CN103564405B - Pear essence and preparation method thereof - Google Patents

Pear essence and preparation method thereof Download PDF

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Publication number
CN103564405B
CN103564405B CN201210279218.6A CN201210279218A CN103564405B CN 103564405 B CN103564405 B CN 103564405B CN 201210279218 A CN201210279218 A CN 201210279218A CN 103564405 B CN103564405 B CN 103564405B
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ethyl
acetate
alcohol
pear essence
propionate
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CN103564405A (en
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翁张丽卿
刘尊烈
郑灿芬
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CHAOZHOU SHUNGUAN BIOLOGICAL TECHNOLOGY CO., LTD.
GUANGDONG SHUNDA FOOD FLAVORING CO., LTD.
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GUANGDONG SHUNDA FOOD FLAVORING CO Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • A23L2/56Flavouring or bittering agents
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/29Fruit flavours
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Detergent Compositions (AREA)
  • Seasonings (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses pear essence. The pear essence mainly comprises the following components: 95-97.5% of ethyl alcohol, 0.5-1% of ethyl butyrate, 0.2-0.7% of ethyl acetate, 0.2-0.7% of ethyl propionate, 0.1-0.5% of ethyl-2-methyl butyrate, 0.1-0.5% of butyl acetate, 0.1-0.6% of isoamyl acetate, 0.1-0.5% of ethyl hexanoate, 0.1-0.5% of hexenyl acetate and 0.1-0.7% of methyl 3-methylthiopropionate. Accordingly, the invention also discloses a preparation method of the pear essence. The preparation method of the pear essence comprises the steps of sequentially adding main ingredients of the pear essence in proportion, uniformly mixing and ripening, thus the pear essence product is obtained. By adopting the preparation method of the pear essence, the pear essence has strong fruit juice taste and sufficient characteristic fragrance and can reserve natural flavour of natural pear juice; the pear essence belongs to a beverage product, and reality, smoothness and fragrance of beverage taste can be obviously enhanced.

Description

A kind of pear essence and preparation method thereof
Technical field
The present invention relates to essence field, particularly relate to a kind of pear essence and preparation method thereof.
Background technology
Since ancient times, pears are deeply by the welcome of consumer, and pears not only delicate mouthfeel also have very high medicinal health effect.The operatic circle is delicious, the crisp succulence of meat, sweet and sour taste, and local flavor fragrance is graceful.Be rich in sugar, protein, fat, carbohydrate and multivitamin, health is played an important role.The all right processing and fabricating pears of the operatic circle are dry, preserved pears, pear syrup, pear juice, canned pear etc., also can be used to wine brewing, vinegar processed.The operatic circle also has medical value, can aid digestion, moistening lung clear away heart-fire, effect of stopping coughing and removing phlegm, carbuncle of bringing down a fever, separate, also has diuresis, profit effect just.Therefore, make a there is pears taste, the edible essence of pears fragrance has certain market significance.
Fragrance is an important quality index of fruit, is mainly derived from the volatile materials of various trace.The fruit drink product of pears taste miscellaneous emerges in an endless stream in the market, but existing pear juice class beverage, generally use pears inspissated juices, and pears are by after the techniques such as squeezing, concentrated, enzymolysis, filtration, sterilization, substantially lost the fragrance of pears.In mouthfeel, pears inspissated juice, also can the bad smell of product after sterilization, affects the trial test of pear nectar, not by the favor of consumer.
Summary of the invention
Embodiment of the present invention technical problem to be solved is, provides a kind of fruit juice feel strong, and feature is fragrant sufficient, can retain the pear essence of the natural flavor of natural pear juice, and it obviously can promote the authenticity of beverage mouthfeel, blurt out sense and fragrance.
Meanwhile, embodiment of the present invention technical problem to be solved is also, the invention provides a kind of method preparing above-mentioned pear essence.
In order to solve the problems of the technologies described above, embodiments provide a kind of pear essence, it mainly consists of the following composition:
Alcohol 95 ~ 97.5%
Ethyl butyrate 0.5 ~ 1%
Ethyl acetate 0.2 ~ 0.7%
Ethyl propionate 0.2 ~ 0.7%
Ethyl 2-methylbutyrate 0.1 ~ 0.5%
Butyl acetate 0.1 ~ 0.5%
Isoamyl acetate 0.1 ~ 0.6%
Ethyl hexanoate 0.1 ~ 0.5%
Leaf Acetate 0.1 ~ 0.5%
3-methyl mercaptomethyl propionate 0.1 ~ 0.7%.
As the improvement of such scheme, described pear essence its mainly consist of the following composition:
Ethanol 96 ~ 96.5%
Ethyl butyrate 0.6 ~ 0.9%
Ethyl acetate 0.3 ~ 0.5%
Ethyl propionate 0.3 ~ 0.5%
Ethyl 2-methylbutyrate 0.1 ~ 0.4%
Butyl acetate 0.1 ~ 0.4%
Isoamyl acetate 0.1 ~ 0.5%
Ethyl hexanoate 0.1 ~ 0.4%
Leaf Acetate 0.1 ~ 0.4%
3-methyl mercaptomethyl propionate 0.1 ~ 0.5%.
