CN103482905B - Environment-friendly ultraviolet light resistant and high-temperature resistant paint for outer walls of buildings - Google Patents
Environment-friendly ultraviolet light resistant and high-temperature resistant paint for outer walls of buildings Download PDFInfo
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- CN103482905B CN103482905B CN201310430321.0A CN201310430321A CN103482905B CN 103482905 B CN103482905 B CN 103482905B CN 201310430321 A CN201310430321 A CN 201310430321A CN 103482905 B CN103482905 B CN 103482905B
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Abstract
Environment-friendly ultraviolet light resistant and high-temperature resistant paint for outer walls of buildings comprises A compositions, B compositions and a C composition, wherein the A compositions comprise the following substances in parts by weight: 25-35 parts of polyaspartic acid ester resin, 20 parts of an aromatics mixed solvent, 8-10 parts of nano-scale ceramic powder, 2-4 parts of mica powder, 10-18 parts of diacetone alcohol, 3-8 parts of ethylene glycol monobutyl ether, 7-11 parts of a cellulose thickener solution with the mass percent of 2%, 1.0-1.4 parts of a polyphosphate dispersing agent solution with the mass percent of 10%, 1-3 parts of an emulgator, 0.1-0.3 part of sodium hydroxide, 30-50 parts of ethyl alcohol, 70-100 parts of deionized water, 140-180 parts of titanium dioxide; the B compositions comprise the following substances in parts by weight: 3-5 parts of a paint curing agent, 0.02-1 part of an initiator, 1 part of a dispersing agent, 0.6 part of a flatting agent, 0.3 part of an antifoaming agent, 0.3 part of a defoaming agent, 25 parts of a modified ammonia curing agent, 2-4 parts of tetrachloroisophthalonitrile, 3-5 parts of a dry film antiseptic; the C composition is an environment-friendly color mixed-phase inorganic pigment.
Description
Technical field
The present invention relates to a kind of new anti-corrosion coating and preparation method thereof, more particularly, relate to a kind of environment-friendly type building beyond the region of objective existence wall uvioresistant, high-temperature resistant coating.
Background technology
In prior art, conventional skin coating is mostly be coating prepared by base-material with vinylbenzene-ACRYLIC EMULSION, pure acrylic latex or elastomeric propylene yogurt liquid.Its shortcoming produces fine cracks after being applied to body of wall, puts forth effort poor, anti-pollution characteristic and poor performance at low temperatures etc.; In addition, be material owing to there is vinylbenzene in coating, smell is quite dense; When exterior wall applies, smell distributes in an atmosphere in a large number, causes pollution; And the set time of such coating is relatively long, therefore, should be noted that Changes in weather during coating, can not constructs in the rainfall connected, therefore, have larger limitation.In NORTHWEST CHINA area, summer is hot, and sun heat radiation intensity is high, and body surface temperature can up to more than more than 70 degrees Celsius, and winter-spring season then dust storm is very large, very strong to the wind abrasion of paint film.Anti-blown sand coating practical in the market adopts urethane, and weathering resistance and anti-blown sand performance generally, and do not have solar heat reflection function, do not have the effect of cooling energy-saving.
Because the constant temperature of the outer surface of building shined upon for a long time raises, the temperature of the material of construction outside surfaces such as outer surface of building is cement, concrete, ceramic tile, metal, insulating brick can reach 40-50 DEG C, on color steel, water-proof material, temperature can reach 60 DEG C, reaches the temperature of boiling hot people.Under such outer surface of building high temperature, in habitat, the inevitable rising of the temperature of plant floor etc., live to normal human subject, material deposits, the safety of equipment all causes very large impact, likely can produce the great potential safety hazards such as blast, if temperature is too high, need cooling, cause the significant wastage of the energy simultaneously.
