CN103497813B - 一种专用于冶金行业连铸机的润滑脂及其制备方法 - Google Patents
一种专用于冶金行业连铸机的润滑脂及其制备方法 Download PDFInfo
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- CN103497813B CN103497813B CN201310391646.2A CN201310391646A CN103497813B CN 103497813 B CN103497813 B CN 103497813B CN 201310391646 A CN201310391646 A CN 201310391646A CN 103497813 B CN103497813 B CN 103497813B
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- Prior art keywords
- base oil
- lubricating grease
- preparation
- acid
- minute
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 239000004519 grease Substances 0.000 title claims abstract description 52
- 230000001050 lubricating effect Effects 0.000 title claims abstract description 47
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000005272 metallurgy Methods 0.000 title claims abstract description 12
- 239000002199 base oil Substances 0.000 claims abstract description 27
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 18
- 230000003647 oxidation Effects 0.000 claims abstract description 16
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 16
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000003112 inhibitor Substances 0.000 claims abstract description 10
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000011575 calcium Substances 0.000 claims abstract description 9
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 9
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 8
- 239000003921 oil Substances 0.000 claims abstract description 8
- 241000158728 Meliaceae Species 0.000 claims abstract description 7
- 239000002253 acid Substances 0.000 claims abstract description 7
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004327 boric acid Substances 0.000 claims abstract description 7
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 7
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 7
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 7
- 150000002632 lipids Chemical class 0.000 claims abstract description 7
- 238000007127 saponification reaction Methods 0.000 claims abstract description 7
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 12
- 238000010792 warming Methods 0.000 claims description 9
- 238000007670 refining Methods 0.000 claims description 7
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical group OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 6
- 239000007866 anti-wear additive Substances 0.000 claims description 6
- -1 octyl group zinc salt Chemical class 0.000 claims description 6
- 239000002480 mineral oil Substances 0.000 claims description 4
- 235000010446 mineral oil Nutrition 0.000 claims description 4
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 3
- YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 claims description 3
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 150000002148 esters Chemical class 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 230000035484 reaction time Effects 0.000 claims description 3
- 238000005070 sampling Methods 0.000 claims description 3
- 238000005086 pumping Methods 0.000 abstract description 6
- 239000000463 material Substances 0.000 abstract description 4
- 239000000047 product Substances 0.000 abstract 1
- 239000013589 supplement Substances 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 14
- 238000005461 lubrication Methods 0.000 description 12
- 235000010216 calcium carbonate Nutrition 0.000 description 6
- 238000009749 continuous casting Methods 0.000 description 6
- 229910000831 Steel Inorganic materials 0.000 description 4
- 238000005266 casting Methods 0.000 description 4
- 239000010959 steel Substances 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- 238000009434 installation Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 208000034189 Sclerosis Diseases 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 230000000903 blocking effect Effects 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 230000001846 repelling effect Effects 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 239000005069 Extreme pressure additive Substances 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 229920002396 Polyurea Polymers 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- VSGNNIFQASZAOI-UHFFFAOYSA-L calcium acetate Chemical compound [Ca+2].CC([O-])=O.CC([O-])=O VSGNNIFQASZAOI-UHFFFAOYSA-L 0.000 description 1
- 239000001639 calcium acetate Substances 0.000 description 1
- 229960005147 calcium acetate Drugs 0.000 description 1
- 235000011092 calcium acetate Nutrition 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- VLHZUYUOEGBBJB-UHFFFAOYSA-N hydroxy stearic acid Natural products OCCCCCCCCCCCCCCCCCC(O)=O VLHZUYUOEGBBJB-UHFFFAOYSA-N 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Landscapes
- Lubricants (AREA)
Abstract
Description
Claims (2)
Priority Applications (1)
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CN201310391646.2A CN103497813B (zh) | 2013-09-02 | 2013-09-02 | 一种专用于冶金行业连铸机的润滑脂及其制备方法 |
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CN201310391646.2A CN103497813B (zh) | 2013-09-02 | 2013-09-02 | 一种专用于冶金行业连铸机的润滑脂及其制备方法 |
Publications (2)
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CN103497813A CN103497813A (zh) | 2014-01-08 |
CN103497813B true CN103497813B (zh) | 2015-08-19 |
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Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105255561A (zh) * | 2015-10-15 | 2016-01-20 | 安徽中天石化股份有限公司 | 一种专用于混料机的润滑脂及其制备方法 |
CN108085118A (zh) * | 2017-12-22 | 2018-05-29 | 原秋杰 | 一种环保型金属加工用酸性润滑剂及工艺 |
CN111500350A (zh) * | 2019-01-31 | 2020-08-07 | 天津海航石油能源科技有限公司 | 一种汽车轴承润滑脂及其制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101824357A (zh) * | 2010-05-27 | 2010-09-08 | 李墨菊 | 一种高性能复合磺酸钙基润滑脂及其制备方法 |
CN102199471A (zh) * | 2010-03-25 | 2011-09-28 | 中国石油化工股份有限公司 | 一种环保型润滑脂组合物及其制备方法 |
CN102703185A (zh) * | 2012-06-15 | 2012-10-03 | 新乡市恒星化工有限责任公司 | 一种复合磺酸钙基润滑脂及其制备方法 |
CN102965178A (zh) * | 2012-10-30 | 2013-03-13 | 武汉博达特种润滑技术有限公司 | 一种高速链条润滑脂及其制备方法 |
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- 2013-09-02 CN CN201310391646.2A patent/CN103497813B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102199471A (zh) * | 2010-03-25 | 2011-09-28 | 中国石油化工股份有限公司 | 一种环保型润滑脂组合物及其制备方法 |
CN101824357A (zh) * | 2010-05-27 | 2010-09-08 | 李墨菊 | 一种高性能复合磺酸钙基润滑脂及其制备方法 |
CN102703185A (zh) * | 2012-06-15 | 2012-10-03 | 新乡市恒星化工有限责任公司 | 一种复合磺酸钙基润滑脂及其制备方法 |
CN102965178A (zh) * | 2012-10-30 | 2013-03-13 | 武汉博达特种润滑技术有限公司 | 一种高速链条润滑脂及其制备方法 |
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C06 | Publication | ||
PB01 | Publication | ||
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SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C56 | Change in the name or address of the patentee | ||
CP03 | Change of name, title or address |
Address after: 246521 Susong Economic Development Zone, Anhui, Anqing Patentee after: ANHUI ZHONG TIAN PETROCHEMICAL Co.,Ltd. Address before: 246521 Susong County Industrial Park, Anhui, Anqing Patentee before: ANQING ZHONGTIAN PETROLEUM CHEMICAL INDUSTRY Co.,Ltd. |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A lubricating grease for continuous casting machine in metallurgical industry and its preparation method Effective date of registration: 20200729 Granted publication date: 20150819 Pledgee: Susong sub branch of China Construction Bank Corp. Pledgor: ANHUI ZHONG TIAN PETROCHEMICAL Co.,Ltd. Registration number: Y2020980004498 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20220919 Granted publication date: 20150819 Pledgee: Susong sub branch of China Construction Bank Corp. Pledgor: ANHUI ZHONG TIAN PETROCHEMICAL Co.,Ltd. Registration number: Y2020980004498 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A lubricating grease specially used for continuous casting machine in metallurgical industry and its preparation method Effective date of registration: 20220930 Granted publication date: 20150819 Pledgee: Susong sub branch of China Construction Bank Corp. Pledgor: ANHUI ZHONG TIAN PETROCHEMICAL Co.,Ltd. Registration number: Y2022980017334 |