CN103621787B - A kind of green non-pollution slowly-releasing fertilizer efficiency aquatic fertilizer and preparation method thereof - Google Patents
A kind of green non-pollution slowly-releasing fertilizer efficiency aquatic fertilizer and preparation method thereof Download PDFInfo
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- CN103621787B CN103621787B CN201310563672.9A CN201310563672A CN103621787B CN 103621787 B CN103621787 B CN 103621787B CN 201310563672 A CN201310563672 A CN 201310563672A CN 103621787 B CN103621787 B CN 103621787B
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Abstract
Disclosed by the invention is a kind of green non-pollution slowly-releasing fertilizer efficiency aquatic fertilizer and preparation method thereof, and feedstuff consists of soybean lecithin, soda ash, citric acid, bacterium chaff part, rice bran, wheat bran, brown sugar and microbe additive etc.Preparation method's step: (1) mixes soybean lecithin, soda ash, citric acid be stirred into puff; (2) microbe additive and water are configured to active bacteria liquid; (3) after all the other components mix, put into fermentation tank fermentation, and pass into hydrogen peroxide and to carry out disinfection sterilization processing; (4) the active bacteria liquid in step (2) is added in the ratio of material 15%-45% in fermentation tank; (5) temperature in fermentation tank is set to 35-40 DEG C; (6) aquaculture feed will fermented, through 50-80 DEG C of oven dry, then cools, obtains aquaculture feed.Present invention alleviates environmental pollution, edible Safety of Aquatic Products of the present invention is convenient to the situation of ingesting that user observes aquatic products simultaneously.
Description
technical field:
The present invention relates to a kind of aquaculture feed and preparation method thereof, be specifically related to a kind of green non-pollution slowly-releasing fertilizer efficiency aquatic fertilizer and preparation method thereof, belong to culture fishery.
background technology:
At present, China's feed industrial development is rapid, to make greater efforts to promote the development of aquaculture, but the chemicals contained in general feed comprises the harmful substances such as sex hormone, growth hormone, antibiotic and heavy metal to exceed standard, very serious to the pollution of the Nature, also be unfavorable for the growth of animal simultaneously, especially aquaculture feed, harmful substance in feed cannot be absorbed by fishes and shrimps, be discharged in water with the form of ight soil, cause water pollution, even some remains in fishes and shrimps body and is consumed directly by humans, and is detrimental to health.Utilize hydroxyapatite etc. itself to have the character of loose structure, fertilizer components is adsorbed in the inner mesh of carrier, reach the object of slow releasing.Hydroxyapatite also has biodegradability properties, and gained catabolite is various trace elements ion, and these elements can be gradually resorbed.Nano controlled-release additive has good biocompatibility, gastrointestinal tract mucous compatibility, each component making it load has controlled-release function, all improve a lot through twice-modified nano-complex drugloading rate and adsorbance, fertilizer efficiency time lengthening more than 3 months, the increment of effective suppression animal pathogen, improves the benefit of the producer.
summary of the invention:
The present invention seeks to, be used for making up the deficiencies in the prior art, and a kind of Safety of Aquatic Products is provided, alleviates environmental pollution, be convenient to user simultaneously and observe aquaculture feed of the situation of ingesting of aquatic products and preparation method thereof.
A kind of green non-pollution slowly-releasing of the present invention fertilizer efficiency aquatic fertilizer, raw material consists of soybean lecithin, soda ash, citric acid, bacterium chaff, rice bran, wheat bran, brown sugar, powdered whiting, urea and microbe additive; Each constituent content is respectively by mass fraction: soybean lecithin 55-65 part, soda ash 35-40 part, citric acid 20-40 part, bacterium chaff 45-95 part, rice bran 35-75 part, wheat bran 40-85 part, brown sugar 5-8 part and microbe additive 4-8 part, composite feeding promoting agent 0.2-0.8 part, nano controlled-release carrier 20-25 part;
The preparation method of described nano controlled-release carrier is:
(1) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(2) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition.To filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed 60min at 600W power ultrasonic, be heated to 90 DEG C with constant temperature heating device, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier;
Described composite feeding promoting agent comprises glycine, glutamic acid, molasses and vomiting nut, with weight parts, and glycine 15-25 part, glutamic acid 30-40 part, molasses 10-20 part and vomiting nut 25-35 part.
