CN103589333A - Far-infrared ray-launching radiating paint used for meter housing and preparation method thereof - Google Patents
Far-infrared ray-launching radiating paint used for meter housing and preparation method thereof Download PDFInfo
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- CN103589333A CN103589333A CN201310474813.XA CN201310474813A CN103589333A CN 103589333 A CN103589333 A CN 103589333A CN 201310474813 A CN201310474813 A CN 201310474813A CN 103589333 A CN103589333 A CN 103589333A
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- 238000002360 preparation method Methods 0.000 title claims description 10
- 239000003973 paint Substances 0.000 title abstract 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 39
- 239000000843 powder Substances 0.000 claims abstract description 33
- QOHMWDJIBGVPIF-UHFFFAOYSA-N n',n'-diethylpropane-1,3-diamine Chemical compound CCN(CC)CCCN QOHMWDJIBGVPIF-UHFFFAOYSA-N 0.000 claims abstract description 13
- -1 dioctyl ester Chemical class 0.000 claims abstract description 10
- 239000000919 ceramic Substances 0.000 claims abstract description 9
- 239000010445 mica Substances 0.000 claims abstract description 9
- 229910052618 mica group Inorganic materials 0.000 claims abstract description 9
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910010271 silicon carbide Inorganic materials 0.000 claims abstract description 9
- 239000010455 vermiculite Substances 0.000 claims abstract description 9
- 229910052902 vermiculite Inorganic materials 0.000 claims abstract description 9
- 235000019354 vermiculite Nutrition 0.000 claims abstract description 9
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 7
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims abstract description 7
- 229920000570 polyether Polymers 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- GHKOFFNLGXMVNJ-UHFFFAOYSA-N Didodecyl thiobispropanoate Chemical compound CCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCC GHKOFFNLGXMVNJ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 4
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 4
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 21
- 238000000576 coating method Methods 0.000 claims description 17
- 239000011248 coating agent Substances 0.000 claims description 16
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 12
- 230000005855 radiation Effects 0.000 claims description 12
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 9
- 229910017083 AlN Inorganic materials 0.000 claims description 7
- PIGFYZPCRLYGLF-UHFFFAOYSA-N Aluminum nitride Chemical compound [Al]#N PIGFYZPCRLYGLF-UHFFFAOYSA-N 0.000 claims description 7
- 229920002050 silicone resin Polymers 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 6
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 6
- 229910052799 carbon Inorganic materials 0.000 claims description 6
- 238000004581 coalescence Methods 0.000 claims description 6
- 150000002334 glycols Chemical class 0.000 claims description 6
- 239000010977 jade Substances 0.000 claims description 6
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims description 6
- 239000002105 nanoparticle Substances 0.000 claims description 6
- WBHHMMIMDMUBKC-QJWNTBNXSA-N ricinoleic acid Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(O)=O WBHHMMIMDMUBKC-QJWNTBNXSA-N 0.000 claims description 6
- 229960003656 ricinoleic acid Drugs 0.000 claims description 6
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 claims description 6
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 3
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims description 3
- 235000006708 antioxidants Nutrition 0.000 claims description 3
- QUBBAXISAHIDNM-UHFFFAOYSA-N ethyldimethylbenzene Natural products CCC1=CC=CC(C)=C1C QUBBAXISAHIDNM-UHFFFAOYSA-N 0.000 claims description 3
- 229910052731 fluorine Inorganic materials 0.000 claims description 3
- 239000011737 fluorine Substances 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 150000002576 ketones Chemical class 0.000 claims description 3
- 239000012046 mixed solvent Substances 0.000 claims description 3
- 238000005502 peroxidation Methods 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 229940095064 tartrate Drugs 0.000 claims description 3
- VXHFNALHLRWIIU-UHFFFAOYSA-N tert-butyl 2,2-dimethylpropanoate Chemical compound CC(C)(C)OC(=O)C(C)(C)C VXHFNALHLRWIIU-UHFFFAOYSA-N 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 4
- 230000017525 heat dissipation Effects 0.000 abstract description 3
- 229910021392 nanocarbon Inorganic materials 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 239000000758 substrate Substances 0.000 abstract description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract 2
- PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 abstract 2
- WGYKZJWCGVVSQN-UHFFFAOYSA-N propylamine Chemical compound CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 abstract 2
