CN103404642A - Solid instant tea containing fulvic acid and preparation method for solid instant tea - Google Patents
Solid instant tea containing fulvic acid and preparation method for solid instant tea Download PDFInfo
- Publication number
- CN103404642A CN103404642A CN2013103632422A CN201310363242A CN103404642A CN 103404642 A CN103404642 A CN 103404642A CN 2013103632422 A CN2013103632422 A CN 2013103632422A CN 201310363242 A CN201310363242 A CN 201310363242A CN 103404642 A CN103404642 A CN 103404642A
- Authority
- CN
- China
- Prior art keywords
- tea
- fulvic acid
- instant tea
- solid instant
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- PUKLDDOGISCFCP-JSQCKWNTSA-N 21-Deoxycortisone Chemical compound C1CC2=CC(=O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@@](C(=O)C)(O)[C@@]1(C)CC2=O PUKLDDOGISCFCP-JSQCKWNTSA-N 0.000 title claims abstract description 56
- FCYKAQOGGFGCMD-UHFFFAOYSA-N Fulvic acid Natural products O1C2=CC(O)=C(O)C(C(O)=O)=C2C(=O)C2=C1CC(C)(O)OC2 FCYKAQOGGFGCMD-UHFFFAOYSA-N 0.000 title claims abstract description 56
- 229940095100 fulvic acid Drugs 0.000 title claims abstract description 56
- 239000002509 fulvic acid Substances 0.000 title claims abstract description 56
- 239000007787 solid Substances 0.000 title claims abstract description 47
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 235000020344 instant tea Nutrition 0.000 title abstract description 16
- 230000001954 sterilising effect Effects 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims abstract description 3
- 241001122767 Theaceae Species 0.000 claims abstract 8
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 36
- 239000000706 filtrate Substances 0.000 claims description 20
- 239000005913 Maltodextrin Substances 0.000 claims description 12
- 229920002774 Maltodextrin Polymers 0.000 claims description 12
- 239000004383 Steviol glycoside Substances 0.000 claims description 12
- CEYULKASIQJZGP-UHFFFAOYSA-L disodium;2-(carboxymethyl)-2-hydroxybutanedioate Chemical compound [Na+].[Na+].[O-]C(=O)CC(O)(C(=O)O)CC([O-])=O CEYULKASIQJZGP-UHFFFAOYSA-L 0.000 claims description 12
- 229940116298 l- malic acid Drugs 0.000 claims description 12
- 229940035034 maltodextrin Drugs 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 12
- PPASLZSBLFJQEF-RKJRWTFHSA-M sodium ascorbate Substances [Na+].OC[C@@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RKJRWTFHSA-M 0.000 claims description 12
- 229960005055 sodium ascorbate Drugs 0.000 claims description 12
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims description 12
- 235000019411 steviol glycoside Nutrition 0.000 claims description 12
- 229930182488 steviol glycoside Natural products 0.000 claims description 12
- 150000008144 steviol glycosides Chemical class 0.000 claims description 12
- 235000019202 steviosides Nutrition 0.000 claims description 12
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 10
- 239000008103 glucose Substances 0.000 claims description 10
- 239000000047 product Substances 0.000 claims description 9
- DLRVVLDZNNYCBX-UHFFFAOYSA-N Polydextrose Polymers OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(O)O1 DLRVVLDZNNYCBX-UHFFFAOYSA-N 0.000 claims description 8
- 239000012141 concentrate Substances 0.000 claims description 7
- 235000008504 concentrate Nutrition 0.000 claims description 6
- 235000013399 edible fruits Nutrition 0.000 claims description 6
- 235000003599 food sweetener Nutrition 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 239000003765 sweetening agent Substances 0.000 claims description 6
- 239000006188 syrup Substances 0.000 claims description 6
- 235000020357 syrup Nutrition 0.000 claims description 6
- 229920001100 Polydextrose Polymers 0.000 claims description 4
- 229940035035 polydextrose Drugs 0.000 claims description 4
- 235000013856 polydextrose Nutrition 0.000 claims description 4
- 239000001259 polydextrose Substances 0.000 claims description 4
- -1 L MALIC ACID Chemical compound 0.000 claims description 2
- 235000001727 glucose Nutrition 0.000 claims description 2
- 235000021552 granulated sugar Nutrition 0.000 claims description 2
- 235000013616 tea Nutrition 0.000 abstract description 49
- 239000000796 flavoring agent Substances 0.000 abstract description 5
- 235000019634 flavors Nutrition 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 239000008280 blood Substances 0.000 abstract description 2