The preparation method of green non-pollution slowly-releasing fertilizer efficiency aquatic fertilizer of the present invention, comprises following step:
(1) according to proportioning described above, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) by microbe additive and water stand-by according to the proportional arrangement Viability bacterium liquid of 1: 900-1500;
(3) after bacterium chaff, rice bran, wheat bran, brown sugar, composite feeding promoting agent, nano controlled-release carrier being mixed according to proportioning described above, put into fermentation tank fermentation, and pass into hydrogen peroxide and to carry out disinfection sterilization processing;
(4) add the active bacteria liquid in step (2) in the ratio of material 15%-45% in described fermentation tank, stir;
(5) temperature in described fermentation tank is set to 35-40 DEG C, fermentation time is set to 36-72 hour, and every day stirs 2-5 time;
(6) aquaculture feed will fermented, through 50-80 DEG C of oven dry, then cools, obtains aquaculture feed.
Mentioned microorganism additive is bacillus subtilis, bafillus natto, lactobacillus acidophilus, candida utili and Lactobacillus plantarum.
Every gram of described aquaculture feed is bacillus subtilis >=8 hundred million, bafillus natto >=8 hundred million, lactobacillus acidophilus >=6 hundred million, candida utili >=8 hundred million containing the amount of microorganism, Lactobacillus plantarum >=8 hundred million.
The environment that the present invention efficiently solves aquaculture waters worsens, and fishes and shrimps easily occur disease, and affect degradation series of problems under its growth and meat thereof, Optimal culture waters, guarantees Safety of Aquatic Products, high-quality and efficient, in addition, the present invention with the addition of puff and soybean lecithin in aquaculture feed, puff absorbs the reaction of moisture generating gasification after feedstuff feeding, produce gas, soybean lecithin then forms oil layer at particle skin in feed granules water absorption course, prevent gas leak, when the proportion of feed granules is lighter than water, namely particle can slowly float, be convenient to the situation of ingesting that user observes aquatic products, slowly floating aquatic product feed of the present invention can slowly float after throwing something and feeding, and wrapped up by oil layer outside feed granules, thus feed granules can not scatter in water, be convenient to ingesting of aquatic products, it also avoid feed nutrient scattering and disappearing in water, and decrease the pollution of feed granules to water body.
detailed description of the invention:
The technological means realized to make the present invention, creation characteristic, reach object and effect is easy to understand, below, set forth the present invention further.
Embodiment 1:
Green non-pollution slowly-releasing fertilizer efficiency aquatic fertilizer of the present invention, raw material consists of soybean lecithin, soda ash, citric acid, bacterium chaff, rice bran, wheat bran, brown sugar, powdered whiting, urea and microbe additive; Each constituent content is respectively by mass fraction: soybean lecithin 55 parts, soda ash 35 parts, citric acid 20 parts, bacterium chaff 45 parts, 35 parts, rice bran, 40 parts, wheat bran, 5 parts, brown sugar and microbe additive 4 parts, composite feeding promoting agent 0.2 part, 20 parts, nano controlled-release carrier;
The preparation method of described nano controlled-release carrier is:
(1) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(2) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition.To filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed 60min at 600W power ultrasonic, be heated to 90 DEG C with constant temperature heating device, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier;
Described composite feeding promoting agent comprises glycine, glutamic acid, molasses and vomiting nut, with weight parts, and glycine 15 parts, 30 parts, glutamic acid, 10 parts, molasses and vomiting nut 25 parts.