- 239000011347 resin Substances 0.000 abstract 2
- 229920005989 resin Polymers 0.000 abstract 2
- 229910052710 silicon Inorganic materials 0.000 abstract 2
- 239000010703 silicon Substances 0.000 abstract 2
- WIHIUTUAHOZVLE-UHFFFAOYSA-N 1,3-diethoxypropan-2-ol Chemical compound CCOCC(O)COCC WIHIUTUAHOZVLE-UHFFFAOYSA-N 0.000 abstract 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 abstract 1
- 239000012975 dibutyltin dilaurate Substances 0.000 abstract 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 235000002906 tartaric acid Nutrition 0.000 abstract 1
- 239000011975 tartaric acid Substances 0.000 abstract 1
- 230000032683 aging Effects 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
Landscapes
- Application Of Or Painting With Fluid Materials (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses far-infrared ray-launching radiating paint used for a meter housing. The far-infrared ray-launching radiating paint is prepared from the following raw materials in parts by weight: 50-54 parts of organic silicon resin, 4-5 parts of diethylin propylamine DEAPA, 2-3 parts of nano carbon, 12-15 parts of aluminum nitride, 6-8 parts of acrylonitrile, 4-6 parts of nano far-infrared ceramic powder, 1-2 parts of silicon carbide, 1-2 parts of nano vermiculite powder, 1-2 parts of nano mica powder, 2-3 parts of dibutyltin dilaurate, 1-2 parts of dioctyl ester, 1-2 parts of polyether glycol, 1-2 parts of tartaric acid, 24-26 parts of ethyl acetate, 1-2 parts of antioxidant DLTP and 4-5 parts of coalescing agent. By adding aluminum nitride and silicon carbide, the far-infrared ray-launching radiating paint used for the meter housing disclosed by the invention has high heat conduction velocity and good radiating effect; by adding the nano far-infrared ceramic powder, the nano vermiculite powder, the nano mica powder and the nano carbon, the paint has the function of launching far-infrared rays while increasing heat dissipation, and is beneficial to body health. Moreover, the paint uses the organic silicon resin as a substrate, and has excellent thermal oxidization stability.
Description
Technical field
The invention belongs to technical field of coatings, relate to a kind of heat radiation coating, more particularly, is a kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof.
Background technology
Along with science and technology progress, all kinds of instrument are also arisen at the historic moment, the heat that instrument is distributed generally can be very not fast, but can long term operation due to instrument, put aside a lot of heats, if distribute heat not in time, can cause instrument overheated, impact normal operation, also easily damages.The coating of the current design of the performance characteristics for instrument is fewer, can not meet the requirement of productive life, and heat dissipation problem is also just more and more focused on by people.There is heatproof and ageing-resistant poor and little to substrate bonding power, the not good and unhandy technical problem of radiating effect in the material that current instrument heat radiation coating is used, is difficult to meet the requirement of heat radiation.
Summary of the invention
The object of this invention is to provide a kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof, it is large that coating of the present invention has cohesive force, the advantage ageing-resistant, heat extraction coefficient is large.
The technical solution adopted in the present invention is:
An emitting far-infrared heat radiation coating for meter housing, is characterized in that being made by the raw material of following weight part: silicone resin 50-54, diethyl amino propylamine DEAPA 4-5, nano-sized carbon 2-3, aluminium nitride 12-15, vinyl cyanide 6-8, nano far infrared ceramic powder 4-6, silicon carbide 1-2, nanometer vermiculite powder 1-2, nano mica powder 1-2, dibutyl tin laurate 2-3, dioctyl ester 1-2, polyether Glycols 1-2, tartrate 1-2, ethyl acetate 24-26, anti-oxidant DLTP 1-2, film coalescence aid 4-5;
Described film coalescence aid is made by the raw material of following weight part: nanometer jade powder 2-4, linking agent TAC2-3, alcohol ester 12 4-5, Silane coupling agent KH550 1-2, vinylbenzene 3-4, ricinolic acid 1-2, MALEIC ANHYDRIDE 2-3, morpholine 2-3, peroxidation trimethylacetic acid tert-butyl ester 0.3-0.4, different fluorine that ketone 1-2, dimethylbenzene 4-5, ethyl acetate 12-13; Preparation method is: nanometer jade powder, morpholine, vinylbenzene, ricinolic acid are mixed, join in ethyl acetate and dimethylbenzene mixed solvent, stir 5-10 minute, be heated to 65-70 ℃, stir 15-30 minute under 800-1200 rev/min, then add alcohol ester 12, Silane coupling agent KH550, MALEIC ANHYDRIDE, stirring reaction 15-30 minute, add other remaining component, stirring reaction 45-60 minute, obtains again.