- 210000004369 blood Anatomy 0.000 abstract description 2
- 230000036772 blood pressure Effects 0.000 abstract description 2
- 235000009508 confectionery Nutrition 0.000 abstract description 2
- 238000011161 development Methods 0.000 abstract description 2
- 238000001035 drying Methods 0.000 abstract description 2
- 239000003205 fragrance Substances 0.000 abstract description 2
- 230000036039 immunity Effects 0.000 abstract description 2
- 230000007721 medicinal effect Effects 0.000 abstract description 2
- 235000019640 taste Nutrition 0.000 abstract 2
- 206010003210 Arteriosclerosis Diseases 0.000 abstract 1
- 206010028980 Neoplasm Diseases 0.000 abstract 1
- 208000011775 arteriosclerosis disease Diseases 0.000 abstract 1
- 206010012601 diabetes mellitus Diseases 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 230000004089 microcirculation Effects 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 210000000952 spleen Anatomy 0.000 abstract 1
- 210000002784 stomach Anatomy 0.000 abstract 1
- 244000269722 Thea sinensis Species 0.000 description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 235000006468 Thea sinensis Nutrition 0.000 description 7
- 235000020279 black tea Nutrition 0.000 description 6
- 238000009835 boiling Methods 0.000 description 6
- 239000004576 sand Substances 0.000 description 6
- 235000000346 sugar Nutrition 0.000 description 6
- 238000002791 soaking Methods 0.000 description 4
- 208000006820 Arthralgia Diseases 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 229910001385 heavy metal Inorganic materials 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000575 pesticide Substances 0.000 description 3
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 235000013334 alcoholic beverage Nutrition 0.000 description 2
- 230000035622 drinking Effects 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000004108 freeze drying Methods 0.000 description 2
- 235000009569 green tea Nutrition 0.000 description 2
- 239000004021 humic acid Substances 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 244000189799 Asimina triloba Species 0.000 description 1
- 235000006264 Asimina triloba Nutrition 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 206010006956 Calcium deficiency Diseases 0.000 description 1
- 235000019224 Camellia sinensis var Qingmao Nutrition 0.000 description 1
- 235000009467 Carica papaya Nutrition 0.000 description 1
- 235000002722 Dioscorea batatas Nutrition 0.000 description 1
- 235000006536 Dioscorea esculenta Nutrition 0.000 description 1
- 240000001811 Dioscorea oppositifolia Species 0.000 description 1
- 235000003416 Dioscorea oppositifolia Nutrition 0.000 description 1
- 208000018522 Gastrointestinal disease Diseases 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 240000000249 Morus alba Species 0.000 description 1
- 235000008708 Morus alba Nutrition 0.000 description 1
- 206010050031 Muscle strain Diseases 0.000 description 1
- 208000000112 Myalgia Diseases 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 208000001132 Osteoporosis Diseases 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- 206010034464 Periarthritis Diseases 0.000 description 1
- 241000270273 Ptyas dhumnades Species 0.000 description 1
- 208000008765 Sciatica Diseases 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000000767 anti-ulcer Effects 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- IQFVPQOLBLOTPF-HKXUKFGYSA-L congo red Chemical compound [Na+].[Na+].C1=CC=CC2=C(N)C(/N=N/C3=CC=C(C=C3)C3=CC=C(C=C3)/N=N/C3=C(C4=CC=CC=C4C(=C3)S([O-])(=O)=O)N)=CC(S([O-])(=O)=O)=C21 IQFVPQOLBLOTPF-HKXUKFGYSA-L 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 208000010643 digestive system disease Diseases 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 210000003414 extremity Anatomy 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 210000001156 gastric mucosa Anatomy 0.000 description 1
- 208000018685 gastrointestinal system disease Diseases 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 210000000987 immune system Anatomy 0.000 description 1
