CN103626314A - Technology for treating nanofiltration concentrated solution of garbage leachate and special device - Google Patents
Technology for treating nanofiltration concentrated solution of garbage leachate and special device Download PDFInfo
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- CN103626314A CN103626314A CN201310548722.6A CN201310548722A CN103626314A CN 103626314 A CN103626314 A CN 103626314A CN 201310548722 A CN201310548722 A CN 201310548722A CN 103626314 A CN103626314 A CN 103626314A
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Abstract
The invention discloses a technology for treating a nanofiltration concentrated solution of garbage leachate. The technology is characterized by comprising the steps of pretreatment, first-stage film treatment and second-stage film treatment. According to the technology, a two-stage material film system is used for concentrating and separating the nanofiltration concentrated solution of the garbage leachate to extract macromolecular organic humic acids which are difficultly biochemical degraded, and the reduction of the concentrated solution is realized; meanwhile, the recycling rate of water for nanofiltration treatment is improved; according to the technology, wastewater is reused, so that the cost is saved, and the pollution to the environment is relieved.
Description
Technical field
The invention belongs to environmental technology field; specifically just relate to a kind of technique and special purpose device that the nanofiltration concentrated solution of percolate is processed; this technique extracted humic acid realize concentrated solution minimizing and process from the nanofiltration concentrated solution of percolate; realized the recycling of percolate; reduce the amount of concentrated solution, protected environment.
Background technology
Along with increasing of China's city quantity increase and population, municipal wastes is also with sharp increase, and the situation of garbage-surrounded city is very severe.At present, refuse treatment mainly be take landfill and burning as main, wherein landfill remains main mode, and accounting, between 45%-50%, is burned accounting 12% left and right, another still have 30% domestic refuse to fail to process, compare with landfill, burning method can effectively reduce rubbish capacity more than 75%, saves soil, be difficult for to produce the pollutions such as sewage permeation, and produce calorific value and can be used for heat supply, generating etc. and recycle.Therefore, the processing mode of waste incineration will be widelyd popularize.
But refuse treatment is no matter be to take landfill, or the mode of burning, the processing of percolate is all technical barrier wherein.Percolate belongs to high concentration hard-degraded organic waste water, have that complicated component, Pollutant levels are high, biological nutrition proportional imbalance, colourity be high, the feature that stink is large, biodegradability is poor, therefore, the processing of percolate is faced with the insoluble technical barrier of some always.At present, percolate mainly adopts the main process of biochemical system+MBR+ nanofiltration+reverse-osmosis treated, makes waste water can reach emission standard.The larger molecular organics matter humic acids that contains a large amount of bio-refractories in the concentrated solution of percolate after nanofiltration is processed, it accounts for the more than 70% of total organic matter, and environment and biochemical treatment system are made a big impact.At present, the processing mode of the nanofiltration concentrated solution of percolate is faced with following problem:
First, concentrated solution is directly in the existing technique of bringing back to life systematic influence system processing power, the nanofiltration concentrated solution of percolate directly returns to biochemical treatment system conventionally, humic acid is difficult to biochemical degradation in system, can build up, its concentration in system is more and more higher, finally affects the processing power of whole treatment system.
Secondly, at garbage incinerating power plant, a large amount of nanofiltration concentrated solutions conventionally returns spray and burns, but in returning spray burning process, not only heat-energy losses is large, and can cause very large corrosion to burning facility, shortens the life-span of burning facility, increase the body of heater cost of overhaul, this mode can cause huge financial loss to incineration plant.
The 3rd, flyash curing is dissolved limited in one's ability, and at garbage incinerating power plant, partial concentration liquid is generally used for flyash curing, but dissolving of flyash curing is limited in one's ability, for garbage incinerating power plant, can produce a large amount of concentrated solutions every day, and this kind of mode is difficult to its whole timely and effective dissolving, and stability is poor in the process of solidifying incineration of refuse flyash, easily produce flying dust swelling, as fast in speed of expansion, sample cracking even destroys etc.
The 4th, high and the wasting of resources of chemical oxidation treatment cost, some enterprise adopts the method for chemical oxidation to process when processing this partial concentration liquid, as Ozonation, catalytic oxidation etc., the speed of this kind of method processing humic acid is fast, efficiency is high, product (carbonic acid gas and water) does not produce pollution to environment, but this mode needs to add a large amount of oxygenants in treating processes, cost is higher, and humic acid is a kind of macromolecule organic, in agriculture production, can be used as organic fertilizer and composting raw material, directly removed, it is a kind of huge wasting of resources.Therefore, chemical oxidation is inapplicable in actual procedure.