The preparation method of the described emitting far-infrared heat radiation coating for meter housing, it is characterized in that comprising the following steps: by ethyl acetate, polyether Glycols, nano-sized carbon, aluminium nitride, nano far infrared ceramic powder, silicon carbide, nanometer vermiculite powder, nano mica powder mixes, be heated to 50-60 ℃, 1100-1600 rev/min of lower stirring reaction 30-40 minute, then, be warming up to 70-80 ℃, add silicone resin, diethyl amino propylamine DEAPA, vinyl cyanide, dibutyl tin laurate, continue to stir 30-40 minute, add again other remaining component, continue stirring reaction 60-80 minute, grinding obtains slurry, obtain.
Beneficial effect of the present invention
The present invention is by adding aluminium nitride, silicon carbide, and heat conduction speed is high, good heat dissipation effect; By adding nano far infrared ceramic powder, nanometer vermiculite powder, nano mica powder, Nano carbon, when having increased thermal diffusivity, also make this coating there is emitting far-infrared function, useful HUMAN HEALTH, and also oilness is good, easily construction; Improved can opening effect, not stratified; This coating is used silicone resin as base material, and good insulating, has excellent thermo-oxidative stability.
Embodiment
An emitting far-infrared heat radiation coating for meter housing, is characterized in that being made by the raw material of following weight part: silicone resin 52, diethyl amino propylamine DEAPA 4, nano-sized carbon 2, aluminium nitride 13, vinyl cyanide 7, nano far infrared ceramic powder 5, silicon carbide 1, nanometer vermiculite powder 1, nano mica powder 1, dibutyl tin laurate 2, dioctyl ester 1, polyether Glycols 1, tartrate 1, ethyl acetate 25, anti-oxidant DLTP 1, film coalescence aid 4;
Described film coalescence aid by following weight part (kilogram) raw material make: your ketone 1 of nanometer jade powder 3, linking agent TAC2, alcohol ester 12, Silane coupling agent KH550 1, vinylbenzene 3, ricinolic acid 1, MALEIC ANHYDRIDE 2, morpholine 2, the peroxidation trimethylacetic acid tert-butyl ester 0.3, different fluorine, dimethylbenzene 4, ethyl acetate 12; Preparation method is: nanometer jade powder, morpholine, vinylbenzene, ricinolic acid are mixed, join in ethyl acetate and dimethylbenzene mixed solvent, stir 8 minutes, be heated to 65 ℃, stir 20 minutes under 1000 revs/min, then add alcohol ester 12, Silane coupling agent KH550, MALEIC ANHYDRIDE, stirring reaction 20 minutes, add other remaining component, stirring reaction 50 minutes, obtains again.
The preparation method of the described emitting far-infrared heat radiation coating for meter housing, it is characterized in that comprising the following steps: by ethyl acetate, polyether Glycols, nano-sized carbon, aluminium nitride, nano far infrared ceramic powder, silicon carbide, nanometer vermiculite powder, nano mica powder mixes, be heated to 55 ℃, 1300 revs/min of lower stirring reactions 30 minutes, then, be warming up to 75 ℃, add silicone resin, diethyl amino propylamine DEAPA, vinyl cyanide, dibutyl tin laurate, continue to stir 35 minutes, add again other remaining component, continue stirring reaction 70 minutes, grinding obtains slurry, obtain.
Coating of the present invention is applied on meter housing to artificial accelerated aging test under 80 ℃ and 300W ultraviolet light irradiation condition, 5000 hours ageing-resistant time, 285 ℃ of heatproof high temperature, bonding shearing force 19MPa., thermal conductivity 250W/(mK).
Claims (2)
1. for an emitting far-infrared heat radiation coating for meter housing, it is characterized in that being made by the raw material of following weight part: silicone resin 50-54, diethyl amino propylamine DEAPA 4-5, nano-sized carbon 2-3, aluminium nitride 12-15, vinyl cyanide 6-8, nano far infrared ceramic powder 4-6, silicon carbide 1-2, nanometer vermiculite powder 1-2, nano mica powder 1-2, dibutyl tin laurate 2-3, dioctyl ester 1-2, polyether Glycols 1-2, tartrate 1-2, ethyl acetate 24-26, anti-oxidant DLTP 1-2, film coalescence aid 4-5;
Described film coalescence aid is made by the raw material of following weight part: nanometer jade powder 2-4, linking agent TAC2-3, alcohol ester 12 4-5, Silane coupling agent KH550 1-2, vinylbenzene 3-4, ricinolic acid 1-2, MALEIC ANHYDRIDE 2-3, morpholine 2-3, peroxidation trimethylacetic acid tert-butyl ester 0.3-0.4, different fluorine that ketone 1-2, dimethylbenzene 4-5, ethyl acetate 12-13; Preparation method is: nanometer jade powder, morpholine, vinylbenzene, ricinolic acid are mixed, join in ethyl acetate and dimethylbenzene mixed solvent, stir 5-10 minute, be heated to 65-70 ℃, stir 15-30 minute under 800-1200 rev/min, then add alcohol ester 12, Silane coupling agent KH550, MALEIC ANHYDRIDE, stirring reaction 15-30 minute, add other remaining component, stirring reaction 45-60 minute, obtains again.