- 210000003127 knee Anatomy 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000003077 lignite Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 210000004165 myocardium Anatomy 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 235000020333 oolong tea Nutrition 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000036407 pain Effects 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 235000020339 pu-erh tea Nutrition 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000007958 sleep Effects 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 201000005671 spondyloarthropathy Diseases 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 230000035922 thirst Effects 0.000 description 1
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses solid instant tea containing fulvic acid and a preparation method for the solid instant tea. The solid instant tea is prepared by performing digesting, mixing, filtering, concentrating, drying, sterilizing, packaging and the like on the fulvic acid and a tea leaf extracting solution, which serve as main raw materials. According to the solid instant tea containing the fulvic acid, the raw materials are readily available; the preparation method is simple; medicinal effects of the fulvic acid are applied to the solid instant tea; the solid instant tea has unique flavor, tastes sour, sweet, fresh and crisp, has the fragrance of tea and is mellow in taste; furthermore, the solid instant tea also has the health protection functions of reducing the blood pressure and the blood fat, improving the immunity of human body, adjusting the spleen and the stomach of human body, resisting cancers, resisting arteriosclerosis, preventing and treating diabetes, improving microcirculation and the like, can be taken for a long time without any side effect and has an extremely good market development prospect.
Description
Technical field
The present invention relates to a kind of instant solid tea that contains fulvic acid and preparation method thereof, belong to food processing field.
Background technology
Instant tea is a kind of brewed simple and convenient, very soluble Powdered tea, its bath is instant, there is no recrement, especially hardly the harmful heavy metal and pesticide remnant of mercurous, a plumbous class, therefore instant tea take again " pure " be its characteristic, won consumers in general's trust, the overall merit that instant tea has concurrently is lightweight, volume is little, packing is skilful, freight charges are economized, development prospect is fine.
Fulvic acid is that in humic acid, molecular weight is minimum, solubility is the highest, also the strongest part of biologically active, contain active function groups many, utilization easily is absorbed by the body, in recent years, many reports affirmed fulvic acid and sodium salt thereof sobering up, hypoglycemic, anti-inflammatory, antiviral, the remarkable result of regulating the aspects such as immune system, antibiotic, antiulcer, show that it has broad application prospects in fields such as medicine, functional foods, fulvic acid is a kind of natural products, through pharmacological evaluation, prove, without any side effects to human body.
The application of fulvic acid at present; mostly concentrate on agricultural and medical aspect; in the research of field of food seldom; as mono-kind of Chinese invention patent CN101265445A, contain assembled alcoholic drinks of fulvic acid and preparation method thereof; the fulvic acid that comprises 0.05%-0.3% in assembled alcoholic drinks; in view of the biologically active of fulvic acid protection gastric mucosa, the health-care effect of outstanding wine.
The instant tea that the fulvic acid of also not take on present market is made as primary raw material, the medical effect of fulvic acid is fully applied, and the patent of instant tea is a lot, quite a few for the instant tea of health protection and therapeutic action, basically adds Chinese herbal medicine and achieves the goal; Bone instant tea as strong as Six-element, formula is lotus seeds, Chinese yam, zaocys dhumnade, pawpaw, mulberry leaf, calcium carbonate, green tea, be applicable to the elderly because of wind, osteoporosis, soreness and weakness of waist and knees, wind-cold-dampness arthralgia, arthralgia and myalgia, the scapulohumeral periarthritis that cold, wet or calcium deficiency causes, cervical spondylopathy, lumbar muscle strain, the multiple pains such as sciatica, the protrasion of the lumbar intervertebral disci, back extremities joint pain, but there is complicated components in Chinese medicine, the unstable shortcoming of quality.
