CN103655688B - A kind of natural high-content wild marjoram perfume (or spice) phenol extraction method - Google Patents
A kind of natural high-content wild marjoram perfume (or spice) phenol extraction method Download PDFInfo
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- CN103655688B CN103655688B CN201310589902.9A CN201310589902A CN103655688B CN 103655688 B CN103655688 B CN 103655688B CN 201310589902 A CN201310589902 A CN 201310589902A CN 103655688 B CN103655688 B CN 103655688B
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Abstract
The present invention relates to a kind of natural high-content wild marjoram perfume (or spice) phenol extraction methods, it is combined for the first time using water vapour circumfluence method, alcohol opposing steam flow method, the active ingredient in wild marjoram grass is made to obtain maximum extraction, solves the chemical industry synthesis of wild marjoram perfume (or spice) phenol, so as to which the cost that wild marjoram perfume (or spice) phenol is made to be extracted from pure natural wild marjoram herb substantially reduces, and purification rate is high, can make it possible natural wild marjoram perfume (or spice) phenol in industry extensively using.
Description
Technical field
The present invention relates to herding veterinary drug technology for producing fields, more particularly to a kind of naturally to extract wild marjoram from wild marjoram grass
The method of fragrant phenol, specifically a kind of natural high-content wild marjoram perfume (or spice) phenol extraction method.
Background technology
Wild marjoram also known as stop dysentery grass, Elsholtzia patrini garcke, south Sinkiang ziziphora herb are Labiatae Origanum herbaceos perennial.Main distribution
In Mediterranean Region to the Central Asia, north African, North America and China's most area, it is born in the hillside, roadside, filling of height above sea level 500-3600m
Clump, meadow, hayashishita.Wild marjoram acrid flavour, cool in nature, nontoxic, herb can be used as medicine, and there is relieving superficies by cooling, qi-regulating dampness elimination to fall to urinate the work(of detumescence
Effect, wild marjoram contains more than 30 kinds of antimicrobial compound, is a kind of potential natural antibiotics and drug growth promoter
The wild marjoram perfume (or spice) phenol extracted from wild marjoram, cause enteritis bacterium common to 31 kinds and shigella flexneri are most wide
The pure Chinese medicine additive of antibacterial is composed, origanum oil is one of feed medicated premix that the approval of the Ministry of Agriculture of China uses, and is had
The Chinese medicine additive for having pure natural active composition safe efficient, green, without incompatibility higher.
At present, due to extracting wild marjoram perfume (or spice) phenol from natural wild marjoram grass, purification rate is not high, of high cost, and purifies ox out
It is impure to volatile oil component, lead to most of feed additive industry, majority uses artificial synthesized wild marjoram perfume (or spice) phenol.
Invention content
The purpose of the present invention is overcoming drawbacks described above, a kind of natural high-content wild marjoram perfume (or spice) phenol extraction method is provided, is adopted for the first time
It is combined with water vapour circumfluence method, alcohol opposing steam flow method, the active ingredient in wild marjoram grass is made to obtain maximum extraction, solves ox
To the chemical industry synthesis of fragrant phenol, so as to which the cost that wild marjoram perfume (or spice) phenol is made to be extracted from pure natural wild marjoram herb substantially reduces, and purify
Rate is high, can make it possible natural wild marjoram perfume (or spice) phenol in industry extensively using.
The present invention solves the following technical scheme that above-mentioned technical problem uses：
A kind of natural high-content wild marjoram perfume (or spice) phenol extraction method, it is characterised in that：Specific method step is as follows：
1st, after wild marjoram herb is taken to crush, 30 mesh are crushed to, 1 part of wild marjoram grass meal adds 8~10 times of purified waters, impregnates 6 hours, will
Steam is passed through in extractor, and the temperature in tank is made to rise at 90 DEG C~100 DEG C, and pressurize 0.1~0.2MPa, and heat reflux 4~6 is small
When, after cooler cools down, obtain origanum volatile oil mixed liquor.
2nd, wild marjoram herbal medicine slag adds 6~8 times of 70% ethyl alcohol, and steam is passed through in extractor, make the temperature in tank rise to 90 DEG C~
At 100 DEG C, pressurize 0.1~0.2MPa, and heat reflux 2 hours extracts 2 times, after cooler cools down, it is molten to obtain origanum volatile oil alcohol
Liquid.
3rd, merge origanum volatile oil mixed liquor and origanum volatile oil alcoholic solution, detached into oil water separator, obtain wild marjoram
Fragrant phenol.
The beneficial effects of the invention are as follows：For the first time using water vapour circumfluence method, alcohol opposing steam flow method is combined is in wild marjoram grass
Active ingredient obtain maximum extraction, the chemical industry synthesis for solving wild marjoram perfume (or spice) phenol, so as to make wild marjoram perfume (or spice) phenol from pure natural ox
The cost extracted into herb substantially reduces, and purification rate is high, can make natural wild marjoram perfume (or spice) phenol in industry extensively using into
It is possible.
