construed as limiting the invention:
Be below embodiments of the invention 1, i.e. optimum embodiment:
120 parts of [prescription] ginsengs, 60 parts of Morinda officinalis, 20 parts, pilose antler, 60 parts of saline cistanches, 60 parts of hippocampus, 60 parts of the barks of eucommia, stone swallow60 parts, 120 parts of barrenwort, 20 parts of cloves, impetuous 20 parts, 20 parts of gekkos, 120 parts of Fructus Cornis, 120 parts of frutus cnidiis, oyster 120Part, 1000 parts of the Radixs Astragali, 60 parts of earthworms, 60 parts of Chinese cassia trees, 60 parts, the fruit of Chinese magnoliavine.
[method for making] above 18 tastes, ginseng, Chinese cassia tree, cloves, the bark of eucommia are dried, and are ground into meal, mix with frutus cnidii, add80% alcohol reflux extracts twice, adds for the first time alcohol 4 volumes and doubly measures, and extracts 8 hours, adds for the second time alcohol 2 volumes and doubly measures, and extracts 6Hour, merge extract, filter, decompression filtrate recycling ethanol is to without alcohol taste, and is concentrated into relative density 1.30～1.34,80 DEG CUnder medicinal extract; The dregs of a decoction and saline cistanche, Morinda officinalis, oyster, stone swallow, the fruit of Chinese magnoliavine, the seed of garden balsam, barrenwort, Fructus Corni, the Radix Astragali add decoctingBoil three times, 10 volumes that add water for the first time are doubly measured, and decoct 2 hours, and 8 volumes that add water for the second time are doubly measured, and decoct 2 hours, add for the third timeWater 6 volumes are doubly measured, and decoct 1 hour, and collecting decoction, filters, and filtrate is concentrated into relative density 1.30～1.34, soaking at 80 DEG CCream; Four tastes such as all the other pilose antlers, oven dry, pulverizing, boiling twice, 8 volumes that add water for the first time are doubly measured, and 6 volumes for the second time add waterDoubly amount, decocts respectively 2 hours, and collecting decoction filters, and filtrate is concentrated into relative density 1.30～1.34, the medicinal extract at 80 DEG C; MedicineSlag adds water, and salt adding acid for adjusting pH value to 4.5～5.0, in 100 DEG C of ordinary-pressure hydrolysis 24 hours, filter, and filtrate adds 10% NaOHSolution regulates pH value to 6.5～7.0, filters, and filtrate decompression is concentrated into relative density 1.30～1.34, the medicinal extract at 80 DEG C; CloseAnd above-mentioned medicinal extract, mix, add starch 250g, mix, dry, pulverize into fine powder, with sucrose 500g, add Diluted Alcohol granulation,Dry, make 1000g, to obtain final product.
Embodiment 2; Method for making is with embodiment 1; Its formula is as follows:
Its raw material by following components by weight percent is prepared from: 90 parts of ginsengs; 40 parts of Morinda officinalis; 15 parts, pilose antler; Saline cistanche 50Part; 50 parts of hippocampus; 50 parts of the barks of eucommia; 50 parts, stone swallow; 100 parts of barrenwort; 15 parts of cloves; Impetuous 15 parts; 15 parts of gekkos; Fructus Corni100 parts; 100 parts of frutus cnidiis; 100 parts of oysters; 900 parts of the Radixs Astragali; 40 parts of earthworms; 40 parts of Chinese cassia trees; 40 parts, the fruit of Chinese magnoliavine.
Embodiment 3; Method for making is with embodiment 1; Its formula is as follows:
Its raw material by following components by weight percent is prepared from: 140 parts of ginsengs; 80 parts of Morinda officinalis; 25 parts, pilose antler; Saline cistanche 70Part; 70 parts of hippocampus; 70 parts of the barks of eucommia; 70 parts, stone swallow; 140 parts of barrenwort; 25 parts of cloves; Impetuous 25 parts; 25 parts of gekkos; Fructus Corni130 parts; 135 parts of frutus cnidiis; 135 parts of oysters; 1050 parts of the Radixs Astragali; 60 parts of earthworms; 60 parts of Chinese cassia trees; Fruit of Chinese magnoliavine 40-65 part.