Summary of the invention
The object of the present invention is to provide a kind of instant solid tea that contains fulvic acid, this component and percentage by weight thereof that contains the instant solid tea of fulvic acid is: fulvic acid 0.5~5.0%, tea extract 70.0~90.0%, citric acid 0.1~1%, L MALIC ACID 0.3~1.6%, natrium citricum 0.5~2.3%, steviol glycoside 0.05~1.0%, D-sodium ascorbate 1.0~5.0%, sweetener 6.0~15.0%, maltodextrin 0.1~6.0%, calgon 1.0~2.0%, described percentage by weight all be take the instant solid tea gross weight that contains fulvic acid and is benchmark, and the percentage by weight sum of all raw materials is 100%.
Described sweetener is the mixture after one or both materials in white granulated sugar, glucose, fruit glucose syrup, polydextrose are mixed by any ratio.
Another object of the present invention is to provide a kind of preparation method who contains the instant solid tea of fulvic acid, concrete steps are as follows:
(1) after in proportion fulvic acid, tea extract being mixed, be heated to fulvic acid and dissolve fully, filter, obtain filtrate A;
(2) in proportion citric acid, L MALIC ACID, natrium citricum, steviol glycoside, D-sodium ascorbate, maltodextrin, calgon, sweetener are mixed, then slowly add in filtrate A, the limit edged stirs, until fully dissolve, filters, and obtains liquor B;
(3) by liquor B at normal temperatures, with the speed of 5000~8000r/min, centrifugal 10~30min, filter, and obtains liquor C;
(4) mass percentage content that liquor C is concentrated into to solid content under vacuum is 10%~50%;
(5) by the concentrate drying obtained in step (4), cross 60~300 purpose sieves, at the temperature of 65~121 ℃, sterilization 10~30min makes finished product.
Tea extract of the present invention lixiviate or ultrasonic-leaching according to a conventional method prepares.
Fulvic acid in the inventive method is that pharmaceutical grade fulvic acid or the fulvic acid that makes with reference to method in patent application 200810233669.X " oxidation and degradation of brown coal is produced the method for humic acid and salt thereof " are (with free of contamination hydrogen peroxide as oxidant, and through purifying, make fulvic acid), commercial refining fulvic acid, after the heavy metal detection does not exceed standard, also can be used.
The present invention contains fulvic acid instant solid tea quality standard:
1, product specification of the present invention: every pouch 1.5g, 20 little packed boxes, pour 1 pouch in cup into while drinking, and brews 3 minutes with the 200ml boiling water, and the active ingredient stripping is namely drinkable;
2, subjective appreciation of the present invention: get 1.5g instant solid tea, brew 3 minutes with the 200ml boiling water, can dissolve fast, standing two minutes, cup end free from admixture, the soup look limpid is bright, and fragrance is pure, have the sweet-smelling of tea and distinctive flavour, smell, free from extraneous odour, mouthfeel is pure;
3, product physical and chemical index testing result of the present invention: soluble property: brew instant, the clarification, do not stay recrement: moisture content≤6%, ash≤12%, Tea Polyphenols >=10%, heavy metal meet the GB11671 requirement;
4, product sanitary index testing result of the present invention: total number of bacteria (CFU/g)≤1000, coliform (MPN/100g)≤30, pathogenic bacteria do not detect, and the Pesticide MRL meets GB 2763 requirements.
Beneficial effect of the present invention:
(1) the instant solid tea that contains fulvic acid of the present invention can increase body immunity, increases the Nutritional myocardium blood flow amount, control gastrointestinal disease, hypertension, antitumor, alleviating physical fatigue, reduce blood pressure and blood lipoid, improve appetite and sleep, and long-term drinking, have no side effect;
(2) the instant solid tea preparation method that contains fulvic acid of the present invention is simple, and cost is low, and quality is easily controlled, and makes fulvic acid that new application arranged aspect food;
(3) the instant solid tea that contains fulvic acid of the present invention is lightweight, volume is little, Instant Drinks are easy to carry, does not contain residues of pesticides, integrates tasty and refreshing and quenches one's thirst, health care.
(4) the instant solid tea flavour sense that contains fulvic acid of the present invention is coordinated, sour and sweet palatability, and exquisiteness, flavour is soft, unique flavor, clear, good stability.