The preparation method of green non-pollution slowly-releasing fertilizer efficiency aquatic fertilizer of the present invention, comprises following step:
(1) according to proportioning described above, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) by microbe additive and water stand-by according to the proportional arrangement Viability bacterium liquid of 1: 900;
(3) after bacterium chaff, rice bran, wheat bran, brown sugar, composite feeding promoting agent, nano controlled-release carrier being mixed according to proportioning described above, put into fermentation tank fermentation, and pass into hydrogen peroxide and to carry out disinfection sterilization processing;
(4) add the active bacteria liquid in step (2) in the ratio of material 15% in described fermentation tank, stir;
(5) temperature in described fermentation tank is set to 35 DEG C, fermentation time is set to 36 hours, stirs 2 every day;
(6) aquaculture feed will fermented, through 50 DEG C of oven dry, then cools, obtains aquaculture feed.
In the present embodiment, microbe additive is bacillus subtilis, bafillus natto, lactobacillus acidophilus, candida utili and Lactobacillus plantarum.Every gram of aquaculture feed containing the amount of microorganism be bacillus subtilis be 8 hundred million, bafillus natto is 8 hundred million, lactobacillus acidophilus is 6 hundred million, candida utili is 8 hundred million, Lactobacillus plantarum is 8 hundred million.
The environment that the present invention efficiently solves aquaculture waters worsens, and fishes and shrimps easily occur disease, and affect degradation series of problems under its growth and meat thereof, Optimal culture waters, guarantees Safety of Aquatic Products, high-quality and efficient.
In addition, the present invention with the addition of puff and soybean lecithin in aquaculture feed, puff absorbs the reaction of moisture generating gasification after feedstuff feeding, produce gas, soybean lecithin then forms oil layer at particle skin in feed granules water absorption course, prevent gas leak, when the proportion of feed granules is lighter than water, namely particle can slowly float, be convenient to the situation of ingesting that user observes aquatic products, slowly floating aquatic product feed of the present invention can slowly float after throwing something and feeding, and wrapped up by oil layer outside feed granules, thus feed granules can not scatter in water, be convenient to ingesting of aquatic products, it also avoid feed nutrient scattering and disappearing in water, and decrease the pollution of feed granules to water body.
Embodiment 2:
A kind of green non-pollution slowly-releasing of the present invention fertilizer efficiency aquatic fertilizer, raw material consists of soybean lecithin, soda ash, citric acid, bacterium chaff, rice bran, wheat bran, brown sugar, powdered whiting, urea and microbe additive; Each constituent content is respectively by mass fraction: soybean lecithin 65 parts, soda ash 40 parts, citric acid 40 parts, bacterium chaff 95 parts, 75 parts, rice bran, 85 parts, wheat bran, 8 parts, brown sugar and microbe additive 8 parts, composite feeding promoting agent 0.8 part, 25 parts, nano controlled-release carrier;
The preparation method of described nano controlled-release carrier is:
(1) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(2) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition.To filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed 60min at 600W power ultrasonic, be heated to 90 DEG C with constant temperature heating device, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier;
Described composite feeding promoting agent comprises glycine, glutamic acid, molasses and vomiting nut, with weight parts, and glycine 25 parts, 40 parts, glutamic acid, 20 parts, molasses and vomiting nut 35 parts.
The preparation method of green non-pollution slowly-releasing fertilizer efficiency aquatic fertilizer of the present invention, comprises following step:
(1) according to proportioning described above, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) by microbe additive and water stand-by according to the proportional arrangement of 1:1500 Viability bacterium liquid;
(3) after bacterium chaff, rice bran, wheat bran, brown sugar, composite feeding promoting agent, nano controlled-release carrier being mixed according to proportioning described above, put into fermentation tank fermentation, and pass into hydrogen peroxide and to carry out disinfection sterilization processing;
(4) add the active bacteria liquid in step (2) in the ratio of material 45% in described fermentation tank, stir;
(5) temperature in described fermentation tank is set to 40 DEG C, fermentation time is set to 72 hours, and every day stirs 2-5 time;
(6) aquaculture feed will fermented, through 80 DEG C of oven dry, then cools, obtains aquaculture feed.
Wherein, microbe additive is bacillus subtilis, bafillus natto, lactobacillus acidophilus, candida utili and Lactobacillus plantarum.