[proterties] this product is tan particle; The micro-raw meat of gas, taste is sweet rear hardship first.
[discriminating] 1. gets this product 10g, and porphyrize adds chloroform 40ml, adds hot reflux 1 hour, discards chloroform solution, and the dregs of a decoction volatilize,The 0.5ml that adds water mix thoroughly moistening after, add water saturated n-butanol 20ml, ultrasonic processing 30 minutes, draws supernatant, adds 3 volumes doublyThe ammonia solution of amount, shakes up, and places layering, gets upper solution evaporate to dryness, and residue adds methyl alcohol 1ml to be made to dissolve, as need testing solution, anotherGet ginseng control medicinal material 1g, be made in the same way of control medicinal material solution. Get again ginsenoside Rb1, Re reference substance, add methyl alcohol and make often1ml, containing the mixed solution of 2mg, as according to product solution, according to thin-layered chromatography test, draws need testing solution and control medicinal material solutionEach 10 μ l, reference substance solution 5 μ l, put respectively on same silica gel g thin-layer plate, with chloroform-ethyl acetate-methanol-water (15: 40:22: 10) 10 DEG C of following lower floor's solution of placing are solvent, launch, and take out, and dry, spray is with 10% ethanol solution of sulfuric acid,105 DEG C are heated to clear spot. In test sample chromatogram, respectively with reference substance and the corresponding position of control medicinal material chromatogram on, aobviousThe spot of same color.
2. get this product 2g, porphyrize, adds ethanol 5ml, and ultrasonic processing 5 minutes is placed, and gets supernatant evaporate to dryness, and residue adds ethanol1ml makes to dissolve, as need testing solution. Separately get frutus cnidii control medicinal material 0.3g, be made in the same way of control medicinal material solution. Get again cnidium monnieriThe plain reference substance of son, adds ethanol and makes the solution of every 1ml containing 1mg, product solution in contrast. According to thin-layered chromatography test, draw and supplyTest sample solution 10 μ l, control medicinal material solution 2 μ l, reference substance solution 1 μ l, puts respectively on same silica gel g thin-layer plate, with benzene-vinegarAcetoacetic ester (30: 1) is solvent, launches, and takes out, and dries, and puts under ultraviolet lamp (365nm) and inspects, in test sample chromatogram, respectivelyWith reference substance chromatogram and the corresponding position of control medicinal material chromatogram on, the fluorescence spot of aobvious same color.
3. get this product 12g, porphyrize, adds chloroform-n-butanol (2: 1) mixed solution 75ml, puts and in water-bath, adds 30 points of hot refluxsClock, lets cool, filters, and filtrate evaporate to dryness, residue adds 2% potassium hydroxide methanol solution 50ml to be made to dissolve, and puts that in water-bath, to add hot reflux 1 littleTime, solution evaporate to dryness, the residue 30ml that adds water makes to dissolve, and moves in separatory funnel, with chloroform-n-butanol (2: 1) mixed solution 50mlJolting is extracted, and divides and gets chloroform-n-butanol layer, with 1% potassium dihydrogen phosphate 50ml washing, discards 1% potassium dihydrogen phosphate layer, carriesGet liquid evaporate to dryness, residue adds methyl alcohol 1ml to be made to dissolve, as need testing solution. Separately get Radix Astragali control medicinal material 3g, add methyl alcohol 20ml, returnFlow 1 hour, filter, it is upper that filtrate is added on neutral alumina column (100-120 order, 5g, internal diameter 10-15mm), with 40% methyl alcohol 100mlWash-out, collects eluent, evaporate to dryness, and the residue 30ml that adds water makes to dissolve, and extracts 2 times each 20ml merging with water saturated n-butanolN-butanol liquid, washes with water 2 times, and each 20ml, discards water liquid, n-butanol liquid evaporate to dryness, and residue adds methyl alcohol 0.5ml to be made to dissolve, and doesFor control medicinal material solution. Separately get Astragaloside IV reference substance, add methyl alcohol and make the solution of every 1ml containing 1mg, product solution in contrast,According to thin-layered chromatography test, draw the each 5 μ l of above-mentioned three kinds of solution, put respectively on same silica gel g thin-layer plate, with chloroform-acetic acidEthyl ester-methanol-water (15: 40: 22: 10) 10 DEG C of following lower floor's solution of placing are solvent, launch, and take out, dry, spray with10% ethanol solution of sulfuric acid, is heated to spot colour developing at 105 DEG C clear. In test sample chromatogram, corresponding with reference substance chromatogramOn position, aobvious identical sepia spot; Under ultraviolet lamp (365nm), aobvious identical orange-yellow fluorescence spot.