The specific embodiment
Below in conjunction with embodiment, the present invention is described in further detail, but protection scope of the present invention is not limited to described content.
Embodiment 1
Component and the percentage by weight of the instant solid black tea of the present embodiment are: fulvic acid 0.95%, black tea extract 90.0%, citric acid 0.1%, L MALIC ACID 0.3%, natrium citricum 0.5%, steviol glycoside 0.05%, D-sodium ascorbate 1.0%, white sand Icing Sugar 6.0%, maltodextrin 0.1%, calgon 1.0%, the percentage by weight sum of all components is 100%.
The preparation method of the described instant solid black tea of the present embodiment is as follows:
(1) take and be milled to 30 purpose black tea 100g, add 1000g water soaking 20min, put into the ultrasonic 15min of ultrasonic wave, then be heated to 50 ℃ of lixiviate 20min, filter cleaner obtains the black tea extract;
(2) take in the black tea extract that the 9.5g fulvic acid joins 900g, heat 10min in the double boiler of 60 ℃, be stirred well to fulvic acid and dissolve fully, A filters to get filtrate;
(3) take citric acid 1.0g, L MALIC ACID 3.0g, natrium citricum 5.0g, steviol glycoside 0.5g, D-sodium ascorbate 10.0g, white sand Icing Sugar 60.0g, maltodextrin 1.0g, calgon 10.0, after being mixed, it slowly adds in filtrate A, the limit edged stirs, until mixture fully dissolves, B filters to get filtrate;
(4) by liquor B at normal temperatures, with 5000r/min, centrifugal 30min, C filters to get filtrate;
(5) liquor C being concentrated into to the solid content percentage composition under vacuum is 10%;
(6) concentrate is placed in to-60 ℃ of ultra low temperature freezer quick-frozens, then is placed on freeze-drying in vacuum freeze drier, make pulvis, cross 80 mesh sieves after pulvis is pulverized, sterilizing 30min under 65 ℃ of conditions, encapsulate to obtain finished product.
Get 1.5g instant solid tea, brew 3 minutes with the 200ml boiling water, namely drinkable.
Table 1. contains fulvic acid instant solid congo red subjective appreciation
Embodiment 2:
Component and the percentage by weight of the instant solid West Lake Dragon Well tea of the present embodiment are: fulvic acid 5.0%, Xihu Longjing Tea tea extract 76.0%, citric acid 1.0%, L MALIC ACID 1.6%, natrium citricum 2.3%, steviol glycoside 1.0%, D-sodium ascorbate 1.5%, white sand Icing Sugar 1.5%, glucose 8.0%, maltodextrin 0.5%, calgon 1.6%, the percentage by weight sum of all components is 100%.
The preparation method of the described instant solid West Lake Dragon Well tea of the present embodiment is as follows:
(1) take and be milled to 40 purpose West Lake Dragon Well tea 90g, add 1000g water soaking 20min, put into the ultrasonic 15min of ultrasonic wave, then be heated to 50 ℃ of lixiviate 20min, filter cleaner obtains the Xihu Longjing Tea tea extract;
(2) take in the Xihu Longjing Tea tea extract that the 50g fulvic acid joins 760g, heat 10min in the double boiler of 70 ℃, be stirred well to fulvic acid and dissolve fully, A filters to get filtrate;
(3) take citric acid 10.0g, L MALIC ACID 16.0g, natrium citricum 23.0g, steviol glycoside 10.0g, D-sodium ascorbate 15.0g, white sand Icing Sugar 15.0g, maltodextrin 5.0g, calgon 16.0 g, glucose 80.0g, after being mixed, it slowly adds in filtrate A, the limit edged stirs, until mixture fully dissolves, B filters to get filtrate;
(4) by liquor B at normal temperatures, with 6000r/min, centrifugal 20min, C filters to get filtrate;
(5) liquor C being concentrated into to the solid content percentage composition under vacuum is 20%;
(6) concentrate is placed in to-70 ℃ of ultra low temperature freezer quick-frozens, then is placed on freeze-drying in vacuum freeze drier, make pulvis, pulvis was pulverized to 80 mesh sieves, sterilizing at 105 ℃ of lower 15min, encapsulate to obtain finished product.