In order to reduce the thermal radiation of the sun, by improving the absorption of reflection minimizing to sunlight heat, therefore there is heat insulation, to reflect functions such as lowering the temperature, anticorrosion coating arise at the historic moment, become reducing sun heat radiation harm to a great extent in the urgent need to, these coating there are fabulous market outlook of painting industry.But there is certain toxicity in traditional reflective insulation material, and unstable chemcial property, not easily preserve for a long time, heat-reflecting heat-insulating performance in time and the change of environment and the defect of change etc.Consider above-mentioned practical situation, those skilled in the art is being devoted to study a kind of novel water corrosion-resistant epoxy paint always, replace existing solvent-borne type protective system, and need again good sticking power, lower cost and better simply preparation method simultaneously.
Summary of the invention
For the deficiency that prior art exists, the invention provides a kind of unioresistant, high-temperature resistant coating.
To achieve these goals, technical scheme of the present invention is as follows:
A kind of environment-friendly type building beyond the region of objective existence wall uvioresistant, high-temperature resistant coating, it is by component A, B component and component C are formed, each component consists of by weight: containing following material and content: polyaspartic ester resin 25-35 part, aromatic hydrocarbons mixed solvent 20 parts, nanometer scale ceramics powder 8-10 part, mica powder 2 ~ 4 parts, diacetone alcohol 10-18 part, ethylene glycol monobutyl ether: 3 ~ 8 parts, the cellulose thickener solution of 2% mass percent 7 ~ 11 parts, the polyphosphoric acid salt dispersant solution of 10% mass percent 1.0 ~ 1.4 parts, emulsifying agent: 1 ~ 3 part, sodium hydroxide: 0.1 ~ 0.3 part, ethanol: 30 ~ 50 parts, deionized water: 70 ~ 100 parts, titanium dioxide: 140 ~ 180 parts, component B, by by weight, includes following material and content: coating curing agent: 3 ~ 5 parts, initiator 0.02 ~ 1 part, dispersion agent 1, flow agent 0.6, defoamer 0.3, deaerating agent 0.3, 25 parts, modification Ammonia solidifying agent, daconil M: 2 ~ 4 parts, dry film mould inhibitor: 5 ~ 3 parts, component C is environment protection colour mixed phase mineral dye, skin coating described above, it prepares by the following method:
The first step: each raw material of weighing: polyaspartic ester resin 25-35 part, aromatic hydrocarbons mixed solvent 20 parts, diacetone alcohol 10-18 part, ethylene glycol monobutyl ether: 3 ~ 8 parts, emulsifying agent: 1 ~ 3 part, sodium hydroxide: 0.1 ~ 0.3 part, ethanol: 30 ~ 50 parts, deionized water: 70 ~ 100 parts, titanium dioxide: press titanium dioxide 18 ~ 22 parts for 140 ~ 180 parts, talcum powder 8 ~ 15 parts, 5 ~ 10 parts, calcium carbonate, mica powder 2 ~ 4 parts, the cellulose thickener solution of 2% mass percent 7 ~ 11 parts, the polyphosphoric acid salt dispersant solution 1.0 ~ 1.4 parts of 10% mass percent takes and separated,
Second step: abrasive grains raw material: titanium dioxide, talcum powder, calcium carbonate, mica powder are mixed merga pass shredder and be ground to particle minimum diameter≤50 μm, obtain mix fine particle,
3rd step: dissolve: second step is ground other raw material that the fine particle of the mixing obtained and the first step take and put into reaction vessel together, stir when being heated to 50 ~ 60 DEG C, churning time is 45 ~ 60 minutes, obtains mixed emulsion;
4th step: filter: namely the 3rd step gained mixed emulsion is obtained environment-friendly type building thing exterior coating by 80 ~ 100 mesh sieve inherent filtrations;
5th step: ratio takes the various raw material of component B and mixing and stirring loads container namely obtains finished product component B by weight;
6th step: according to component A: component B: component C=(600 ~ 1000): (30 ~ 50): the weight ratio of 1 takes component C and inserts in container the component C that gets product; And rationally take component A and component B in proportion;
7th step: the finished product component C claimed in the 6th step inserted in finished product component B, abundant stirring and dissolving, obtains lysate; Lysate is joined in finished product component A, stir and obtain skin epoxypaint.
