CN103421608A - Preparation method of essence containing natural honeysuckle extract and toothpaste containing essence - Google Patents
Preparation method of essence containing natural honeysuckle extract and toothpaste containing essence Download PDFInfo
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- CN103421608A CN103421608A CN2013103599871A CN201310359987A CN103421608A CN 103421608 A CN103421608 A CN 103421608A CN 2013103599871 A CN2013103599871 A CN 2013103599871A CN 201310359987 A CN201310359987 A CN 201310359987A CN 103421608 A CN103421608 A CN 103421608A
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Abstract
The invention relates to oral hygiene products, in particular to a preparation method of essence containing natural honeysuckle extract and a toothpaste containing the essence. The method includes: weighing honeysuckle, ethanol and purified water for mixing, soaking under negative pressure, heating for decoction, and filtering to obtain filtrate and residue; decoloring the filtrate, and concentrating to obtain honeysuckle extract; well mixing natural menthol, dementholized peppermint oil, fennel oil, eugenol and spearmint oil with the honeysuckle extract, and standing to obtain the honeysuckle extract essence. The honeysuckle extract essence is rich, stable and lasting in fragrance, capable of decreasing swelling to relieve pain, activating blood to scatter stasis, removing prickly heat to stop itching and refreshing. The toothpaste containing the essence is capable of clearing heat, decreasing internal heat, diminishing inflammation, removing bad breath, and the like, and especially capable of well relieving gum swelling and bleeding. Due to the fact that the ingredients of the toothpaste are the natural extract, natural inflammation diminishing, pain easing and bleeding stopping functions are provided without any side effects.
Description
Technical field
The present invention relates to dental care products, specifically relate to a kind of essence that contains natural Flos Lonicerae extract and toothpaste preparation method.
Background technology
Toothpaste is to be used from cleaning teeth with toothbrush one, the protection oral hygiene, and a kind of daily necessities to human-body safety, have very long history.Along with social progress, various types of toothpaste is come out one after another, and natural extract is applied in toothpaste and solves relevant oral problem as activeconstituents, has become market mainstream focus.
Japanese Honeysuckle is the general designation of Chinese medicinal materials and plant.The plant Japanese Honeysuckle has another name called honeysuckle, is the perennial half evergreen winding bejuco of Caprifoliaceae." Japanese Honeysuckle " one come from Compendium of Material Medica, because Flos Lonicerae is just opened as white, after transfer yellow to, Japanese Honeysuckle hence obtains one's name.The medicinal material Japanese Honeysuckle is Caprifoliaceae woodbine honeysuckle and belongs to together, the plant drying Alabastrum or just opened flower.Japanese Honeysuckle is described as clearing heat and detoxicating good medicine from ancient times.The sweet cold air fragrance of its property, clearing away heat with drugs sweet in flavor and cold in nature and not injuring one's stomach, fragrance thoroughly reaches and can be eliminating evil.Japanese Honeysuckle can dispelling wind-heat, removing summer-heat blood poison, and for various febrile diseases, as body heat, dermexanthesis, send out the diseases such as spot, hot carbuncle carbuncle, swelling and pain in the throat, all effect is remarkable.
Summary of the invention
One of purpose of the present invention be to provide a kind ofly have that swelling and pain relieving, promoting blood circulation to remove blood stasis, the miliaria of dispelling are antipruritic, the natural Flos Lonicerae extract essence of the effect that produces refreshing effect to the mind and preparation method thereof.
In order to realize this purpose, the technical solution adopted in the present invention is: a kind of preparation method of natural Flos Lonicerae extract essence comprises the steps:
1., taking is Japanese Honeysuckle by weight proportion: ethanol: pure water=0.6～1.25: 0.45～0.85: 3.5～4.5 raw material;
2., Japanese Honeysuckle, ethanol, pure water are mixed, be-0.050 in vacuum tightness～-soak 36～48h under the condition of 0.060MPa, reheat decoction 4～5h, filter to get filtrate and filter residue;
3., by filtrate decolouring, and (for example, before concentrated, be 80～120L, concentrated then be 1L) concentrated to be by volume 80～120: 1, obtains Flos Lonicerae extract;
4., according to the weight part meter, 10～15 parts of 18～25 parts of Natural menthols, 30～36 parts of Peppermint Oils, 0.8～1.2 part of olium anisi, 0.4～0.6 part of Eugenol, 0.5～1 part of Oleum Menthae Rotundifoliae and Flos Lonicerae extracts are stirred, standing 12～36h, obtain natural Flos Lonicerae extract essence.