As the improvement of such scheme, described pear essence its mainly consist of the following composition:
Ethanol 96.2600%
Ethyl butyrate 0.7016%
Ethyl acetate 0.4000%
Ethyl propionate 0.4000%
Ethyl 2-methylbutyrate 0.2565%
Butyl acetate 0.2506%
Isoamyl acetate 0.2934%
Ethyl hexanoate 0.2376%
Leaf Acetate 0.2048%
3-methyl mercaptomethyl propionate 0.3276%.
As the improvement of such scheme, described pear essence also comprises following one-tenth and is grouped into:
Hexanal 0.04 ~ 0.08%; Ethyl n-valerate 0.004 ~ 0.009%; N-butanol 0.01 ~ 0.05%; Trans-2-butene acetoacetic ester 0.003 ~ 0.008%; Methyl caproate 0.003 ~ 0.008%; Isoamyl alcohol 0.01 ~ 0.03%; 2-hexenoic aldehyde (leaf aldehyde) 0.01 ~ 0.03%; Hexyl acetate 0.1 ~ 0.3%; 2-hydroxyl-Ding-3-ketone 0.001 ~ 0.005%; Iso-amyl iso-valeriate 0.001 ~ 0.003%; Cognac oil 0.01 ~ 0.04%; N-hexyl alcohol 0.05 ~ 0.1%; Leaf-alcohol 0.01 ~ 0.03%; Furfural 0.01 ~ 0.03%; Octyl acetate 0.02 ~ 0.06%; N-octyl alcohol 0.003 ~ 0.008%; 3-methyl mercapto ethyl propionate 0.01 ~ 0.05%; Diethyl malonate 0.02 ~ 0.06%; Propane diols 0.03 ~ 0.08%; Alpha-terpineol 0.005 ~ 0.01%; Damascenone 0.003 ~ 0.008%; Benzyl carbinol 0.05 ~ 0.1%; Eugenol 0.02 ~ 0.07%; Vanillic aldehyde 0.003 ~ 0.008%.
As the improvement of such scheme, described pear essence also comprises following one-tenth and is grouped into:
Hexanal 0.0625%; Ethyl n-valerate 0.0067%; N-butanol 0.0250%; Trans-2-butene acetoacetic ester 0.0059%; Methyl caproate 0.0053%; Isoamyl alcohol 0.0162%; 2-hexenoic aldehyde (leaf aldehyde) 0.0150%; Hexyl acetate 0.1400%; 2-hydroxyl-Ding-3-ketone 0.0026%; Iso-amyl iso-valeriate 0.0014%; Cognac oil 0.0209%; N-hexyl alcohol 0.0700%; Leaf-alcohol 0.0163%; Furfural 0.0230%; Octyl acetate 0.0447%; N-octyl alcohol 0.0060%; 3-methyl mercapto ethyl propionate 0.0331%; Diethyl malonate 0.0417%; Propane diols 0.0513%; Alpha-terpineol 0.0085%; Damascenone 0.0054%; Benzyl carbinol 0.0697%; Eugenol 0.0403 %; Vanillic aldehyde 0.0050%.
Correspondingly, embodiments provide a kind of preparation method of pear essence, the main component of described pear essence is added successively according to proportioning, mixes, after the main component maturation of described pear essence, obtain pear essence product;
The main component of described pear essence is as follows:
Alcohol 95 ~ 97.5%
Ethyl butyrate 0.5 ~ 1%
Ethyl acetate 0.2 ~ 0.7%
Ethyl propionate 0.2 ~ 0.7%
Ethyl 2-methylbutyrate 0.1 ~ 0.5%
Butyl acetate 0.1 ~ 0.5%
Isoamyl acetate 0.1 ~ 0.6%
Ethyl hexanoate 0.1 ~ 0.5%
Leaf Acetate 0.1 ~ 0.5%
3-methyl mercaptomethyl propionate 0.1 ~ 0.7%.
As the improvement of such scheme, described pear essence its mainly consist of the following composition:
Ethanol 96 ~ 96.5%
Ethyl butyrate 0.6 ~ 0.9%
Ethyl acetate 0.3 ~ 0.5%
Ethyl propionate 0.3 ~ 0.5%
Ethyl 2-methylbutyrate 0.1 ~ 0.4%
Butyl acetate 0.1 ~ 0.4%
Isoamyl acetate 0.1 ~ 0.5%
Ethyl hexanoate 0.1 ~ 0.4%
Leaf Acetate 0.1 ~ 0.4%
3-methyl mercaptomethyl propionate 0.1 ~ 0.5%.
As the improvement of such scheme, described pear essence its mainly consist of the following composition:
Ethanol 96.2600%
Ethyl butyrate 0.7016%
Ethyl acetate 0.4000%
Ethyl propionate 0.4000%
Ethyl 2-methylbutyrate 0.2565%
Butyl acetate 0.2506%
Isoamyl acetate 0.2934%
Ethyl hexanoate 0.2376%
Leaf Acetate 0.2048%
3-methyl mercaptomethyl propionate 0.3276%.