Described dispersion agent is EFKA-5065 dispersion agent and the EFKA-4050 dispersion agent mixture according to 1:3; The EFKA-3777 flow agent that described flow agent is and EFKA-3239 flow agent are according to the mixture of 2:1, and defoamer is hydrophobically modified silicon-dioxide or mineral oil.Defoamer is polydimethylsiloxane or silicone emulsion or the fatty acid ester compounded thing of higher alcohols or polyoxyethylene polyoxypropylene tetramethylolmethane ether or polyoxyethylene polyoxy propyl alcohol amidogen ether or polypropylene glycerol aether and polyoxypropylene.Described mould inhibitor is Sodium Fluoride or 10, the two phenoxazine arsenic of 10 '-oxo.
Therefore, the present invention has following main beneficial effect: good fluidity, anti-mildew and anti-corrosion performance is excellent, coating dry fast with setting rate, match colors flexible, be convenient to rapid construction, making method is simple, easy to operate, required equipment is simple and easy, do not need the input of a large amount of equipment aspects.
Embodiment
In order to further illustrate the present invention, below in conjunction with embodiment, inner wall heat-preservation coating provided by the invention is described in detail, but they can not be interpreted as limiting the scope of the present invention.
Embodiment 1
A kind of environment-friendly type building beyond the region of objective existence wall uvioresistant, high-temperature resistant coating, it is by component A, B component and component C are formed, each component consists of by weight: containing following material and content: polyaspartic ester resin 25-35 part, aromatic hydrocarbons mixed solvent 20 parts, nanometer scale ceramics powder 8-10 part, mica powder 2 ~ 4 parts, diacetone alcohol 10-18 part, ethylene glycol monobutyl ether: 3 ~ 8 parts, the cellulose thickener solution of 2% mass percent 7 ~ 11 parts, the polyphosphoric acid salt dispersant solution of 10% mass percent 1.0 ~ 1.4 parts, emulsifying agent: 1 ~ 3 part, sodium hydroxide: 0.1 ~ 0.3 part, ethanol: 30 ~ 50 parts, deionized water: 70 ~ 100 parts, titanium dioxide: 140 ~ 180 parts, component B, by by weight, includes following material and content: coating curing agent: 3 ~ 5 parts, initiator 0.02 ~ 1 part, dispersion agent 1, flow agent 0.6, defoamer 0.3, deaerating agent 0.3, 25 parts, modification Ammonia solidifying agent, daconil M: 2 ~ 4 parts, dry film mould inhibitor: 5 ~ 3 parts, component C is environment protection colour mixed phase mineral dye, skin coating described above, it prepares by the following method:
The first step: each raw material of weighing: polyaspartic ester resin 25-35 part, aromatic hydrocarbons mixed solvent 20 parts, diacetone alcohol 10-18 part, ethylene glycol monobutyl ether: 3 ~ 8 parts, emulsifying agent: 1 ~ 3 part, sodium hydroxide: 0.1 ~ 0.3 part, ethanol: 30 ~ 50 parts, deionized water: 70 ~ 100 parts, titanium dioxide: press titanium dioxide 18 ~ 22 parts for 140 ~ 180 parts, talcum powder 8 ~ 15 parts, 5 ~ 10 parts, calcium carbonate, mica powder 2 ~ 4 parts, the cellulose thickener solution of 2% mass percent 7 ~ 11 parts, the polyphosphoric acid salt dispersant solution 1.0 ~ 1.4 parts of 10% mass percent takes and separated,
Second step: abrasive grains raw material: titanium dioxide, talcum powder, calcium carbonate, mica powder are mixed merga pass shredder and be ground to particle minimum diameter≤50 μm, obtain mix fine particle,
3rd step: dissolve: second step is ground other raw material that the fine particle of the mixing obtained and the first step take and put into reaction vessel together, stir when being heated to 50 ~ 60 DEG C, churning time is 45 ~ 60 minutes, obtains mixed emulsion;
4th step: filter: namely the 3rd step gained mixed emulsion is obtained environment-friendly type building thing exterior coating by 80 ~ 100 mesh sieve inherent filtrations;
5th step: ratio takes the various raw material of component B and mixing and stirring loads container namely obtains finished product component B by weight;
6th step: according to component A: component B: component C=(600 ~ 1000): (30 ~ 50): the weight ratio of 1 takes component C and inserts in container the component C that gets product; And rationally take component A and component B in proportion;
7th step: the finished product component C claimed in the 6th step inserted in finished product component B, abundant stirring and dissolving, obtains lysate; Lysate is joined in finished product component A, stir and obtain skin epoxypaint.