Preferably, described step 1. in the volumn concentration of ethanol be 40～75%.
Preferably, described step 2. middle decocting time is 4.5h, and decocting temperature is 65～85 ℃.
Preferably, described step is concentrated in 3. is to carry out at 100: 1 by volume, and thickening temperature is 70～100 ℃.
Preferably, described step 4. in time of repose be 24h.
In addition, the invention also discloses a kind of natural Flos Lonicerae extract essence according to the described preparation of above-mentioned preparation method.
Another object of the present invention is to provide a good drug efficacy, without any side effects, can play heat-clearing, fall fire, the effects such as anti-inflammatory, antihalitosis, there is especially the toothpaste of good remission effect for gum redness and gingival hemorrhage.
In order to realize this purpose, the technical solution adopted in the present invention is: the toothpaste that contains natural Flos Lonicerae extract essence, contain weight ratio and be 1.5～2.5% natural Flos Lonicerae extract essence in its lotion total composition.
As a kind of preferred implementation of the toothpaste that contains natural Flos Lonicerae extract essence of the present invention, this toothpaste also comprises following component:
Three of purpose of the present invention is to provide a kind of preparation method of this toothpaste, comprises the steps:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1;
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2;
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, heat 5～10min, form mixture D 3;
D, sorbyl alcohol is mixed with mixture D 2, heat 5～10min, form mixture D 4;
E, mixture D 3, D4 are added in the emulsification pot, add natural Flos Lonicerae extract essence and mix, under vacuum, stir 3～5min, make lotion, be filled into multiple-unit tube.
Preferably, described step c Heating temperature is 50～70 ℃, and the steps d Heating temperature is 60～70 ℃.
The essence that the present invention contains natural Flos Lonicerae extract and toothpaste preparation method, its beneficial effect shows:
1, the natural Flos Lonicerae extract essence of preparation give off a strong fragrance, stable and stay length, and have can swelling and pain relieving, promoting blood circulation to remove blood stasis, the miliaria of dispelling is antipruritic, the effect that produces refreshing effect to the mind.
2, the toothpaste that contains natural Flos Lonicerae extract essence of preparation, can play heat-clearing, fall fire, the effects such as anti-inflammatory, antihalitosis, has good remission effect for gum redness and gingival hemorrhage especially.Because main component is natural extract, there is natural anti-inflammatory, analgesia, hemostatic function, without any side effects.Simultaneously, old and young women and children are all suitable, and life-time service is useful and harmless.
3, the manufacture craft of toothpaste is simple, is applicable to suitability for industrialized production.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated, it should be noted that, various raw materials are the delicatessen food level, or obtain according to the prior art preparation.
Embodiment 1
1, the preparation of natural Flos Lonicerae extract essence
1., extracting honeysuckle 416g (after drying, lower with), 70% ethanol 283g and pure water 1500g mix, and under the condition that is-0.050MPa in vacuum tightness, soaks 48h.
2., be heated to 85 ℃ and decoct 4.5h, filter to get filtrate and filter residue.
3., by filtrate with gac (weight percent is not higher than 5%) decolouring, 100 ℃ of constant temperature are concentrated into the 20g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 37g, Peppermint Oil 47g, olium anisi 1.7g, Eugenol 0.8g and Oleum Menthae Rotundifoliae 1.3g, stir, standing 24h, obtain natural Flos Lonicerae extract essence.