As the improvement of such scheme, described pear essence also comprises following one-tenth and is grouped into:
Hexanal 0.04 ~ 0.08%; Ethyl n-valerate 0.004 ~ 0.009%; N-butanol 0.01 ~ 0.05%; Trans-2-butene acetoacetic ester 0.003 ~ 0.008%; Methyl caproate 0.003 ~ 0.008%; Isoamyl alcohol 0.01 ~ 0.03%; 2-hexenoic aldehyde (leaf aldehyde) 0.01 ~ 0.03%; Hexyl acetate 0.1 ~ 0.3%; 2-hydroxyl-Ding-3-ketone 0.001 ~ 0.005%; Iso-amyl iso-valeriate 0.001 ~ 0.003%; Cognac oil 0.01 ~ 0.04%; N-hexyl alcohol 0.05 ~ 0.1%; Leaf-alcohol 0.01 ~ 0.03%; Furfural 0.01 ~ 0.03%; Octyl acetate 0.02 ~ 0.06%; N-octyl alcohol 0.003 ~ 0.008%; 3-methyl mercapto ethyl propionate 0.01 ~ 0.05%; Diethyl malonate 0.02 ~ 0.06%; Propane diols 0.03 ~ 0.08%; Alpha-terpineol 0.005 ~ 0.01%; Damascenone 0.003 ~ 0.008%; Benzyl carbinol 0.05 ~ 0.1%; Eugenol 0.02 ~ 0.07%; Vanillic aldehyde 0.003 ~ 0.008%.
As the improvement of such scheme, described pear essence also comprises following one-tenth and is grouped into:
Hexanal 0.0625%; Ethyl n-valerate 0.0067%; N-butanol 0.0250%; Trans-2-butene acetoacetic ester 0.0059%; Methyl caproate 0.0053%; Isoamyl alcohol 0.0162%; 2-hexenoic aldehyde (leaf aldehyde) 0.0150%; Hexyl acetate 0.1400%; 2-hydroxyl-Ding-3-ketone 0.0026%; Iso-amyl iso-valeriate 0.0014%; Cognac oil 0.0209%; N-hexyl alcohol 0.0700%; Leaf-alcohol 0.0163%; Furfural 0.0230%; Octyl acetate 0.0447%; N-octyl alcohol 0.0060%; 3-methyl mercapto ethyl propionate 0.0331%; Diethyl malonate 0.0417%; Propane diols 0.0513%; Alpha-terpineol 0.0085%; Damascenone 0.0054%; Benzyl carbinol 0.0697%; Eugenol 0.0403 %; Vanillic aldehyde 0.0050%.
Implement the embodiment of the present invention, there is following beneficial effect:
The present invention, by analyzing the fragrance component of pears, constantly allocates test, obtains the formula closest to nature, soft pear essence.Described pear essence formula is made up of 30 Multiple components, and fragrance is very natural, and fruit juice feel is strong, and feature is fragrant sufficient, can retain the natural flavor of natural pear juice, and security is good.The present invention is used for beverage series products, obviously can promote the authenticity of beverage mouthfeel, blurt out and feel and fragrance.
Accompanying drawing explanation
Fig. 1 is the flow chart of the preparation method of a kind of pear essence of the present invention.
Detailed description of the invention
For making the object, technical solutions and advantages of the present invention clearly, below in conjunction with accompanying drawing, the present invention is described in further detail.
Embodiments provide a kind of pear essence, it mainly consists of the following composition:
Alcohol 95 ~ 97.5%
Ethyl butyrate 0.5 ~ 1%
Ethyl acetate 0.2 ~ 0.7%
Ethyl propionate 0.2 ~ 0.7%
Ethyl 2-methylbutyrate 0.1 ~ 0.5%
Butyl acetate 0.1 ~ 0.5%
Isoamyl acetate 0.1 ~ 0.6%
Ethyl hexanoate 0.1 ~ 0.5%
Leaf Acetate 0.1 ~ 0.5%
3-methyl mercaptomethyl propionate 0.1 ~ 0.7%.
Preferably, described pear essence its mainly consist of the following composition:
Ethanol 96 ~ 96.5%
Ethyl butyrate 0.6 ~ 0.9%
Ethyl acetate 0.3 ~ 0.5%
Ethyl propionate 0.3 ~ 0.5%
Ethyl 2-methylbutyrate 0.1 ~ 0.4%
Butyl acetate 0.1 ~ 0.4%
Isoamyl acetate 0.1 ~ 0.5%
Ethyl hexanoate 0.1 ~ 0.4%
Leaf Acetate 0.1 ~ 0.4%
3-methyl mercaptomethyl propionate 0.1 ~ 0.5%.