Described dispersion agent is EFKA-5065 dispersion agent and the EFKA-4050 dispersion agent mixture according to 1:3; The EFKA-3777 flow agent that described flow agent is and EFKA-3239 flow agent are according to the mixture of 2:1, and defoamer is hydrophobically modified silicon-dioxide or mineral oil.Defoamer is polydimethylsiloxane or silicone emulsion or the fatty acid ester compounded thing of higher alcohols or polyoxyethylene polyoxypropylene tetramethylolmethane ether or polyoxyethylene polyoxy propyl alcohol amidogen ether or polypropylene glycerol aether and polyoxypropylene.Described mould inhibitor is Sodium Fluoride or 10, the two phenoxazine arsenic of 10 '-oxo.
The present invention detects the performance of the coating obtained, and detailed process is as follows:
Employing " GB/T 9756-2009 synthetic paint resin emulsion interior wall coating " detects the Typical physical performances such as outward appearance, application property and the water tolerance obtaining the inner wall heat-preservation coating that the present embodiment obtains;
" in GB 18582-2008 indoor decorating and refurnishing materials interior wall coating limits of harmful substances standard " is adopted to measure the harmful substance contents of the interior wall that the present embodiment provides;
Fungicidal properties is excellent: what product of the present invention is coated in buildings does not get on the exterior wall of sunlight, under the natural condition of 20-40 DEG C of outside air temperatures, continuous every day identical tap water is sprayed for metope of the same area, in 60 days, use on skin of the present invention and do not see any mildew, and in prior art, employ the exterior coating of 20 brands at random, there is mildew in various degree.
The present invention have passed through following Performance Detection: have employed the coating that preparation method of the present invention obtains, its key technical indexes as shown in the table:
| Sequence number | Interventions Requested | Technical requirements | Assay | Conclusion |
| 1 | Condition in container | Without lump, in uniform state after stirring | Meet the requirements | Qualified |
| 2 | Smell | Tasteless | Meet the requirements | Qualified |
| 3 | Application property | Brush two roads accessible | Meet the requirements | Qualified |
| 4 | Low-temperature stability (-20 DEG C) | Never degenerate | Meet the requirements | Qualified |
| 5 | 25 DEG C of set times | ≤24h | 12h | Qualified |
| 6 | Appearance of film | Normally | Meet the requirements | Qualified |
| 7 | Water-fastness | 96h is without exception | Meet the requirements | Qualified |
| 8 | Acid resistance | 48h is without exception | Meet the requirements | Qualified |
| 9 | Abrasion resistance (secondary) | ≥500 | 2500 | Qualified |
| 10 | Midew proof | During humidity 40%, continuous 60 days without mildew | Without mildew | Qualified |
As can be seen from the above table, the water corrosion-resistant epoxy paint prepared by method of the present invention, comparing other water-based anticorrosive paint has following advantage:
1. higher to the sticking power of base material;
2. film chemical-resistant is better;
3. can be used in combination with other waterborne polymeric, complementary in performance;
4. raw material variety is few, pollution-free, and making method is simple, and required equipment is few: without benzene, aldehydes matter in the present invention, therefore pollution-free, and basic odorlessness; Starting material in the present invention are easily purchased and advantage of lower cost; Only need in the present invention once to heat, and carry out at ambient pressure, therefore do not need complicated reactor, security improves greatly.