[inspection]
1. granularity: can not and can, by particle and the powder summation of No. five sieves, must not cross 15% by a sieve.
2. moisture: must not cross 6.0%.
3. melting: should all dissolve, must not have the foreign matters such as breeze, allow slight haze.
4. limit test of microbe:
[assay] is according to high effective liquid chromatography for measuring.
Chromatographic condition and system suitability: with octadecylsilane chemically bonded silica be filler; 0.075mol/L phosphorusAcid solution (with triethylamine adjusting pH value to 4.5)-acetonitrile (73: 27) is mobile phase; Detection wavelength is 270nm.. Number of theoretical plate is pressedIcariin peak calculates should be not less than 4000.
The preparation of reference substance solution: precision takes the icariin reference substance 10mg that is dried to constant weight at 105 DEG C, putsIn 100ml measuring bottle, dissolve and be diluted to scale with methyl alcohol, shaking up. Precision measures 5ml, puts in 10ml measuring bottle, adds mobile phase to carvingDegree, shakes up. Obtain and (in every 1ml, contain icariin 50 μ g).
The preparation of need testing solution: this product under content uniformity item, porphyrize, gets 3g, accurately weighed, put in 100ml measuring bottle,Precision adds 70% ethanol 50ml, weighed weight, and placement is spent the night, and ultrasonic processing 20 minutes, lets cool, more weighed weight, with 70%Ethanol is supplied the weight of less loss, shakes up, and filters, and gets subsequent filtrate, to obtain final product.
Determination method: accurate reference substance solution and the each 10 μ l of need testing solution of drawing respectively, injection liquid chromatography, measures,Obtain.
Every bag of this product is containing icariin (C33H40O15) must not be less than 2.0mg.
[function cures mainly] beneficial gas establishing-Yang, Tianjing Busuiye medicinal, for the insufficiency of the kidney yang, having a dizzy spell due to deficiency of YIN-essence,impairment of YIN-essence, breathes hardWeak, the diseases such as seminal emission.
[usage and dosage] boiling water is taken after mixing it with water, a 4g, and 2-3 time on the one, surrounding is a course for the treatment of.
[points for attention] (1) hypertrophy of the prostate person be cautious use of.
(2) hyperthyroidism, hyperpietic follow the doctor's advice.
[storage] seals, puts shady and cool dry place.
Known by above analysis, drug effect of the present invention is outstanding, has the splendid effect of curing the disease.
More than show and described general principle of the present invention, principal character and advantage of the present invention. The technology of this areaPersonnel should understand the present invention and not be restricted to the described embodiments, and that in above-described embodiment and description, describes just illustrates thisBright principle, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these variationsAll fall in claimed scope with improving.