Get 1.5g instant solid tea, brew 3 minutes with the 200ml boiling water, namely drinkable.
Table 2. contains fulvic acid instant solid green tea subjective appreciation
Embodiment 3:
Component and the percentage by weight of the instant solid Anxi Tieguanyin Tea tea of this enforcement are: fulvic acid 1.2%, Anxi Tieguanyin Tea tea extract 80.0%, citric acid 0.5%, L MALIC ACID 0.2%, natrium citricum 0.6%, steviol glycoside 0.5%, D-sodium ascorbate 0.6%, fruit glucose syrup 15%, maltodextrin 1.0%, calgon 0.4%, the percentage by weight sum of all components is 100%.
The preparation method of the described instant solid Anxi Tieguanyin Tea of the present embodiment tea is as follows:
(1) take and be milled to 30 purpose Anxi Tieguanyin Tea 90g, add 1000g water soaking 20min, put into the ultrasonic 15min of ultrasonic wave, then be heated to 55 ℃ of lixiviate 30min, filter cleaner obtains the Anxi Tieguanyin Tea tea extract;
(2) take in the Anxi Tieguanyin Tea tea extract that the 12g fulvic acid joins 800 g, heat 8min in the double boiler of 80 ℃, be stirred well to fulvic acid and dissolve fully, A filters to get filtrate;
(3) take citric acid 5.0g, L MALIC ACID 2.0g, natrium citricum 6.0g, steviol glycoside 5.0g, D-sodium ascorbate 6.0g, fruit glucose syrup 150.0g, maltodextrin 10.0g, calgon 4.0g mixing, after being mixed, it slowly adds in filtrate A, the limit edged stirs, until mixture fully dissolves, B filters to get filtrate;
(4) by liquor B at normal temperatures, with 7000r/min, centrifugal 15min, C filters to get filtrate;
(5) liquor C being concentrated into to the solid content percentage composition under vacuum is 40%;
(6) concentrate after concentrating, EAT is 120 ℃, leaving air temp is spray-drying under 100 ℃ of conditions, makes pulvis, crosses 80 mesh sieves after pulvis is pulverized, sterilizing at 75 ℃ of lower 30min, encapsulates to obtain finished product.
Get 1.5g instant solid tea, brew 3 minutes with the 200ml boiling water, namely drinkable.
Table 3. contains fulvic acid instant solid oolong tea subjective appreciation
Embodiment 4
Component and the percentage by weight of the instant solid yunnan puer tea of the present embodiment are: fulvic acid 2.0%, yunnan puer tea extract 70.0%, citric acid 0.8%, L MALIC ACID 1.0%, natrium citricum 1.8%, steviol glycoside 0.8%, D-sodium ascorbate 5%, white sand Icing Sugar 5%, polydextrose 4.5%, fruit glucose syrup 1.1%, maltodextrin 6.0%, calgon 2.0%, the percentage by weight sum of all components is 100%.
The preparation method of the described instant solid yunnan puer tea of the present embodiment is as follows:
(1) take and be milled to 20 purpose yunnan puer tea 90g, add 1000g water soaking 20min, put into the ultrasonic 15min of ultrasonic wave, then be heated to 70 ℃ of lixiviate 20min, filter cleaner obtains the yunnan puer tea extract;
(2) take in the yunnan puer tea tea extract that the 20g fulvic acid joins 700g, heat 8min in the double boiler of 80 ℃, be stirred well to fulvic acid and dissolve fully, A filters to get filtrate;
(3) take citric acid 8.0g, L MALIC ACID 10.0g, natrium citricum 18.0g, steviol glycoside 8.0g, D-sodium ascorbate 50.0g, white sand Icing Sugar 50g, maltodextrin 60.0g, calgon 20.0g, polydextrose 45g, fruit glucose syrup 11g, after being mixed, it slowly adds in filtrate A, the limit edged stirs, until mixture dissolves fully, B filters to get filtrate;
(4) by liquor B at normal temperatures, with 8000r/min, centrifugal 10min, C filters to get filtrate;
(5) liquor C being concentrated into to the solid content percentage composition under vacuum is 50%;
(6) concentrate after concentrating, EAT is 120 ℃, leaving air temp is spray-drying under 100 ℃ of conditions, makes pulvis, crosses 80 mesh sieves after pulvis is pulverized, sterilizing at 75 ℃ of lower 30min, encapsulates to obtain finished product.
