CN103572593B - The Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain - Google Patents
The Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain Download PDFInfo
- Publication number
- CN103572593B CN103572593B CN201310509209.6A CN201310509209A CN103572593B CN 103572593 B CN103572593 B CN 103572593B CN 201310509209 A CN201310509209 A CN 201310509209A CN 103572593 B CN103572593 B CN 103572593B
- Authority
- CN
- China
- Prior art keywords
- cotton fabric
- historical relic
- triethoxy
- aminopropyl
- gamma
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 229920000742 Cotton Polymers 0.000 title claims abstract description 42
- 239000004744 fabric Substances 0.000 title claims abstract description 39
- 238000000034 method Methods 0.000 title claims abstract description 16
- 238000005728 strengthening Methods 0.000 title claims abstract description 11
- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000007864 aqueous solution Substances 0.000 claims abstract description 16
- 230000003014 reinforcing effect Effects 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 8
- 208000027418 Wounds and injury Diseases 0.000 abstract description 2
- 230000006378 damage Effects 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 208000014674 injury Diseases 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 239000007822 coupling agent Substances 0.000 description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical group O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 125000003368 amide group Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- SCPYDCQAZCOKTP-UHFFFAOYSA-N silanol Chemical compound [SiH3]O SCPYDCQAZCOKTP-UHFFFAOYSA-N 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention relates to the Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain, first configuration quality percentage is the gamma-aminopropyl-triethoxy-silane aqueous solution of 0.5 ~ 2%; Then this aqueous solution is sprayed onto equably on poor rotten COTTON FABRIC cultural artifact surface, till dripping; Naturally, after drying, the COTTON FABRIC historical relic through reinforcing namely is obtained.The beneficial effect of the invention is: 1) adopt gamma-aminopropyl-triethoxy-silane to reinforce COTTON FABRIC historical relic, improves COTTON FABRIC historical relic intensity, simultaneously little to historical relic injury, does not affect outward appearance and the feel of historical relic.2) method is simple and easy, without the need to high-temperature process, without the need to special apparatus, is applicable to various special occasions and uses, be specially adapted to emergency, simple to operate.3) low, effective, the good endurance of cost.4) nontoxic, harmless, pollution-free, meet the trend of environmental protection development.
Description
Technical field
The present invention relates to Techniques of Relics Protection field, the Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of especially a kind of grain.
Background technology
Cotton is as far back as ground plantations such as Xinjiang, Yunnan, Hainan, and to first bright epoch, cotton gradually part replaces silk fiber crops, becomes the natural fabric crop that China is important.The COTTON FABRIC historical relic be unearthed so far is from the pre-Qin days to clearly bright, and the historical relic in each age has, and mainly exists with the first-class form of cloth, clothing, cotton blanket and cotton.Therefore COTTON FABRIC is part important in China's culture treasure-house, and carrying out reinforcing to the rotten COTTON FABRIC historical relic of grain be unearthed and be significant, is also always lacked research field.In order to the requirement that satisfied collection is studied and displayed, need to carry out necessary reinforcing to increase its intensity to COTTON FABRIC.
COTTON FABRIC is reinforced follow following basic principle: (1) keeps original appearance principle, and (2) ageing-resistant principle, (3) intervene principle less, (4) invertibity principle.
Summary of the invention
The present invention will solve the shortcoming of above-mentioned prior art, provides the Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain.The present invention adopts gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) to reinforce COTTON FABRIC historical relic, while improving COTTON FABRIC historical relic intensity, does not affect outward appearance and the feel of historical relic.
The present invention solves the technical scheme that its technical problem adopts: adopt following steps:
1) configuration quality percentage is the gamma-aminopropyl-triethoxy-silane aqueous solution of 0.5 ~ 2%;
2) the gamma-aminopropyl-triethoxy-silane aqueous solution that step 1) is obtained is sprayed onto on poor rotten COTTON FABRIC cultural artifact surface, equably till dripping;
3), after naturally drying, the COTTON FABRIC historical relic through reinforcing is obtained.
Inventing useful effect is: 1) main body of cotton is cellulose, gamma-aminopropyl-triethoxy-silane (coupling agent KH-550), for amido functional group silane, the silanol energy that hydrolysis generates and cellulosic hydroxyl reaction, the silica structure that condensation generation silica structure is formed between fiber molecule instead of original hydrogen bond, the intensity of COTTON FABRIC can be improved, simultaneously little to historical relic injury.2) method is simple and easy, without the need to high-temperature process, without the need to special apparatus, is applicable to various special occasions and uses, be specially adapted to emergency, simple to operate.3) low, effective, the good endurance of cost.4) nontoxic, harmless, pollution-free, meet the trend of environmental protection development.
Detailed description of the invention
The invention will be further described below:
Embodiment 1: the Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain, comprises the following steps:
First configuration quality percentage is gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) aqueous solution of 0.5%; Then this gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) aqueous solution is sprayed onto on poor rotten COTTON FABRIC cultural artifact surface equably, till dripping; Naturally, after drying, the COTTON FABRIC historical relic through reinforcing namely is obtained.