2. the preparation method of the emitting far-infrared heat radiation coating for meter housing according to claim 1, it is characterized in that comprising the following steps: by ethyl acetate, polyether Glycols, nano-sized carbon, aluminium nitride, nano far infrared ceramic powder, silicon carbide, nanometer vermiculite powder, nano mica powder mixes, be heated to 50-60 ℃, 1100-1600 rev/min of lower stirring reaction 30-40 minute, then, be warming up to 70-80 ℃, add silicone resin, diethyl amino propylamine DEAPA, vinyl cyanide, dibutyl tin laurate, continue to stir 30-40 minute, add again other remaining component, continue stirring reaction 60-80 minute, grinding obtains slurry, obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310474813.XA CN103589333B (en) | 2013-10-12 | 2013-10-12 | A kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310474813.XA CN103589333B (en) | 2013-10-12 | 2013-10-12 | A kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof |
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| Publication Number | Publication Date |
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| CN103589333A true CN103589333A (en) | 2014-02-19 |
| CN103589333B CN103589333B (en) | 2016-03-16 |
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| CN201310474813.XA Active CN103589333B (en) | 2013-10-12 | 2013-10-12 | A kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105038495A (en) * | 2015-07-08 | 2015-11-11 | 当涂县科辉商贸有限公司 | Nanometer cellulose-loaded super thermal-insulation heat-preserving paint and preparation method thereof |
| CN107163836A (en) * | 2017-07-11 | 2017-09-15 | 合肥东恒锐电子科技有限公司 | The manufacture method of a kind of electronic equipment heat radiation coating |
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| CN101353553A (en) * | 2008-09-02 | 2009-01-28 | 飞力固有限公司 | Heat radiation coating and preparation thereof |
| KR100972753B1 (en) * | 2009-11-19 | 2010-07-28 | 탁명수 | Aluminum nitride coating composite for sinking heat, heat sink using the composite and manufacturing method of the heat sink |
| CN102634245A (en) * | 2012-04-28 | 2012-08-15 | 江苏元京电子科技有限公司 | Ultraviolet light polymerization heat conduction and dissipation coating and preparation method thereof |
| CN102838892A (en) * | 2012-09-28 | 2012-12-26 | 江苏元京电子科技有限公司 | Ultraviolet curing and heat-conducting radiating coating and preparation method thereof |
| CN102964948A (en) * | 2012-11-15 | 2013-03-13 | 江苏元京电子科技有限公司 | Heat-curing heat-conduction heat-dissipation paint and preparation method thereof |
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2013
- 2013-10-12 CN CN201310474813.XA patent/CN103589333B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101353553A (en) * | 2008-09-02 | 2009-01-28 | 飞力固有限公司 | Heat radiation coating and preparation thereof |
| KR100972753B1 (en) * | 2009-11-19 | 2010-07-28 | 탁명수 | Aluminum nitride coating composite for sinking heat, heat sink using the composite and manufacturing method of the heat sink |
| CN102634245A (en) * | 2012-04-28 | 2012-08-15 | 江苏元京电子科技有限公司 | Ultraviolet light polymerization heat conduction and dissipation coating and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105038495A (en) * | 2015-07-08 | 2015-11-11 | 当涂县科辉商贸有限公司 | Nanometer cellulose-loaded super thermal-insulation heat-preserving paint and preparation method thereof |
| CN107163836A (en) * | 2017-07-11 | 2017-09-15 | 合肥东恒锐电子科技有限公司 | The manufacture method of a kind of electronic equipment heat radiation coating |
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| Publication number | Publication date |
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| CN103589333B (en) | 2016-03-16 |
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Denomination of invention: Far-infrared ray-launching radiating paint used for meter housing and preparation method thereof Effective date of registration: 20190925 Granted publication date: 20160316 Pledgee: Tianchang Science and Technology Financing Guarantee Co., Ltd. Pledgor: ANHUI AUTOMATION INSTRUMENT CO., LTD. Registration number: Y2019340000085 |
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Denomination of invention: A far infrared radiating coating for instrument case and its preparation method Effective date of registration: 20200918 Granted publication date: 20160316 Pledgee: Tianchang Science and Technology Financing Guarantee Co.,Ltd. Pledgor: ANHUI AUTOMATION INSTRUMENT Co.,Ltd. Registration number: Y2020980006198 |
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