More preferably, described pear essence its mainly consist of the following composition:
Ethanol 96.2600%
Ethyl butyrate 0.7016%
Ethyl acetate 0.4000%
Ethyl propionate 0.4000%
Ethyl 2-methylbutyrate 0.2565%
Butyl acetate 0.2506%
Isoamyl acetate 0.2934%
Ethyl hexanoate 0.2376%
Leaf Acetate 0.2048%
3-methyl mercaptomethyl propionate 0.3276%.
Further, described pear essence also comprises following one-tenth and is grouped into:
Hexanal 0.04 ~ 0.08%; Ethyl n-valerate 0.004 ~ 0.009%; N-butanol 0.01 ~ 0.05%; Trans-2-butene acetoacetic ester 0.003 ~ 0.008%; Methyl caproate 0.003 ~ 0.008%; Isoamyl alcohol 0.01 ~ 0.03%; 2-hexenoic aldehyde (leaf aldehyde) 0.01 ~ 0.03%; Hexyl acetate 0.1 ~ 0.3%; 2-hydroxyl-Ding-3-ketone 0.001 ~ 0.005%; Iso-amyl iso-valeriate 0.001 ~ 0.003%; Cognac oil 0.01 ~ 0.04%; N-hexyl alcohol 0.05 ~ 0.1%; Leaf-alcohol 0.01 ~ 0.03%; Furfural 0.01 ~ 0.03%; Octyl acetate 0.02 ~ 0.06%; N-octyl alcohol 0.003 ~ 0.008%; 3-methyl mercapto ethyl propionate 0.01 ~ 0.05%; Diethyl malonate 0.02 ~ 0.06%; Propane diols 0.03 ~ 0.08%; Alpha-terpineol 0.005 ~ 0.01%; Damascenone 0.003 ~ 0.008%; Benzyl carbinol 0.05 ~ 0.1%; Eugenol 0.02 ~ 0.07%; Vanillic aldehyde 0.003 ~ 0.008%.
Preferably, described pear essence also comprises following one-tenth and is grouped into:
Hexanal 0.0625%; Ethyl n-valerate 0.0067%; N-butanol 0.0250%; Trans-2-butene acetoacetic ester 0.0059%; Methyl caproate 0.0053%; Isoamyl alcohol 0.0162%; 2-hexenoic aldehyde (leaf aldehyde) 0.0150%; Hexyl acetate 0.1400%; 2-hydroxyl-Ding-3-ketone 0.0026%; Iso-amyl iso-valeriate 0.0014%; Cognac oil 0.0209%; N-hexyl alcohol 0.0700%; Leaf-alcohol 0.0163%; Furfural 0.0230%; Octyl acetate 0.0447%; N-octyl alcohol 0.0060%; 3-methyl mercapto ethyl propionate 0.0331%; Diethyl malonate 0.0417%; Propane diols 0.0513%; Alpha-terpineol 0.0085%; Damascenone 0.0054%; Benzyl carbinol 0.0697%; Eugenol 0.0403 %; Vanillic aldehyde 0.0050%.
Because composition spices used in pear essence formula of the present invention is in National Standard of the People's Republic of China GB2760 the spices allowing to use, therefore pear essence security of the present invention is good.
Pear essence sensory evaluation of the present invention:
1, fragrance: with distinguishing that fragrant paper picks 1cm essence, judge fragrance.
Result: can smell pure and fresh pears fragrance, fragrance is very natural.
2, taste: be added in 100g water by 0.1g essence, judges its fragrance.
Result: have strong pear juice sense and there is the natural flavor of natural pear juice.
Therefore, the present invention, by analyzing the fragrance component of pears, constantly allocates test, obtains the formula closest to nature, soft pear essence.Described pear essence formula is made up of 30 Multiple components, and fragrance is very natural, and fruit juice feel is strong, and feature is fragrant sufficient, can retain the natural flavor of natural pear juice, and security is good.The present invention is used for beverage series products, obviously can promote the authenticity of beverage mouthfeel, blurt out and feel and fragrance.
As shown in Figure 1, embodiments provide a kind of preparation method of pear essence, comprising:
S101, adds according to proportioning successively by the main component of described pear essence.
The main component of described pear essence is as follows:
Alcohol 95 ~ 97.5%
Ethyl butyrate 0.5 ~ 1%
Ethyl acetate 0.2 ~ 0.7%
Ethyl propionate 0.2 ~ 0.7%
Ethyl 2-methylbutyrate 0.1 ~ 0.5%
Butyl acetate 0.1 ~ 0.5%
Isoamyl acetate 0.1 ~ 0.6%
Ethyl hexanoate 0.1 ~ 0.5%
Leaf Acetate 0.1 ~ 0.5%
3-methyl mercaptomethyl propionate 0.1 ~ 0.7%.
Preferably, in S101, all the components of described pear essence is added successively according to proportioning.