Specific embodiment
Specific embodiment is further described a kind of natural high-content wild marjoram perfume (or spice) phenol extraction method of the present invention below.
A kind of natural high-content wild marjoram perfume (or spice) phenol extraction method, it is characterised in that：Specific method step is as follows：
1st, after wild marjoram herb is taken to crush, 30 mesh are crushed to, 1 part of wild marjoram grass meal adds 8~10 times of purified waters, impregnates 6 hours, will
Steam is passed through in extractor, and the temperature in tank is made to rise at 90 DEG C~100 DEG C, and pressurize 0.1~0.2MPa, and heat reflux 4~6 is small
When, after cooler cools down, obtain origanum volatile oil mixed liquor；
2nd, wild marjoram herbal medicine slag adds 6~8 times of 70% ethyl alcohol, and steam is passed through in extractor, make the temperature in tank rise to 90 DEG C~
At 100 DEG C, pressurize 0.1~0.2MPa, and heat reflux 2 hours extracts 2 times, after cooler cools down, it is molten to obtain origanum volatile oil alcohol
Liquid；
3rd, merge origanum volatile oil mixed liquor and origanum volatile oil alcoholic solution, detached into oil water separator, obtain wild marjoram
Fragrant phenol.
One kind of embodiment described above, only more preferably specific embodiment of the invention, those skilled in the art
The usual variations and alternatives that member carries out in the range of technical solution of the present invention should all include within the scope of the present invention.
Claims (1)
- A kind of 1. natural high-content wild marjoram perfume (or spice) phenol extraction method, it is characterised in that：Specific method step is as follows：（1）, wild marjoram herb is taken to crush after, be crushed to 30 mesh, 1 part of wild marjoram grass meal adds 8~10 times of purified waters, impregnates 6 hours, will steam Vapour is passed through in extractor, and the temperature in tank is made to rise at 90 DEG C~100 DEG C, and pressurize 0.1~0.2MPa, heat reflux 4~6 hours, After cooler cools down, origanum volatile oil mixed liquor is obtained；（2）, wild marjoram herbal medicine slag add 6~8 times of 70% ethyl alcohol, steam is passed through in extractor, make the temperature in tank rise to 90 DEG C~ At 100 DEG C, pressurize 0.1~0.2MPa, and heat reflux 2 hours extracts 2 times, after cooler cools down, it is molten to obtain origanum volatile oil alcohol Liquid；（3）, merge origanum volatile oil mixed liquor and origanum volatile oil alcoholic solution, detached into oil water separator, obtain wild marjoram perfume Phenol.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310589902.9A CN103655688B (en) | 2013-11-20 | 2013-11-20 | A kind of natural high-content wild marjoram perfume (or spice) phenol extraction method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310589902.9A CN103655688B (en) | 2013-11-20 | 2013-11-20 | A kind of natural high-content wild marjoram perfume (or spice) phenol extraction method |
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| CN103655688A CN103655688A (en) | 2014-03-26 |
| CN103655688B true CN103655688B (en) | 2018-06-26 |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111632043A (en) * | 2020-06-05 | 2020-09-08 | 中农牧生物科技(厦门)有限公司 | Plant essential oil for improving poultry respiratory diseases and preparation method thereof |
| CN113499362A (en) * | 2021-07-10 | 2021-10-15 | 四川成邦药业有限公司 | Preparation method and preparation device of liquid oregano phenol containing organic acid |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1943619A (en) * | 2006-11-03 | 2007-04-11 | 湖北福人药业股份有限公司 | Method for preparing Chinese medicine volatile oil of origanum and soft capsule thereof |
| CN102935110A (en) * | 2012-11-02 | 2013-02-20 | 青岛康地恩药业股份有限公司 | Coated granules containing natural oregano oil for birds and preparation method thereof |
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2013
- 2013-11-20 CN CN201310589902.9A patent/CN103655688B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1943619A (en) * | 2006-11-03 | 2007-04-11 | 湖北福人药业股份有限公司 | Method for preparing Chinese medicine volatile oil of origanum and soft capsule thereof |
| CN102935110A (en) * | 2012-11-02 | 2013-02-20 | 青岛康地恩药业股份有限公司 | Coated granules containing natural oregano oil for birds and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 从紫丁香中提取丁子香酚研究;张宏波;《齐齐哈尔大学学报》;20010331;第17卷(第01期);40-42页 * |
| 牛至药材的质量标准研究;张潇月;《成都中医药大学硕士学位论文》;20111230;第1页 * |
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Denomination of invention: Method for extracting natural high-content oregano fragrant phenol Effective date of registration: 20190813 Granted publication date: 20180626 Pledgee: Agricultural Bank of China, Limited by Share Ltd, Longyan, Xinluo branch Pledgor: FUJIAN JONORM BIOLOGICAL PHARMACEUTICAL CO., LTD. Registration number: Y2019990000064 |
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