Chinese Patent Application No. 201210289032.9 discloses a kind of percolate advanced treatment process, and the water outlet first percolate being obtained through MBR system is carried out one-level nanofiltration processing and obtained one-level nanofiltration product water and concentrated solution; Then by processing through one-level nanofiltration the product water obtaining, carry out reverse-osmosis treated, concentrated solution carries out the one-level that one-level membrane separation obtains and sees through liquid and one-level concentrated solution; Then one-level step being obtained sees through liquid and carries out secondary nanofiltration processing, and one-level concentrated solution carries out secondary membrane separation and obtains secondary through liquid and secondary concentrated solution; Finally the secondary obtaining in the 3rd step is seen through to liquid and proceed one-level membrane separation, secondary concentrated solution as fertilizer sources is used.This technology is just processed for garbage filter night, still can exist nanofiltration concentrated solution to exist and cannot obtain fully effective processing.
Summary of the invention
The object of the invention is the technical barrier that the nanofiltration concentrated solution for existing percolate cannot be effectively addressed, a kind of nanofiltration concentrated solution treatment process and special purpose device of percolate are provided, can from the nanofiltration concentrated solution of percolate, extract humic acids, improved the recovery utilization rate of water simultaneously, increase the economic benefit of garbage leachate treatment process, reduced the pollution of percolate to environment.
Technical scheme
In order to realize above-mentioned technical purpose, the present invention designs a kind of nanofiltration concentrated solution treatment process of percolate, and it comprises the following steps:
First, nanofiltration concentrated solution is passed into pretreatment system and carries out water quality regulation, the pH value that regulates nanofiltration concentrated solution 4~9, redox potential ORP is adjusted to 150-250mV, is beneficial to the concentrating and separating to humic acids;
Then water outlet after pretreatment is utilized to membrane sepn mode, under 10-30bar pressure condition, make non-target component obtain seeing through liquid by membrane sepn mode, and humic acids is trapped within concentrated solution, form humic acids dope, finally obtain concentration ratio and go out through pre-treatment the humic acids dope that water concentration improves 30~60 times;
Finally, by seeing through liquid and further adopt the mode of membrane sepn, under 5-15bar pressure condition, make water obtain filtered solution by membrane sepn mode, and solute is trapped within through in liquid, thereby the rate of recovery that obtains water is between 65-85%;
In order to realize above-mentioned technique, the present invention also designs a kind of special purpose device of nanofiltration concentrated solution treatment process of rubbish percolate, it is characterized in that: it comprises raw water box, raw water box exit end connects pretreatment system, the first intake pump is housed on the connecting pipeline of raw water box and pretreatment system, pretreatment system output terminal is connected with one-level accurate filter, the output terminal of one-level accurate filter is connected to a stage material membrane module, on one-level accurate filter and a stage material membrane module connecting pipeline, high-pressure pump is housed, the liquid outlet that sees through of one stage material membrane module is connected to the middle water tank that produces, concentrated solution outlet is connected to humic acid collection box, the middle water tank exit end that produces is connected to secondary accurate filter, middle producing on water tank and secondary accurate filter connecting pipeline is equipped with the second intake pump, secondary accurate filter output terminal is connected to two stage material membrane modules, , on secondary accurate filter and two stage material membrane module connecting pipelines, secondary high-pressure pump is housed, two stage material film groups are produced water out and are connected back raw water box, concentrated solution outlet connects can biochemical system water tank.
Beneficial effect
The present invention adopts two stage material film systems to carry out concentrating and separating to the nanofiltration concentrated solution of percolate, extract the larger molecular organics humic acid of bio-refractory, and realized concentrated solution minimizing, also improved the rate of recovery of the water of nanofiltration processing simultaneously, this Technology has been carried out regeneration to waste water, save cost, reduced the pollution to environment.
Accompanying drawing explanation
Accompanying drawing 1 is process flow sheet of the present invention.
Accompanying drawing 2 is special purpose device connection diagrams in the present invention.
Embodiment
Below in conjunction with drawings and Examples, the present invention will be further described.
Embodiment
As shown in Figure 1,1, a kind of nanofiltration concentrated solution treatment process of percolate, it is characterized in that, it comprises the following steps:
First, nanofiltration concentrated solution is passed into pretreatment system and carries out water quality regulation, the pH value that regulates nanofiltration concentrated solution 4~9, redox potential ORP is adjusted to 150-250mV, is beneficial to the concentrating and separating to humic acids;
Then, to utilize membrane sepn mode through the pretreated water outlet of step (1), under 10-30bar pressure condition, make non-target component obtain seeing through liquid by membrane sepn mode, and humic acids is trapped within concentrated solution, form humic acids dope, finally obtain concentration ratio and go out through pre-treatment the humic acids dope that water concentration improves 30~60 times;
Then, the mode that liquid further adopts membrane sepn that sees through by step (2), make water obtain filtered solution by membrane sepn mode, and solute is trapped within through in liquid under 5-15bar pressure condition, thereby the rate of recovery that obtains water is between 65-85%;
Further, by the filtered solution obtaining, again pass into nanofiltration and produce water, further promote the rate of recovery of nanofiltration concentrated solution.