The all the components of described pear essence is as follows:
Alcohol 95 ~ 97.5%; Ethyl butyrate 0.5 ~ 1%; Ethyl acetate 0.2 ~ 0.7%; Ethyl propionate 0.2 ~ 0.7%; Ethyl 2-methylbutyrate 0.1 ~ 0.5%; Butyl acetate 0.1 ~ 0.5%; Isoamyl acetate 0.1 ~ 0.6%; Ethyl hexanoate 0.1 ~ 0.5%; Leaf Acetate 0.1 ~ 0.5%; 3-methyl mercaptomethyl propionate 0.1 ~ 0.7%; Hexanal 0.04 ~ 0.08%; Ethyl n-valerate 0.004 ~ 0.009%; N-butanol 0.01 ~ 0.05%; Trans-2-butene acetoacetic ester 0.003 ~ 0.008%; Methyl caproate 0.003 ~ 0.008%; Isoamyl alcohol 0.01 ~ 0.03%; 2-hexenoic aldehyde (leaf aldehyde) 0.01 ~ 0.03%; Hexyl acetate 0.1 ~ 0.3%; 2-hydroxyl-Ding-3-ketone 0.001 ~ 0.005%; Iso-amyl iso-valeriate 0.001 ~ 0.003%; Cognac oil 0.01 ~ 0.04%; N-hexyl alcohol 0.05 ~ 0.1%; Leaf-alcohol 0.01 ~ 0.03%; Furfural 0.01 ~ 0.03%; Octyl acetate 0.02 ~ 0.06%; N-octyl alcohol 0.003 ~ 0.008%; 3-methyl mercapto ethyl propionate 0.01 ~ 0.05%; Diethyl malonate 0.02 ~ 0.06%; Propane diols 0.03 ~ 0.08%; Alpha-terpineol 0.005 ~ 0.01%; Damascenone 0.003 ~ 0.008%; Benzyl carbinol 0.05 ~ 0.1%; Eugenol 0.02 ~ 0.07%; Vanillic aldehyde 0.003 ~ 0.008%.
S102, mixes the main component of described pear essence.
Preferably, all the components of described pear essence is mixed.
S103, after the main component maturation of described pear essence, obtains pear essence product.
Preferably, after all the components maturation of described pear essence, obtain pear essence product.
The present invention is set forth further below with specific embodiment
Embodiment 1
One, the formula of pear essence
Table one
CAS Chinese name Proportioning
141-78-6 Ethyl acetate 0.4000
64-17-5 Ethanol 96.2600
105-37-3 Ethyl propionate 0.4000
105-54-4 Ethyl butyrate 0.7016
7452-79-1 Ethyl 2-methylbutyrate 0.2565
123-86-4 Butyl acetate 0.2506
66-25-1 Hexanal 0.0625
123-92-2 Isoamyl acetate 0.2934
539-82-2 Ethyl n-valerate 0.0067
71-36-3 N-butanol 0.0250
10544-63-5 Trans-2-butene acetoacetic ester 0.0059
106-70-7 Methyl caproate 0.0053
123-51-3 Isoamyl alcohol 0.0162
6728-26-3 2-hexenoic aldehyde (leaf aldehyde) 0.0150
123-66-0 Ethyl hexanoate 0.2376
142-92-7 Hexyl acetate 0.1400
513-86-0 2-hydroxyl-Ding-3-ketone 0.0026
659-70-1 Iso-amyl iso-valeriate 0.0014
3681-71-8 Leaf Acetate 0.2048
106-30-9 Cognac oil 0.0209
111-27-3 N-hexyl alcohol 0.0700
928-96-1 Leaf-alcohol 0.0163
98-01-1 Furfural 0.0230
112-14-1 Octyl acetate 0.0447
13532-18-8 3-methyl mercaptomethyl propionate 0.3276
111-87-5 N-octyl alcohol 0.0060
13327-56-5 3-methyl mercapto ethyl propionate 0.0331
105-53-3 Diethyl malonate 0.0417
57-55-6 Propane diols 0.0513
98-55-5 Alpha-terpineol 0.0085
23696-85-7 Damascenone 0.0054
60-12-8 Benzyl carbinol 0.0697
97-53-0 Eugenol 0.0403
121-33-5 Vanillic aldehyde 0.0050
Amount to   100.0000
It should be noted that, CAS(Chemical Abstracts Service, American Chemical Society divides into digest society of histochemistry).
Two, the preparation of pear essence
By the formula of table one, each constituent of pear essence is added successively according to proportioning, mixes, after the constituent maturation of described pear essence, obtain pear essence product.