Claims (2)
1. a Chinese medicine preparation for beneficial gas establishing-Yang and Tianjing Busuiye medicinal, is characterized in that, prepared by its raw material by following components by weight percentForm: ginseng 90-140 part; Morinda officinalis 40-80 part; Pilose antler 15-25 part; Saline cistanche 50-70 part; Hippocampus 50-70 part; Bark of eucommia 50-70 parts; Stone swallow 50-70 part; Barrenwort 100-140 part; Cloves 15-25 part; Impetuous 15-25 part; Gekko 15-25 part; Fructus Corni100-130 part; Frutus cnidii 100-135 part; Oyster 100-135 part; Radix Astragali 900-1050 part; Earthworm 40-60 part; Chinese cassia tree 40-60Part; Fruit of Chinese magnoliavine 40-65 part;
Comprise following steps:
● just system: ginseng, Chinese cassia tree, cloves, the bark of eucommia are dried, and are ground into powder, cross 60 mesh sieves, mix with frutus cnidii;
● extraction and concentration: add 80% alcohol reflux and extract twice, add for the first time alcohol 4 volumes and doubly measure, extract 8 hours, for the second timeAdd alcohol 2 volumes and doubly measure, extract 6 hours, merge extract, filter, decompression filtrate recycling ethanol, and be concentrated into relative density 1.30Medicinal extract at～1.34,80 DEG C;
● decoct and concentrate: the dregs of a decoction and saline cistanche, Morinda officinalis, oyster, stone swallow, the fruit of Chinese magnoliavine, the seed of garden balsam, barrenwort, Fructus Corni, HuangStilbene boiling three times, 10 volumes that add water for the first time are doubly measured, and decoct 2 hours, and 8 volumes that add water for the second time are doubly measured, decoct 2 hours,6 volumes that add water for the third time are doubly measured, and decoct 1 hour, and collecting decoction, filters, and filtrate is concentrated into relative density 1.30～1.34,80 DEG CUnder medicinal extract; By pilose antler, hippocampus, gekko, earthworm oven dry, pulverizing, boiling twice, 8 volumes that add water for the first time are doubly measured, and secondInferior 6 volumes that add water are doubly measured, and decoct respectively 2 hours, and collecting decoction, filters, and filtrate is concentrated into relative density 1.30～1.34,80 DEG CUnder medicinal extract;
Regulate pH and concentrated: the dregs of a decoction add water, salt adding acid for adjusting pH value to 4.5～5.0, in 100 DEG C of ordinary-pressure hydrolysis 24 hours, filterCross, filtrate add 10% sodium hydroxide solution regulate pH value to 6.5～7.0, filtration, filtrate decompression be concentrated into relative density 1.30～Medicinal extract at 1.34,80 DEG C.
2. the Chinese medicine preparation of a kind of beneficial gas establishing-Yang as claimed in claim 1 and Tianjing Busuiye medicinal, is characterized in that, it is by weighing as followsThe raw material of amount component is prepared from: 120 parts of ginsengs; 60 parts of Morinda officinalis; 20 parts, pilose antler; 60 parts of saline cistanches; 60 parts of hippocampus; The bark of eucommia 60Part; 60 parts, stone swallow; 120 parts of barrenwort; 20 parts of cloves; Impetuous 20 parts; 20 parts of gekkos; 120 parts of Fructus Cornis; 120 parts of frutus cnidiis;120 parts of oysters; 1000 parts of the Radixs Astragali; 60 parts of earthworms; 60 parts of Chinese cassia trees; 60 parts, the fruit of Chinese magnoliavine.
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| CN104678045A (en) * | 2014-12-18 | 2015-06-03 | 南方医科大学 | Method for detecting radix sophorae flavescentis-eucalyptus robusta rash-eliminating gel medicine |
| CN104522236A (en) * | 2014-12-19 | 2015-04-22 | 青岛崂好人海洋生物技术有限公司 | Method for preparing spirifer composite health tea pills |
| CN105147838B (en) * | 2015-09-30 | 2018-09-11 | 北华大学 | With the immune composition and its preparation method and application with antifatigue effect of enhancing |
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