Every gram of aquaculture feed containing the amount of microorganism be bacillus subtilis be 10 hundred million, bafillus natto is 10 hundred million, lactobacillus acidophilus is 8 hundred million, candida utili is 10 hundred million, Lactobacillus plantarum is 10 hundred million.
Utilize hydroxyapatite etc. itself to have the character of loose structure, fertilizer components is adsorbed in the inner mesh of carrier, reach the object of slow releasing.Hydroxyapatite also has biodegradability properties, and gained catabolite is various trace elements ion, and these elements can be gradually resorbed.Nano controlled-release additive has good biocompatibility, gastrointestinal tract mucous compatibility, each component making it load has controlled-release function, all improve a lot through twice-modified nano-complex drugloading rate and adsorbance, fertilizer efficiency time lengthening more than 3 months, the increment of effective suppression animal pathogen, improves the benefit of the producer.
More than show and describe general principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and description just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (1)
1. a green non-pollution slowly-releasing fertilizer efficiency aquatic fertilizer, is characterized in that, raw material composition is respectively by mass fraction:
Soybean lecithin 55-65 part, soda ash 35-40 part, citric acid 20-40 part, bacterium chaff 45-95 part, rice bran 35-75 part, wheat bran 40-85 part, brown sugar 5-8 part and microbe additive 4-8 part, composite feeding promoting agent 0.2-0.8 part, nano controlled-release carrier 20-25 part;
The preparation method of described nano controlled-release carrier is:
(1) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(2) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition; To filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound;
(3) above-mentioned 1 part of twice-modified compound is disperseed 60min at 600W power ultrasonic, be heated to 90 DEG C with constant temperature heating device, and stir 60 minutes with mechanical agitator 1200r/min, obtain nano controlled-release carrier;
Described composite feeding promoting agent comprises glycine, glutamic acid, molasses and vomiting nut, with weight parts, and glycine 15-25 part, glutamic acid 30-40 part, molasses 10-20 part and vomiting nut 25-35 part;
Described microbe additive is bacillus subtilis, bafillus natto, lactobacillus acidophilus, candida utili and Lactobacillus plantarum;
Every gram of described aquatic fertilizer is bacillus subtilis >=8 hundred million, bafillus natto >=8 hundred million, lactobacillus acidophilus >=6 hundred million, candida utili >=8 hundred million containing the amount of microorganism, Lactobacillus plantarum >=8 hundred million.
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| CN104445639A (en) * | 2014-11-28 | 2015-03-25 | 镇江拜因诺生物科技有限公司 | Purifying agent for river crab aquaculture water |
| CN105732172A (en) * | 2015-12-29 | 2016-07-06 | 苏州市阳澄湖三家村蟹业有限公司 | Highly-soluble sustain-released aquaculture feed |
| CN107616365A (en) * | 2017-10-25 | 2018-01-23 | 安徽泰益生物科技有限公司 | A kind of balanced leech feed of nutrition |
| CN107736502A (en) * | 2017-10-25 | 2018-02-27 | 安徽泰益生物科技有限公司 | A kind of leech feed that can improve water quality |
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| CN101715890B (en) * | 2009-12-22 | 2012-10-24 | 佛山市顺德区全兴水产饲料有限公司 | Slowly floating aquatic product feed and production process thereof |
| CN102002141B (en) * | 2010-11-19 | 2012-05-23 | 安徽大学 | Preparation method of polyurethane-nano kaolin composite material |
| CN101999515A (en) * | 2010-11-19 | 2011-04-06 | 江苏东宝粮油集团有限公司 | Process for producing basal feed for replacing grain crops by using active bacteria preparation zymophyte bran |
| CN102429127A (en) * | 2011-11-30 | 2012-05-02 | 刘爱国 | Aquatic bio-feed |
| CN103250877B (en) * | 2013-05-17 | 2015-12-23 | 兰州天峰生物科技有限责任公司 | A kind of natural Chinese medicinal herb animal feed additive and application thereof |
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