Embodiment 2
One, the formula of pear essence
Table two
CAS Chinese name Proportioning
141-78-6 Ethyl acetate 0.7000
64-17-5 Ethanol 95.2000
105-37-3 Ethyl propionate 0.7000
105-54-4 Ethyl butyrate 0.9016
7452-79-1 Ethyl 2-methylbutyrate 0.3965
123-86-4 Butyl acetate 0.3647
66-25-1 Hexanal 0.0725
123-92-2 Isoamyl acetate 0.3934
539-82-2 Ethyl n-valerate 0.0009
71-36-3 N-butanol 0.0500
10544-63-5 Trans-2-butene acetoacetic ester 0.0080
106-70-7 Methyl caproate 0.0080
123-51-3 Isoamyl alcohol 0.0300
6728-26-3 2-hexenoic aldehyde (leaf aldehyde) 0.0300
123-66-0 Ethyl hexanoate 0.1376
142-92-7 Hexyl acetate 0.1300
513-86-0 2-hydroxyl-Ding-3-ketone 0.0050
659-70-1 Iso-amyl iso-valeriate 0.0030
3681-71-8 Leaf Acetate 0.1048
106-30-9 Cognac oil 0.0309
111-27-3 N-hexyl alcohol 0.1000
928-96-1 Leaf-alcohol 0.0300
98-01-1 Furfural 0.0300
112-14-1 Octyl acetate 0.0600
13532-18-8 3-methyl mercaptomethyl propionate 0.1276
111-87-5 N-octyl alcohol 0.0080
13327-56-5 3-methyl mercapto ethyl propionate 0.0631
105-53-3 Diethyl malonate 0.0517
57-55-6 Propane diols 0.0713
98-55-5 Alpha-terpineol 0.0100
23696-85-7 Damascenone 0.0080
60-12-8 Benzyl carbinol 0.0997
97-53-0 Eugenol 0.0657
121-33-5 Vanillic aldehyde 0.0080
Amount to   100.0000
Two, the preparation of pear essence
By the formula of table two, each constituent of pear essence is added successively according to proportioning, mixes, after the constituent maturation of described pear essence, obtain pear essence product.
Embodiment 3
One, the formula of pear essence
Table three
CAS Chinese name Proportioning
141-78-6 Ethyl acetate 0.2000
64-17-5 Ethanol 97.2600
105-37-3 Ethyl propionate 0.2000
105-54-4 Ethyl butyrate 0.5016
7452-79-1 Ethyl 2-methylbutyrate 0.1565
123-86-4 Butyl acetate 0.1506
66-25-1 Hexanal 0.0625
123-92-2 Isoamyl acetate 0.1934
539-82-2 Ethyl n-valerate 0.0067
71-36-3 N-butanol 0.0250
10544-63-5 Trans-2-butene acetoacetic ester 0.0059
106-70-7 Methyl caproate 0.0053
123-51-3 Isoamyl alcohol 0.0162
6728-26-3 2-hexenoic aldehyde (leaf aldehyde) 0.0150
123-66-0 Ethyl hexanoate 0.1376
142-92-7 Hexyl acetate 0.1400
513-86-0 2-hydroxyl-Ding-3-ketone 0.0026
659-70-1 Iso-amyl iso-valeriate 0.0014
3681-71-8 Leaf Acetate 0.1562
106-30-9 Cognac oil 0.0209
111-27-3 N-hexyl alcohol 0.0700
928-96-1 Leaf-alcohol 0.0163
98-01-1 Furfural 0.0230
112-14-1 Octyl acetate 0.0447
13532-18-8 3-methyl mercaptomethyl propionate 0.3222
111-87-5 N-octyl alcohol 0.0060
13327-56-5 3-methyl mercapto ethyl propionate 0.0331
105-53-3 Diethyl malonate 0.0417
57-55-6 Propane diols 0.0513
98-55-5 Alpha-terpineol 0.0085
23696-85-7 Damascenone 0.0054
60-12-8 Benzyl carbinol 0.0697
97-53-0 Eugenol 0.0457
121-33-5 Vanillic aldehyde 0.0050
Amount to   100.0000
Two, the preparation of pear essence
By the formula of table three, each constituent of pear essence is added successively according to proportioning, mixes, after the constituent maturation of described pear essence, obtain pear essence product.
Embodiment 4
One, the formula of pear essence
Table four
CAS Chinese name Proportioning
141-78-6 Ethyl acetate 0.2000
64-17-5 Ethanol 96.5000
105-37-3 Ethyl propionate 0.3000
105-54-4 Ethyl butyrate 0.6016
7452-79-1 Ethyl 2-methylbutyrate 0.3565
123-86-4 Butyl acetate 0.2506
66-25-1 Hexanal 0.0625
123-92-2 Isoamyl acetate 0.3934
539-82-2 Ethyl n-valerate 0.0067
71-36-3 N-butanol 0.0450
10544-63-5 Trans-2-butene acetoacetic ester 0.0059
106-70-7 Methyl caproate 0.0053
123-51-3 Isoamyl alcohol 0.0262
6728-26-3 2-hexenoic aldehyde (leaf aldehyde) 0.0250
123-66-0 Ethyl hexanoate 0.1376
142-92-7 Hexyl acetate 0.1600
513-86-0 2-hydroxyl-Ding-3-ketone 0.0026
659-70-1 Iso-amyl iso-valeriate 0.0014
3681-71-8 Leaf Acetate 0.1562
106-30-9 Cognac oil 0.0209
111-27-3 N-hexyl alcohol 0.0700
928-96-1 Leaf-alcohol 0.0163
98-01-1 Furfural 0.0230
112-14-1 Octyl acetate 0.0447
13532-18-8 3-methyl mercaptomethyl propionate 0.3222
111-87-5 N-octyl alcohol 0.0060
13327-56-5 3-methyl mercapto ethyl propionate 0.0331
105-53-3 Diethyl malonate 0.0417
57-55-6 Propane diols 0.0513
98-55-5 Alpha-terpineol 0.0085
23696-85-7 Damascenone 0.0054
60-12-8 Benzyl carbinol 0.0697
97-53-0 Eugenol 0.0457
121-33-5 Vanillic aldehyde 0.0050
Amount to   100.0000
Two, the preparation of pear essence
By the formula of table four, each constituent of pear essence is added successively according to proportioning, mixes, after the constituent maturation of described pear essence, obtain pear essence product.