The preparation of the toothpaste that 2, contains natural Flos Lonicerae extract essence
Composition and ratio is as following table (in 100g, lower same)
| Raw material | Weight/g | Raw material | Weight/g |
| Natural Flos Lonicerae extract essence | 2.5 | Sodium monoflurophosphate | 1 |
| Sorbyl alcohol | 75 | Tertiary sodium phosphate | 0.5 |
| Silicon-dioxide | 17 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 50 ℃ of heating 10min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,70 ℃ of heating 10min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural Flos Lonicerae extract essence and mix, under vacuum, stir 5min, make lotion, be filled into multiple-unit tube.
Embodiment 2
1, the preparation of natural Flos Lonicerae extract essence
1., extracting honeysuckle 400g, 65% ethanol 275g and pure water 1400g mix, and under the condition that is-0.060MPa in vacuum tightness, soaks 45h.
2., be heated to 75 ℃ and decoct 4h, filter to get filtrate and filter residue.
3., by filtrate decolouring, 95 ℃ of constant temperature are concentrated into the 19g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 36g, Peppermint Oil 45g, olium anisi 1.6g, Eugenol 0.7g and Oleum Menthae Rotundifoliae 1.2g, stir, standing 18h, obtain natural Flos Lonicerae extract essence.
The preparation of the toothpaste that 2, contains natural Flos Lonicerae extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural Flos Lonicerae extract essence | 2.2 | Sodium monoflurophosphate | 0.9 |
| Sorbyl alcohol | 68 | Tertiary sodium phosphate | 0.45 |
| Silicon-dioxide | 20 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 60 ℃ of heating 7min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,65 ℃ of heating 5min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural Flos Lonicerae extract essence and mix, under vacuum, stir 4min, make lotion, be filled into multiple-unit tube.
Embodiment 3
1, the preparation of natural Flos Lonicerae extract essence
1., extracting honeysuckle 380g, 60% ethanol 275g and pure water 1400g mix, and under the condition that is-0.060MPa in vacuum tightness, soaks 40h.
2., be heated to 75 ℃ and decoct 5h, filter to get filtrate and filter residue.
3., by filtrate decolouring, 90 ℃ of constant temperature are concentrated into the 17g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 34g, Peppermint Oil 43g, olium anisi 1.4g, Eugenol 0.7g and Oleum Menthae Rotundifoliae 1.1g, stir, standing 30h, obtain natural Flos Lonicerae extract essence.
The preparation of the toothpaste that 2, contains natural Flos Lonicerae extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural Flos Lonicerae extract essence | 2 | Sodium monoflurophosphate | 0.8 |
| Sorbyl alcohol | 67 | Tertiary sodium phosphate | 0.35 |
| Silicon-dioxide | 20 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 65 ℃ of heating 5min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,60 ℃ of heating 10min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural Flos Lonicerae extract essence and mix, under vacuum, stir 3min, make lotion, be filled into multiple-unit tube.
Embodiment 4
1, the preparation of natural Flos Lonicerae extract essence
1., extracting honeysuckle 360g, 50% ethanol 260g and pure water 1300g mix, and under the condition that is-0.050MPa in vacuum tightness, soaks 38h.
2., be heated to 73 ℃ and decoct 4h, filter to get filtrate and filter residue.
3., by filtrate decolouring, 80 ℃ of constant temperature are concentrated into the 16g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 26g, Peppermint Oil 38g, olium anisi 1.2g, Eugenol 0.6g and Oleum Menthae Rotundifoliae 1g, stir, standing 12h, obtain natural Flos Lonicerae extract essence.
The preparation of the toothpaste that 2, contains natural Flos Lonicerae extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural Flos Lonicerae extract essence | 1.8 | Sodium monoflurophosphate | 0.7 |
| Sorbyl alcohol | 75 | Tertiary sodium phosphate | 0.25 |
| Silicon-dioxide | 18 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 70 ℃ of heating 8min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,70 ℃ of heating 5min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural Flos Lonicerae extract essence and mix, under vacuum, stir 3min, make lotion, be filled into multiple-unit tube.
Embodiment 5
1, the preparation of natural Flos Lonicerae extract essence
1., extracting honeysuckle 320g, 45% ethanol 250g and pure water 1200g mix, and under the condition that is-0.055MPa in vacuum tightness, soaks 37h.