Embodiment 2: the Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain, comprises the following steps:
First configuration quality percentage is gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) aqueous solution of 2%; Then this gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) aqueous solution is sprayed onto on poor rotten COTTON FABRIC cultural artifact surface equably, till dripping; Naturally, after drying, the COTTON FABRIC historical relic through reinforcing namely is obtained.
Embodiment 3: the Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain, comprises the following steps:
First configuration quality percentage is gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) aqueous solution of 1%; Then this gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) aqueous solution is sprayed onto on poor rotten COTTON FABRIC cultural artifact surface equably, till dripping; Naturally, after drying, the COTTON FABRIC historical relic through reinforcing namely is obtained.
Embodiment 4: the Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain, comprises the following steps:
First configuration quality percentage is gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) aqueous solution of 1.5%; Then this gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) aqueous solution is sprayed onto on poor rotten COTTON FABRIC cultural artifact surface equably, till dripping; Naturally, after drying, the COTTON FABRIC historical relic through reinforcing namely is obtained.
Embodiment 5: the Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain, comprises the following steps:
First configuration quality percentage is gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) aqueous solution of 1.8%; Then this gamma-aminopropyl-triethoxy-silane (coupling agent KH-550) aqueous solution is sprayed onto on poor rotten COTTON FABRIC cultural artifact surface equably, till dripping; Naturally, after drying, the COTTON FABRIC historical relic through reinforcing namely is obtained.
In addition to the implementation, the present invention can also have other embodiments.All employings are equal to the technical scheme of replacement or equivalent transformation formation, all drop on the protection domain of application claims.
Claims (1)
1. a Simplified Method of Strengthening for the rotten COTTON FABRIC historical relic of grain, is characterized in that adopting following steps:
1) configuration quality percentage is the gamma-aminopropyl-triethoxy-silane aqueous solution of 0.5 ~ 2%;
2) the gamma-aminopropyl-triethoxy-silane aqueous solution that step 1) is obtained is sprayed onto on poor rotten COTTON FABRIC cultural artifact surface, equably till dripping;
3), after naturally drying, the COTTON FABRIC historical relic through reinforcing is obtained.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310509209.6A CN103572593B (en) | 2013-10-24 | 2013-10-24 | The Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310509209.6A CN103572593B (en) | 2013-10-24 | 2013-10-24 | The Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103572593A CN103572593A (en) | 2014-02-12 |
| CN103572593B true CN103572593B (en) | 2015-10-21 |
Family
ID=50045255
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310509209.6A Expired - Fee Related CN103572593B (en) | 2013-10-24 | 2013-10-24 | The Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103572593B (en) |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9008423D0 (en) * | 1990-04-12 | 1990-06-13 | Albright & Wilson | Treatment of fabrics |
| US6969769B2 (en) * | 2002-06-14 | 2005-11-29 | Vanson Halosource, Inc. | N-halamine siloxanes for use in biocidal coatings and materials |
| CN102277717A (en) * | 2011-05-31 | 2011-12-14 | 陕西科技大学 | Far infrared surface treatment method for linings of warm-keeping shoes |
-
2013
- 2013-10-24 CN CN201310509209.6A patent/CN103572593B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN103572593A (en) | 2014-02-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101974850A (en) | Preparation method of ecological non-ironing silk fabric | |
| CN102691203A (en) | Preparation method of antibacterial and anti-ultraviolet fiber/fabric loaded with nano-titania | |
| CN102321974A (en) | Preparation method of superhydrophobic ultraviolet resistant textile | |
| CN103572589B (en) | A kind of amino acid-TG enzyme method for strengthening of fragile woollen fabrics | |
| CN105696326A (en) | Multifunctional textile finishing liquid and finishing method thereof | |
| CN105154994A (en) | Corn bran fibers | |
| CN103882711A (en) | Silk wrinkle-resistant finishing method | |
| CN103572593B (en) | The Simplified Method of Strengthening of the rotten COTTON FABRIC historical relic of a kind of grain | |
| CN103114456B (en) | Ramine socks and treatment method thereof | |
| CN102732977A (en) | Method for degumming silk cotton | |
| CN106702793A (en) | Preparation method of inorganic-organic composite inkjet printing paste | |
| CN103572597A (en) | Antibacterial reinforcement method of rotten cotton fabric cultural relics | |
| CN112144135A (en) | Preparation method of functional viscose containing chlorella protein algae extract | |
| CN103603183B (en) | Composite bionic reinforcing method of decayed cotton fabric culture relic | |
| CN104420215A (en) | Softening finishing method for linen fabrics | |
| CN102978957A (en) | Pretreatment process of cotton fabrics | |
| CN104928920A (en) | Antibacterial afterfinish process of printed cotton fabric | |
| CN104313871A (en) | Preparation method of lyophobic nano fiber fabric | |
| CN103422337B (en) | A kind of compound destarch auxiliary agent | |
| CN108914574B (en) | Preparation method of anti-wrinkle shrink-proof silk-woven fabric | |
| CN103572596A (en) | Method for reinforcing fragile cotton fabrics with cyanoethyl chitosan | |
| CN110258108B (en) | Crease-resistant finishing method for cotton fabric | |
| CN103046337A (en) | Method for producing jeans wear | |
| CN201800278U (en) | Knit fabric and pola fleece mixed cloth | |
| CN202187219U (en) | Anti-ultraviolet fabric structure |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151021 Termination date: 20181024 |