Respectively sensory evaluation is done to the pear essence of embodiment 1 to 4 below:
(1), experimental technique: described every sensory evaluation experiment is implemented by three groups, and often group has 3 ~ 5 housebroken tasters.By the pear essence of the embodiment of the present invention 1 to 4, do the sensory evaluation such as fragrance, taste with the pear essence of prior art and contrast, method is as follows:
1, fragrance: with distinguishing that fragrant paper picks 1cm essence, judge fragrance.
2, taste: be added in 100g water by 0.1g essence, judges its fragrance.
Finally, three experiment groups are carried out analysis and arrangement to the evaluation result that every sensory evaluation is tested, sums up result.
(2), experimental result:
Project Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Prior art
Fragrance Pure and fresh, natural pears fragrance, and fragrance is elegant, full Pure and fresh, natural pears fragrance Pure and fresh, natural pears fragrance Pure and fresh, natural pears fragrance Fragrance is light, be mingled with bad smell
Taste There is natural, strong pear juice sense There is natural pear juice sense There is natural pear juice sense There is natural pear juice sense Pear juice sense is not strong, mouthfeel is complicated
In sum, implement the embodiment of the present invention, there is following beneficial effect:
The present invention, by analyzing the fragrance component of pears, constantly allocates test, obtains the formula closest to nature, soft pear essence.Described pear essence formula is made up of 30 Multiple components, and fragrance is very natural, and fruit juice feel is strong, and feature is fragrant sufficient, can retain the natural flavor of natural pear juice, and security is good.The present invention is used for beverage series products, obviously can promote the authenticity of beverage mouthfeel, blurt out and feel and fragrance.
Above disclosedly be only one or more preferred embodiments of the present invention, certainly can not limit the interest field of the present invention with this, therefore according to the equivalent variations that the claims in the present invention are done, still belong to the scope that the present invention is contained.

Claims (4)

1. a pear essence, is characterized in that, it consists of the following composition:
Alcohol 95 ~ 97.5%; Ethyl butyrate 0.5 ~ 1%; Ethyl acetate 0.2 ~ 0.7%; Ethyl propionate 0.2 ~ 0.7%; Ethyl 2-methylbutyrate 0.1 ~ 0.5%; Butyl acetate 0.1 ~ 0.5%; Isoamyl acetate 0.1 ~ 0.6%; Ethyl hexanoate 0.1 ~ 0.5%; Leaf Acetate 0.1 ~ 0.5%; 3-methyl mercaptomethyl propionate 0.1 ~ 0.7%; Hexanal 0.04 ~ 0.08%; Ethyl n-valerate 0.004 ~ 0.009%; N-butanol 0.01 ~ 0.05%; Trans-2-butene acetoacetic ester 0.003 ~ 0.008%; Methyl caproate 0.003 ~ 0.008%; Isoamyl alcohol 0.01 ~ 0.03%; 2-hexenoic aldehyde 0.01 ~ 0.03%; Hexyl acetate 0.1 ~ 0.3%; 2-hydroxyl-Ding-3-ketone 0.001 ~ 0.005%; Iso-amyl iso-valeriate 0.001 ~ 0.003%; Cognac oil 0.01 ~ 0.04%; N-hexyl alcohol 0.05 ~ 0.1%; Leaf-alcohol 0.01 ~ 0.03%; Furfural 0.01 ~ 0.03%; Octyl acetate 0.02 ~ 0.06%; N-octyl alcohol 0.003 ~ 0.008%; 3-methyl mercapto ethyl propionate 0.01 ~ 0.05%; Diethyl malonate 0.02 ~ 0.06%; Propane diols 0.03 ~ 0.08%; Alpha-terpineol 0.005 ~ 0.01%; Damascenone 0.003 ~ 0.008%; Benzyl carbinol 0.05 ~ 0.1%; Eugenol 0.02 ~ 0.07%; Vanillic aldehyde 0.003 ~ 0.008%.