2., be heated to 72 ℃ and decoct 5h, filter to get filtrate and filter residue.
3., by filtrate decolouring, 80 ℃ of constant temperature are concentrated into the 13g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 21g, Peppermint Oil 33g, olium anisi 1g, Eugenol 0.5g and Oleum Menthae Rotundifoliae 0.7g, stir, standing 36h, obtain natural Flos Lonicerae extract essence.
The preparation of the toothpaste that 2, contains natural Flos Lonicerae extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural Flos Lonicerae extract essence | 1.7 | Sodium monoflurophosphate | 0.6 |
| Sorbyl alcohol | 75 | Tertiary sodium phosphate | 0.15 |
| Silicon-dioxide | 18 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 55 ℃ of heating 5min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,60 ℃ of heating 8min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural Flos Lonicerae extract essence and mix, under vacuum, stir 4min, make lotion, be filled into multiple-unit tube.
Embodiment 6
1, the preparation of natural Flos Lonicerae extract essence
1., extracting honeysuckle 200g, 40% ethanol 150g and pure water 1000g mix, and under the condition that is-0.055MPa in vacuum tightness, soaks 36h.
2., be heated to 65 ℃ and decoct 4h, filter to get filtrate and filter residue.
3., by filtrate decolouring, 80 ℃ of constant temperature are concentrated into the 10g Flos Lonicerae extract.
4., in Flos Lonicerae extract, add Natural menthol 18g, Peppermint Oil 30g, olium anisi 0.8g, Eugenol 0.4g and Oleum Menthae Rotundifoliae 0.5g, stir, standing 25h, obtain natural Flos Lonicerae extract essence.
The preparation of the toothpaste that 2, contains natural Flos Lonicerae extract essence
Composition and ratio is as following table
| Raw material | Weight/g | Raw material | Weight/g |
| Natural Flos Lonicerae extract essence | 1.5 | Sodium monoflurophosphate | 0.55 |
| Sorbyl alcohol | 50 | Tertiary sodium phosphate | 0.1 |
| Silicon-dioxide | 21 | Xylo-Mucine | 1.2 |
| The lauryl alcohol sodium sulfovinate | 1.65 | Soluble saccharin | 0.25 |
| Pure water | Complement to 100 | ? | ? |
Preparation process is:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1.
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2.
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, 65 ℃ of heating 9min, form mixture D 3.
D, sorbyl alcohol is mixed with mixture D 2,65 ℃ of heating 5min, form mixture D 4.
E, mixture D 3, D4 are added in the emulsification pot, add natural Flos Lonicerae extract essence and mix, under vacuum, stir 5min, make lotion, be filled into multiple-unit tube.
The comparative example 1
Only be with the difference of embodiment 1, do not add natural Flos Lonicerae extract essence while preparing toothpaste, other component and content identical with embodiment 1 (not enough 100g supplies with pure water).
Clinical trial result
Test method: choose there are gingival hemorrhage, the red and swollen symptom experimenter of gum 90 people are tested, men and women each half, the age is from 18～59 years old, 30 years old mean age.Be divided at random 2 groups, experimental group is used the toothpaste (being added with natural Flos Lonicerae extract essence) of embodiment 1 preparation, control group is used the toothpaste (not adding natural Flos Lonicerae extract essence) of comparative example's 1 preparation, and every morning, evening respectively brush teeth once.
Brush teeth before test, first record experimenter's the red and swollen symptom of gingival hemorrhage, gum.
Brush teeth test after the 7th day, the more unified red and swollen symptom variation of gingival hemorrhage, gum of checking the experimenter.
Criterion: after the test of brushing teeth, experimenter's gingival hemorrhage reduce or eliminate, the gum redness alleviates or eliminates be effective, otherwise, unchanged or gingival hemorrhage increase and the gum redness add severe one all be considered as invalid.