More than show and describe ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (4)
1. an environment-friendly type building beyond the region of objective existence wall uvioresistant, high-temperature resistant coating, it is by component A, B component and component C are formed, each component consists of by weight: containing following material and content: component A is by by weight, include following material and content: polyaspartic ester resin 25-35 part, aromatic hydrocarbons mixed solvent 20 parts, nanometer scale ceramics powder 8-10 part, mica powder 2 ~ 4 parts, diacetone alcohol 10-18 part, ethylene glycol monobutyl ether: 3 ~ 8 parts, the cellulose thickener solution of 2% mass percent 7 ~ 11 parts, the polyphosphoric acid salt dispersant solution of 10% mass percent 1.0 ~ 1.4 parts, emulsifying agent: 1 ~ 3 part, sodium hydroxide: 0.1 ~ 0.3 part, ethanol: 30 ~ 50 parts, deionized water: 70 ~ 100 parts, titanium dioxide: 140 ~ 180 parts, component B, by by weight, includes following material and content: coating curing agent: 3 ~ 5 parts, initiator 0.02 ~ 1 part, dispersion agent 1, flow agent 0.6, defoamer 0.3, deaerating agent 0.3, 25 parts, modification Ammonia solidifying agent, daconil M: 2 ~ 4 parts, dry film mould inhibitor: 5 ~ 3 parts, component C is environment protection colour mixed phase mineral dye, skin coating described above, it prepares by the following method:
The first step: each raw material of weighing: polyaspartic ester resin 25-35 part, aromatic hydrocarbons mixed solvent 20 parts, diacetone alcohol 10-18 part, ethylene glycol monobutyl ether: 3 ~ 8 parts, emulsifying agent: 1 ~ 3 part, sodium hydroxide: 0.1 ~ 0.3 part, ethanol: 30 ~ 50 parts, deionized water: 70 ~ 100 parts, titanium dioxide: press titanium dioxide 18 ~ 22 parts for 140 ~ 180 parts, talcum powder 8 ~ 15 parts, 5 ~ 10 parts, calcium carbonate, mica powder 2 ~ 4 parts, the cellulose thickener solution of 2% mass percent 7 ~ 11 parts, the polyphosphoric acid salt dispersant solution 1.0 ~ 1.4 parts of 10% mass percent takes and separated,
Second step: abrasive grains raw material: titanium dioxide, talcum powder, calcium carbonate, mica powder are mixed merga pass shredder and be ground to particle minimum diameter≤50 μm, obtain mix fine particle,
3rd step: dissolve: second step is ground other raw material that the fine particle of the mixing obtained and the first step take and put into reaction vessel together, stir when being heated to 50 ~ 60 DEG C, churning time is 45 ~ 60 minutes, obtains mixed emulsion;
4th step: filter: namely the 3rd step gained mixed emulsion is obtained environment-friendly type building thing exterior coating by 80 ~ 100 mesh sieve inherent filtrations;
5th step: ratio takes the various raw material of component B and mixing and stirring loads container namely obtains finished product component B by weight;
6th step: according to component A: component B: component C=(600 ~ 1000): (30 ~ 50): the weight ratio of 1 takes component C and inserts in container the component C that gets product; And rationally take component A and component B in proportion;
7th step: the finished product component C claimed in the 6th step inserted in finished product component B, abundant stirring and dissolving, obtains lysate; Lysate is joined in finished product component A, stir and obtain skin epoxypaint.
2. environment-friendly type building beyond the region of objective existence wall uvioresistant according to claim 1, high-temperature resistant coating, is characterized in that: described dispersion agent is EFKA-5065 dispersion agent and the EFKA-4050 dispersion agent mixture according to 1:3; The EFKA-3777 flow agent that described flow agent is and EFKA-3239 flow agent are according to the mixture of 2:1, and defoamer is hydrophobically modified silicon-dioxide or mineral oil.