Further, by again pass into the biochemical treatment system of percolate through liquid, further improve the recovery utilization rate that sees through liquid.
A kind of special purpose device of the nanofiltration concentrated solution treatment process for above-mentioned rubbish percolate, it is characterized in that: it comprises raw water box 1, raw water box 1 exit end connects pretreatment system 2, the first intake pump 3 is housed on the connecting pipeline of raw water box 1 and pretreatment system 2, pretreatment system 2 output terminals are connected with one-level accurate filter 4, the output terminal of one-level accurate filter 4 is connected to a stage material membrane module 5, on one-level accurate filter 4 and stage material membrane module 5 connecting pipelines, high-pressure pump 6 is housed, the liquid outlet that sees through of one stage material membrane module 5 is connected to the middle water tank 7 that produces, concentrated solution outlet is connected to humic acid collection box 8, middle water tank 7 exit end that produce are connected to secondary accurate filter 9, middle producing on water tank 4 and secondary accurate filter 9 connecting pipelines is equipped with the second intake pump 10, secondary accurate filter 9 output terminals are connected to two stage material membrane modules 11, , on secondary accurate filter 9 and two stage material membrane module 11 connecting pipelines, secondary high-pressure pump 12 is housed, two stage material membrane modules 11 produce water out and connect back raw water box 1, concentrated solution outlet connects can biochemical system water tank.
Further, in a described stage material membrane module 5 and two stage material membrane modules 11, recycle pump is all housed, removes the pollutant sediment on film surface.
Further, the two ends of a described stage material membrane module 5 and two stage material membrane modules 11 are connected to film cleaning equipment.
The present invention adjusted the nanofiltration concentrated solution of percolate after water quality before entering pretreatment system 2, first passed through material raw water box 1, water quality and quantity was adjusted, for pretreatment system 2 provides the water source of continous-stable; The water outlet of raw water box 1 promotes and enters pretreatment system 2 through the first intake pump 3, carries out water quality regulation to weak acid environment, prevents one-level film surface scale, is easy to carry out membrane sepn; Then the water outlet through pretreatment system 2 enters a stage material membrane module 5, by one-level high-pressure pump 6 adherence pressures, waste water sees through diaphragm under pressure-driven, produce dense water and see through liquid, dense water mainly contains humic acid, can be recovered utilization, see through liquid concentration and reduce, can enter the further recycle-water of two stage material membrane modules 11; Then by one-level film saw through liquid before entering two stage material film units 5, in the middle of being introduced into, produce water tank 7,7 pairs of water quality and quantities of intermediate water tank are adjusted, for two stage material membrane modules 11 provide the water source of continous-stable; The water outlet of intermediate water tank 7 enters two stage material membrane modules 11, by secondary high-pressure pump 12 adherence pressures, waste water sees through diaphragm under pressure-driven, further concentrating and separating, dense water mainly contains small organic molecule matter, can return to biochemical system recycle, produce water and can be incorporated to nanofiltration product water, improve the water rate of recovery.
The present invention adopts two stage material film systems to carry out concentrating and separating to the nanofiltration concentrated solution of percolate, extract the larger molecular organics humic acid of bio-refractory, and realized concentrated solution minimizing, also improved the rate of recovery of the water of nanofiltration processing simultaneously, this Technology has been carried out regeneration to waste water, save cost, reduced the pollution to environment.
Claims (6)
1. a nanofiltration concentrated solution treatment process for percolate, is characterized in that, it comprises the following steps:
(1) nanofiltration concentrated solution is passed into pretreatment system and carries out water quality regulation, the pH value that regulates nanofiltration concentrated solution 4~9, redox potential ORP is adjusted to 150-250mV, is beneficial to the concentrating and separating to humic acids;
(2) will utilize membrane sepn mode through the pretreated water outlet of step (1), under 10-30bar pressure condition, make non-target component obtain seeing through liquid by membrane sepn mode, and humic acids is trapped within concentrated solution, form humic acids dope, finally obtain concentration ratio and go out through pre-treatment the humic acids dope that water concentration improves 30~60 times;
(3) by the mode that liquid further adopts membrane sepn that sees through to step (2), under 5-15bar pressure condition, make water obtain filtered solution by membrane sepn mode, and solute is trapped within through in liquid, thereby the rate of recovery that obtains water is between 65-85%.
2. the nanofiltration concentrated solution treatment process of a kind of percolate according to claim 1, is characterized in that: the filtered solution obtaining in described step (3), and again pass into nanofiltration and produce water, further promote the rate of recovery of nanofiltration concentrated solution.
3. the nanofiltration concentrated solution treatment process of a kind of percolate according to claim 1, is characterized in that: in described step (2), see through the biochemical treatment system that liquid passes into percolate again, further improve the recovery utilization rate that sees through liquid.