Check after the experimenter uses seven days, result is as follows:
From experimenter's assay, the toothpaste that contains natural Flos Lonicerae extract essence of the present invention, efficient 84.4% for alleviating the gingival hemorrhage symptom, for alleviating the red and swollen symptom of gum efficient, be 82.2%, all obviously be better than the statistic data of control group.Therefore, the toothpaste that contains natural Flos Lonicerae extract essence of the present invention, all have good prevention and result for the treatment of for gingival hemorrhage, gum redness.
Above content is only that the present invention is conceived to example and explanation; affiliated those skilled in the art make various modifications to described specific embodiment or supplement or adopt similar mode to substitute; only otherwise depart from the design of invention or surmount this scope as defined in the claims, all should belong to protection scope of the present invention.
Claims (10)
1. the preparation method of a natural Flos Lonicerae extract essence, is characterized in that comprising the steps:
1., taking is Japanese Honeysuckle by weight proportion: ethanol: pure water=0.6～1.25: 0.45～0.85: 3.5～4.5 raw material;
2., Japanese Honeysuckle, ethanol, pure water are mixed, be-0.050 in vacuum tightness～-soak 36～48h under the condition of 0.060MPa, reheat decoction 4～5h, filter to get filtrate and filter residue;
3., by filtrate decolouring, and concentrated at 80～120: 1, obtain Flos Lonicerae extract;
4., according to the weight part meter, 10～15 parts of 18～25 parts of Natural menthols, 30～36 parts of Peppermint Oils, 0.8～1.2 part of olium anisi, 0.4～0.6 part of Eugenol, 0.5～1 part of Oleum Menthae Rotundifoliae and Flos Lonicerae extracts are stirred, standing 12～36h, obtain natural Flos Lonicerae extract essence.
2. the preparation method of natural Flos Lonicerae extract essence according to claim 1, is characterized in that, the described step 1. volumn concentration of middle ethanol is 40～75%.
3. the preparation method of natural Flos Lonicerae extract essence according to claim 1, is characterized in that, described step 2. middle decocting time is 4.5h, and decocting temperature is 65～85 ℃.
4. the preparation method of natural Flos Lonicerae extract essence according to claim 1, is characterized in that, described step is concentrated in 3. is to carry out at 100: 1 by volume, and thickening temperature is 70～100 ℃.
5. the preparation method of natural Flos Lonicerae extract essence according to claim 1, is characterized in that, described step 4. middle time of repose is 24h.
6. the natural Flos Lonicerae extract essence prepared as preparation method as described in claim 1～5 any one.
7. one kind contains the toothpaste of natural Flos Lonicerae extract essence as claimed in claim 6, it is characterized in that, contains weight ratio in the lotion of toothpaste total composition and be 1.5～2.5% natural Flos Lonicerae extract essence.
8. the toothpaste that contains natural Flos Lonicerae extract essence according to claim 7, is characterized in that, also comprises following component:
9. the preparation method of toothpaste as claimed in claim 8, is characterized in that, comprises the steps:
A, the lauryl alcohol sodium sulfovinate is dissolved in pure water, forms mixture D 1;
B, Xylo-Mucine is scattered in silicon-dioxide, forms mixture D 2;
C, tertiary sodium phosphate, soluble saccharin, sodium monoflurophosphate and mixture D 1 are mixed, heat 5～10min, form mixture D 3;
D, sorbyl alcohol is mixed with mixture D 2, heat 5～10min, form mixture D 4;
E, mixture D 3, D4 are added in the emulsification pot, add natural Flos Lonicerae extract essence and mix, under vacuum, stir 3～5min, make lotion, be filled into multiple-unit tube.
10. preparation method according to claim 9, is characterized in that, described step c Heating temperature is 50～70 ℃, and the steps d Heating temperature is 60～70 ℃.
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| CN109394650A (en) * | 2018-12-19 | 2019-03-01 | 安徽省旌德博仕达农业科技有限公司 | A kind of rhizoma polygonati toothpaste and preparation method thereof |
| CN111888268A (en) * | 2020-09-18 | 2020-11-06 | 江苏曼威药业有限公司 | Whitening and acid-proof toothpaste composition containing nano-silver and preparation method thereof |
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