3. environment-friendly type building beyond the region of objective existence wall uvioresistant according to claim 1, high-temperature resistant coating, is characterized in that: defoamer is polydimethylsiloxane or silicone emulsion or the fatty acid ester compounded thing of higher alcohols or polyoxyethylene polyoxypropylene tetramethylolmethane ether or polyoxyethylene polyoxy propyl alcohol amidogen ether or polypropylene glycerol aether and polyoxypropylene.
4. environment-friendly type building beyond the region of objective existence wall uvioresistant according to claim 1, high-temperature resistant coating, is characterized in that: described mould inhibitor is Sodium Fluoride or 10, the two phenoxazine arsenic of 10 '-oxo.
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| CN201310430321.0A CN103482905B (en) | 2013-09-22 | 2013-09-22 | Environment-friendly ultraviolet light resistant and high-temperature resistant paint for outer walls of buildings |
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| CN201310430321.0A CN103482905B (en) | 2013-09-22 | 2013-09-22 | Environment-friendly ultraviolet light resistant and high-temperature resistant paint for outer walls of buildings |
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| CN103482905B true CN103482905B (en) | 2015-07-01 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105925105A (en) * | 2016-06-27 | 2016-09-07 | 青岛华联装饰工程有限公司 | Quick-dried external building coating material and preparation method thereof |
| CN106118159A (en) * | 2016-06-27 | 2016-11-16 | 青岛华联装饰工程有限公司 | A kind of uvioresistant, resistant to elevated temperatures skin coating and preparation method thereof |
| CN106082880A (en) * | 2016-06-27 | 2016-11-09 | 青岛华联装饰工程有限公司 | A kind of environmental protection flame retardant architectural decoration coating material and preparation method thereof |
| CN110863343B (en) * | 2019-11-27 | 2023-06-06 | 浙江圣山科纺有限公司 | Environment-friendly ultraviolet-resistant finishing agent and outdoor cloth applying same |
| CN112979990B (en) * | 2021-02-06 | 2022-08-02 | 佛山市万化科技有限公司 | Water-based polyaspartic acid ester emulsion and preparation method thereof |
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| JPH0274549A (en) * | 1988-09-08 | 1990-03-14 | Hitachi Chem Co Ltd | Production of translucent artificial stone |
| KR100260020B1 (en) * | 1998-02-05 | 2000-06-15 | 장병주 | Liquefied non-shrinkage mixture for crack prevention of cement mortar and concrete |
| CN102108244A (en) * | 2010-12-22 | 2011-06-29 | 北京东方雨虹防水技术股份有限公司 | Fatty group polyurea finish with high elongation rate and preparation method thereof |
| CN102250505A (en) * | 2011-07-27 | 2011-11-23 | 株洲时代电气绝缘有限责任公司 | Putty for repairing aerogenerator blade and preparation method therefore |
| CN102775877A (en) * | 2012-07-19 | 2012-11-14 | 洛阳七维防腐工程材料有限公司 | Method for preparing and spaying anticorrosion coating for western wind farm tower |
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2013
- 2013-09-22 CN CN201310430321.0A patent/CN103482905B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0274549A (en) * | 1988-09-08 | 1990-03-14 | Hitachi Chem Co Ltd | Production of translucent artificial stone |
| KR100260020B1 (en) * | 1998-02-05 | 2000-06-15 | 장병주 | Liquefied non-shrinkage mixture for crack prevention of cement mortar and concrete |
| CN102108244A (en) * | 2010-12-22 | 2011-06-29 | 北京东方雨虹防水技术股份有限公司 | Fatty group polyurea finish with high elongation rate and preparation method thereof |
| CN102250505A (en) * | 2011-07-27 | 2011-11-23 | 株洲时代电气绝缘有限责任公司 | Putty for repairing aerogenerator blade and preparation method therefore |
| CN102775877A (en) * | 2012-07-19 | 2012-11-14 | 洛阳七维防腐工程材料有限公司 | Method for preparing and spaying anticorrosion coating for western wind farm tower |
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