4. the special purpose device for the nanofiltration concentrated solution treatment process of above-mentioned rubbish percolate, it is characterized in that: it comprises raw water box (1), raw water box (1) exit end connects pretreatment system (2), the first intake pump (3) is housed on the connecting pipeline of raw water box (1) and pretreatment system (2), pretreatment system (2) output terminal is connected with one-level accurate filter (4), the output terminal of one-level accurate filter (4) is connected to a stage material membrane module (5), on one-level accurate filter (4) and stage material membrane module (5) connecting pipeline, high-pressure pump (6) is housed, the liquid outlet that sees through of one stage material membrane module (5) is connected to the middle water tank (7) that produces, concentrated solution outlet is connected to humic acid collection box (8), middle water tank (7) exit end that produces is connected to secondary accurate filter (9), middle producing on water tank (4) and secondary accurate filter (9) connecting pipeline is equipped with the second intake pump (10), secondary accurate filter (9) output terminal is connected to two stage material membrane modules (11), on secondary accurate filter (9) and two stage material membrane module (11) connecting pipelines, secondary high-pressure pump (12) is housed, two stage material membrane modules (11) produce water out and connect back raw water box (1), concentrated solution outlet connects can biochemical system water tank.
5. the special purpose device of the nanofiltration concentrated solution treatment process of a kind of percolate as claimed in claim 4, it is characterized in that: in a described stage material membrane module (5) and two stage material membrane modules (11), recycle pump is all housed, removes the pollutant sediment on film surface.
6. the special purpose device of the nanofiltration concentrated solution treatment process of a kind of percolate as claimed in claim 4, is characterized in that: the two ends of a described stage material membrane module (5) and two stage material membrane modules (11) are connected to film cleaning equipment.
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CN104230051A (en) * | 2014-09-04 | 2014-12-24 | 上海晶宇环境工程有限公司 | Landfill leachate reverse osmosis concentrated solution treatment process and special equipment thereof |
CN104310659A (en) * | 2014-11-12 | 2015-01-28 | 福州大学 | Separating reclaiming technology for humic acid in garbage leachate MBR+NF concentrated liquid containing high concentration of SO42 |
CN104496079A (en) * | 2014-12-23 | 2015-04-08 | 北京桑德环境工程有限公司 | Treatment method for garbage leachate membrane concentrated solution |
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CN102951741A (en) * | 2012-08-14 | 2013-03-06 | 上海晶宇环境工程有限公司 | Landfill leachate deep processing technology and special equipment |
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CN104310659B (en) * | 2014-11-12 | 2016-06-01 | 福州大学 | Containing high density SO42-Percolate MBR+NF concentrated solution in humic acids process for separating and recovering |
CN104310659A (en) * | 2014-11-12 | 2015-01-28 | 福州大学 | Separating reclaiming technology for humic acid in garbage leachate MBR+NF concentrated liquid containing high concentration of SO42 |
CN104496079A (en) * | 2014-12-23 | 2015-04-08 | 北京桑德环境工程有限公司 | Treatment method for garbage leachate membrane concentrated solution |
CN105293662A (en) * | 2015-11-24 | 2016-02-03 | 福州大学 | Method for removing and recycling high-concentration Ca<2+> and Mg<2+> in leachate MBR and NF concentrate |
CN105777819A (en) * | 2016-05-10 | 2016-07-20 | 上海晶宇环境工程股份有限公司 | Process for extracting fulvic acid from garbage leachate membrane concentrated liquid and special device thereof |
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CN106397790A (en) * | 2016-10-21 | 2017-02-15 | 中国环境科学研究院 | Extraction equipment for hydrophilic-hydrophobic humic acid in water |
CN106519259B (en) * | 2016-10-21 | 2018-03-09 | 中国环境科学研究院 | A kind of equipment for extracting water body fulvic acid |
CN106496592B (en) * | 2016-10-21 | 2018-03-09 | 中国环境科学研究院 | Equipment for extracting hydrophobic humic acid in water body |
CN106397790B (en) * | 2016-10-21 | 2018-06-08 | 中国环境科学研究院 | The double property humic acid extraction equipments of hydrophilic-hydrophobic in a kind of water body |
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CN109354292B (en) * | 2018-12-14 | 2021-11-19 | 湖南军信环保股份有限公司 | Reduction treatment process for landfill leachate membrane filtration concentrated solution |
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CN110550785A (en) * | 2019-10-14 | 2019-12-10 | 广州市适然环境工程技术有限公司 | Nanofiltration concentrated solution softening treatment device for landfill leachate |
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CN112919694A (en) * | 2021-01-27 | 2021-06-08 | 成都硕特环保科技有限公司 | Integrated treatment method and system for leachate of garbage transfer station |
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