2. pear essence as claimed in claim 1, it is characterized in that, described pear essence consists of the following composition:
Ethanol 96 ~ 96.5%; Ethyl butyrate 0.6 ~ 0.9%; Ethyl acetate 0.3 ~ 0.5%; Ethyl propionate 0.3 ~ 0.5%; Ethyl 2-methylbutyrate 0.1 ~ 0.4%; Butyl acetate 0.1 ~ 0.4%; Isoamyl acetate 0.1 ~ 0.5%; Ethyl hexanoate 0.1 ~ 0.4%; Leaf Acetate 0.1 ~ 0.4%; 3-methyl mercaptomethyl propionate 0.1 ~ 0.5%; Hexanal 0.04 ~ 0.08%; Ethyl n-valerate 0.004 ~ 0.009%; N-butanol 0.01 ~ 0.05%; Trans-2-butene acetoacetic ester 0.003 ~ 0.008%; Methyl caproate 0.003 ~ 0.008%; Isoamyl alcohol 0.01 ~ 0.03%; 2-hexenoic aldehyde 0.01 ~ 0.03%; Hexyl acetate 0.1 ~ 0.3%; 2-hydroxyl-Ding-3-ketone 0.001 ~ 0.005%; Iso-amyl iso-valeriate 0.001 ~ 0.003%; Cognac oil 0.01 ~ 0.04%; N-hexyl alcohol 0.05 ~ 0.1%; Leaf-alcohol 0.01 ~ 0.03%; Furfural 0.01 ~ 0.03%; Octyl acetate 0.02 ~ 0.06%; N-octyl alcohol 0.003 ~ 0.008%; 3-methyl mercapto ethyl propionate 0.01 ~ 0.05%; Diethyl malonate 0.02 ~ 0.06%; Propane diols 0.03 ~ 0.08%; Alpha-terpineol 0.005 ~ 0.01%; Damascenone 0.003 ~ 0.008%; Benzyl carbinol 0.05 ~ 0.1%; Eugenol 0.02 ~ 0.07%; Vanillic aldehyde 0.003 ~ 0.008%.
3. pear essence as claimed in claim 1, it is characterized in that, described pear essence consists of the following composition:
Ethanol 96.2600%; Ethyl butyrate 0.7016%; Ethyl acetate 0.4000%; Ethyl propionate 0.4000%; Ethyl 2-methylbutyrate 0.2565%; Butyl acetate 0.2506%; Isoamyl acetate 0.2934%; Ethyl hexanoate 0.2376%; Leaf Acetate 0.2048%; 3-methyl mercaptomethyl propionate 0.3276%; Hexanal 0.04 ~ 0.08%; Ethyl n-valerate 0.004 ~ 0.009%; N-butanol 0.01 ~ 0.05%; Trans-2-butene acetoacetic ester 0.003 ~ 0.008%; Methyl caproate 0.003 ~ 0.008%; Isoamyl alcohol 0.01 ~ 0.03%; 2-hexenoic aldehyde 0.01 ~ 0.03%; Hexyl acetate 0.1 ~ 0.3%; 2-hydroxyl-Ding-3-ketone 0.001 ~ 0.005%; Iso-amyl iso-valeriate 0.001 ~ 0.003%; Cognac oil 0.01 ~ 0.04%; N-hexyl alcohol 0.05 ~ 0.1%; Leaf-alcohol 0.01 ~ 0.03%; Furfural 0.01 ~ 0.03%; Octyl acetate 0.02 ~ 0.06%; N-octyl alcohol 0.003 ~ 0.008%; 3-methyl mercapto ethyl propionate 0.01 ~ 0.05%; Diethyl malonate 0.02 ~ 0.06%; Propane diols 0.03 ~ 0.08%; Alpha-terpineol 0.005 ~ 0.01%; Damascenone 0.003 ~ 0.008%; Benzyl carbinol 0.05 ~ 0.1%; Eugenol 0.02 ~ 0.07%; Vanillic aldehyde 0.003 ~ 0.008%.
4. pear essence as claimed in claim 1, it is characterized in that, described pear essence consists of the following composition:
Alcohol 95 ~ 97.5%; Ethyl butyrate 0.5 ~ 1%; Ethyl acetate 0.2 ~ 0.7%; Ethyl propionate 0.2 ~ 0.7%; Ethyl 2-methylbutyrate 0.1 ~ 0.5%; Butyl acetate 0.1 ~ 0.5%; Isoamyl acetate 0.1 ~ 0.6%; Ethyl hexanoate 0.1 ~ 0.5%; Leaf Acetate 0.1 ~ 0.5%; 3-methyl mercaptomethyl propionate 0.1 ~ 0.7%; Hexanal 0.0625%; Ethyl n-valerate 0.0067%; N-butanol 0.0250%; Trans-2-butene acetoacetic ester 0.0059%; Methyl caproate 0.0053%; Isoamyl alcohol 0.0162%; 2-hexenoic aldehyde 0.0150%; Hexyl acetate 0.1400%; 2-hydroxyl-Ding-3-ketone 0.0026%; Iso-amyl iso-valeriate 0.0014%; Cognac oil 0.0209%; N-hexyl alcohol 0.0700%; Leaf-alcohol 0.0163%; Furfural 0.0230%; Octyl acetate 0.0447%; N-octyl alcohol 0.0060%; 3-methyl mercapto ethyl propionate 0.0331%; Diethyl malonate 0.0417%; Propane diols 0.0513%; Alpha-terpineol 0.0085%; Damascenone 0.0054%; Benzyl carbinol 0.0697%; Eugenol 0.0403 %; Vanillic aldehyde 0.0050%.
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