Get 1.5g instant solid tea, brew 3 minutes with the 200ml boiling water, namely drinkable.
Table 4. contains fulvic acid instant solid Pu'er tea subjective appreciation
Claims (3)
1. instant solid tea that contains fulvic acid, it is characterized in that: the component of this instant solid tea and percentage by weight thereof are: fulvic acid 0.5~5.0%, tea extract 70.0~90.0%, citric acid 0.1~1.0%, L MALIC ACID 0.3~1.6%, natrium citricum 0.5~2.3%, steviol glycoside 0.05~1.0%, D-sodium ascorbate 1.0~5.0%, sweetener 6.0~15.0%, maltodextrin 0.1~6.0%, calgon 1.0~2.0%, the percentage by weight sum of all components is 100%.
2. the instant solid tea that contains fulvic acid according to claim 1, is characterized in that sweetener is one or both in white granulated sugar, glucose, fruit glucose syrup, polydextrose.
3. the preparation method who contains the instant solid tea of fulvic acid claimed in claim 1 is characterized in that carrying out according to the following steps:
(1) in proportion fulvic acid, tea extract are heated to fulvic acid after mixing and dissolve fully, filter, obtain filtrate A;
(2) in proportion citric acid, L MALIC ACID, natrium citricum, steviol glycoside, D-sodium ascorbate, maltodextrin, calgon, sweetener are mixed to get to mixture, then mixture is added in filtrate A, the limit edged stirs, until mixture fully dissolves, filter, obtain liquor B;
(3) at normal temperatures, by the speed of liquor B with 5000~8000r/min, centrifugal 10~30min, filter, and obtains liquor C;
(4) mass percentage content that liquor C is concentrated into to solid content is 10%~50%;
(5) concentrate that obtains in step (4) is dry, sieve, namely obtain finished product after sterilizing.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310363242.2A CN103404642B (en) | 2013-08-20 | 2013-08-20 | A kind of instant solid tea containing fulvic acid and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310363242.2A CN103404642B (en) | 2013-08-20 | 2013-08-20 | A kind of instant solid tea containing fulvic acid and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103404642A true CN103404642A (en) | 2013-11-27 |
CN103404642B CN103404642B (en) | 2015-11-04 |
Family
ID=49597732
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310363242.2A Expired - Fee Related CN103404642B (en) | 2013-08-20 | 2013-08-20 | A kind of instant solid tea containing fulvic acid and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103404642B (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104546910A (en) * | 2014-12-18 | 2015-04-29 | 昆明理工大学 | Application of fulvic acid in preparing appetite improving and digestion promoting oral preparation |
CN106172954A (en) * | 2016-08-10 | 2016-12-07 | 昆明理工大学 | Fulvic acid application in Pu-erh tea fermentation |
CN109287808A (en) * | 2018-10-26 | 2019-02-01 | 昆明理工大学 | A kind of boat leaf Farfugium kaemferi health protection tea and preparation method thereof |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1313042A (en) * | 2000-03-15 | 2001-09-19 | 付立春 | Process for preparing instant beverage of powdered food |
CN1568827A (en) * | 2003-07-16 | 2005-01-26 | 刘南凯 | Humic acid healthy drink and application of humic acid to drink |
CN101721425A (en) * | 2009-12-02 | 2010-06-09 | 昆明理工大学 | Fulvic acid health-care product with sober-up and anti-drunk function |
CN102669336A (en) * | 2012-05-31 | 2012-09-19 | 上海海洋大学 | Preparation method of liquorice, flower and green tea solid drink |
CN103098923A (en) * | 2011-11-11 | 2013-05-15 | 周祯璇 | Instant tea beverage |
-
2013
- 2013-08-20 CN CN201310363242.2A patent/CN103404642B/en not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1313042A (en) * | 2000-03-15 | 2001-09-19 | 付立春 | Process for preparing instant beverage of powdered food |
CN1568827A (en) * | 2003-07-16 | 2005-01-26 | 刘南凯 | Humic acid healthy drink and application of humic acid to drink |
CN101721425A (en) * | 2009-12-02 | 2010-06-09 | 昆明理工大学 | Fulvic acid health-care product with sober-up and anti-drunk function |
CN103098923A (en) * | 2011-11-11 | 2013-05-15 | 周祯璇 | Instant tea beverage |
CN102669336A (en) * | 2012-05-31 | 2012-09-19 | 上海海洋大学 | Preparation method of liquorice, flower and green tea solid drink |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104546910A (en) * | 2014-12-18 | 2015-04-29 | 昆明理工大学 | Application of fulvic acid in preparing appetite improving and digestion promoting oral preparation |
CN106172954A (en) * | 2016-08-10 | 2016-12-07 | 昆明理工大学 | Fulvic acid application in Pu-erh tea fermentation |
CN106172954B (en) * | 2016-08-10 | 2019-09-27 | 昆明理工大学 | Application of the fulvic acid in Pu-erh tea fermentation |
CN109287808A (en) * | 2018-10-26 | 2019-02-01 | 昆明理工大学 | A kind of boat leaf Farfugium kaemferi health protection tea and preparation method thereof |
Also Published As
Publication number | Publication date |
---|---|
CN103404642B (en) | 2015-11-04 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
WO2018058851A1 (en) | Siraitia grosvenorii-prebiotics-chrysanthemum instant tea beverage and preparation method therefor | |
CN103750491B (en) | The Japanese Premna jelly health beverages that a kind of fast and easy is edible | |
CN105996045A (en) | Method for preparing self-made flavored health-caring brown sugar | |
CN103271190B (en) | Chrysanthemum tea granule with matcha flavor, and preparation method of same | |
CN104095090A (en) | Barley health care tea with overflowing fragrance and preparation method thereof | |
CN103404642B (en) | A kind of instant solid tea containing fulvic acid and preparation method thereof | |
CN106070813A (en) | Green tea powder nourishing medicinal granule | |
CN109430612A (en) | A kind of date-wolfberry fruit juice and its production method | |
CN107712520A (en) | A kind of penthorum chinense pursh beverage and preparation method thereof | |
CN105831545B (en) | A kind of processing method of instant plant gel food | |
KR20110056908A (en) | Composition of mixed herb medicine for leached tea | |
CN103749827A (en) | Preparation method of red ginseng/fig tea | |
CN109123015A (en) | A kind of Hubei Chinese flowering crabapple herbal tea and preparation method thereof | |
CN108936183A (en) | A kind of compound endothelium corneum gigeriae galli solid beverage | |
CN101366907A (en) | Lily green tea beauty treatment weight reducing particle | |
CN104082695A (en) | Herbal tea lotus root starch and preparation method thereof | |
CN107467287A (en) | A kind of tea for reducing hypertension and fat | |
CN106689589A (en) | Okra conditioning health tea and preparation method thereof | |
CN105832891A (en) | Injection for treating mastitis of female minks and preparation method of injection | |
CN105166902A (en) | Preparation method of quick-dissolving type okra submicron powder and quick-dissolving type okra submicron powder prepared through preparation method | |
CN111838499A (en) | Health-preserving solid beverage for adjusting human immunity and preparation method thereof | |
CN100551249C (en) | Sour and hot tea and preparation method thereof | |
CN109479974A (en) | A kind of preparation method of low sugar health care milk tea | |
CN103610050A (en) | Russule-containing nutritional cream and production method thereof | |
CN104642576A (en) | Preparation method of concentrated health-care health-preserving tea product |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151104 Termination date: 20210820 |
|
CF01 | Termination of patent right due to non-payment of annual fee |