CN103386286B - Recyclable reaction vessel system - Google Patents
Recyclable reaction vessel system Download PDFInfo
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- CN103386286B CN103386286B CN201310276264.5A CN201310276264A CN103386286B CN 103386286 B CN103386286 B CN 103386286B CN 201310276264 A CN201310276264 A CN 201310276264A CN 103386286 B CN103386286 B CN 103386286B
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Abstract
The invention belongs to the field of industrial chemical production equipment, and specifically relates to a reaction-vessel condensation-reaction circulation system used in industrial chemical production reactions. The recyclable reaction vessel system comprises a reaction vessel and a condensation circulation apparatus connected with the reaction vessel, and the condensation circulation apparatus comprises a buffer tank and a condensation glass tank which are both connected with the reaction vessel and are connected with each other. The recyclable reaction vessel system of the invention helps to realize that a gaseous material in the reaction vessel enters into the buffer tank, successively enters into the condensation glass tank from the buffer tank, and is liquefied in the condensation glass tank or reflows into the reaction vessel for a reaction, and helps to realize circulation of forward flow, condensation and backflow of the material in the circulation reaction vessel system.
Description
Technical field
The invention belongs to industrial chemical production equipment field, relate to the reactor condensation reaction circulatory system used in the reaction of a kind of Chemical Manufacture in particular.
Technical background
In the reactor of Chemical Manufacture, frequent needs by reaction or gaseous feed reacting through reactor after condensation liquefaction, in the prior art, this kind of reaction cycle device all can not well by gas liquefaction, well can not realize circulation, the cleaning of condenser and the recovery of waste material can not be realized.
Summary of the invention
The technical problem to be solved in the present invention be to provide a kind of can realization response gaseous liquefied a kind of reactor system of reflux cycle reaction.
For solving the problems of the technologies described above, the invention provides a kind of reactor system capable of circulation, the condensation circulating device comprising reactor and be connected with reactor, condensation circulating device comprises the surge tank and anti-condensation glass tank that are connected with reactor, is connected between surge tank with anti-condensation glass tank.
Preferably, surge tank position is higher than anti-condensation glass tank, and anti-condensation glass tank position is higher than reactor.
Preferably, pump is provided with between reactor and surge tank.
Preferably, surge tank top is connected with anti-condensation glass tank top by pipeline one.
Preferably, pipeline one sets up pipeline two separately, pipeline two is connected with return water pipe.
Preferably, anti-condensation glass pot bottom is connected with reactor top by glass tube one.
Preferably, glass tube one sets up glass tube two separately, glass tube two is connected with return water pipe.
Preferably, anti-condensation glass pot bottom is also provided with the pipeline three be connected with air duct.
The beneficial effect of employing technique scheme is: a kind of reactor system capable of circulation, the condensation circulating device comprising reactor and be connected with reactor, condensation circulating device comprises the surge tank and anti-condensation glass tank that are connected with reactor, be connected between surge tank with anti-condensation glass tank, adopt this connected mode, surge tank can be entered by gaseous material in realization response still, anti-condensation glass tank is being entered into from surge tank, carry out liquefying in anti-condensation glass tank or being back in reactor, react, realize the just stream of material in circular response still system, the circulation of condensation and backflow, surge tank position is higher than anti-condensation glass tank, anti-condensation glass tank position is higher than reactor, by reactor, surge tank and anti-condensation glass tank adopt the installation of this position relationship, be convenient to the circulation of material, pump is provided with between reactor and surge tank, utilize pump that the Gaseous materials in reactor is pumped into surge tank, surge tank top is connected with anti-condensation glass tank top by pipeline one, the material of gaseous state is entered from anti-condensation glass tank top, make that there is enough cooling liquid processes, gas material can fully be liquefied, pipeline one sets up pipeline two separately, described pipeline two is connected with return water pipe, be convenient to the waste water of the steam liquefied reclaimed in anti-condensation glass tank, anti-condensation glass pot bottom is connected with reactor top by glass tube one, adopt glass tube one, glass main component is quartz, comparatively stable, be not easy to the material reaction of post liquefaction, glass tube one sets up glass tube two separately, described glass tube two is connected with return water pipe, be convenient to the waste water reclaiming post liquefaction, anti-condensation glass pot bottom is also provided with the pipeline three be connected with air duct, the pressure balance inside and outside anti-condensation glass tank can be ensured after whole system is quit work.
Accompanying drawing explanation
Fig. 1 is the structural representation of a kind of reactor system capable of circulation of the present invention,
Wherein, 1, reactor, 2, glass tube two, 3, return water pipe, 4, pump, 5, pipeline two, 6, pipeline one, 7, surge tank, 9, anti-condensation glass tank, 10, pipeline three, 11, air duct, 12, glass tube one.
Detailed description of the invention
Below in conjunction with Figure of description, technical scheme of the present invention and structure are described, so that those skilled in the art understand.
As shown in Figure 1, a kind of reactor system capable of circulation, the condensation circulating device comprising reactor 1 and be connected with reactor 1, condensation circulating device comprises the surge tank 7 and anti-condensation glass tank 9 that are connected with reactor 1, be connected between surge tank 7 with anti-condensation glass tank 9, surge tank 7 position is higher than anti-condensation glass tank 9, anti-condensation glass tank 9 position is higher than reactor 1, pump 4 is provided with between reactor 1 and surge tank 7, surge tank 7 top is connected with anti-condensation glass tank 9 top by pipeline 1, pipeline 1 sets up pipeline 25 separately, pipeline 25 is connected with return water pipe 3, be connected with reactor 1 top by glass tube 1 bottom anti-condensation glass tank 9, glass tube 1 sets up glass tube 22 separately, glass tube 22 is connected with return water pipe 3, the pipeline 3 10 be connected with air duct 11 is also provided with bottom anti-condensation glass tank 9.
The beneficial effect of employing technique scheme is: a kind of reactor system capable of circulation, the condensation circulating device comprising reactor and be connected with reactor, condensation circulating device comprises the surge tank and anti-condensation glass tank that are connected with reactor, be connected between surge tank with anti-condensation glass tank, adopt this connected mode, surge tank can be entered by gaseous material in realization response still, anti-condensation glass tank is being entered into from surge tank, carry out liquefying in anti-condensation glass tank or being back in reactor, react, realize the just stream of material in circular response still system, the circulation of condensation and backflow, surge tank position is higher than anti-condensation glass tank, anti-condensation glass tank position is higher than reactor, by reactor, surge tank and anti-condensation glass tank adopt the installation of this position relationship, be convenient to the circulation of material, pump is provided with between reactor and surge tank, utilize pump that the Gaseous materials in reactor is pumped into surge tank, surge tank top is connected with anti-condensation glass tank top by pipeline one, the material of gaseous state is entered from anti-condensation glass tank top, make that there is enough cooling liquid processes, gas material can fully be liquefied, pipeline one sets up pipeline two separately, described pipeline two is connected with return water pipe, be convenient to the waste water of the steam liquefied reclaimed in anti-condensation glass tank, anti-condensation glass pot bottom is connected with reactor top by glass tube one, adopt glass tube one, glass main component is quartz, comparatively stable, be not easy to the material reaction of post liquefaction, glass tube one sets up glass tube two separately, described glass tube two is connected with return water pipe, be convenient to the waste water reclaiming post liquefaction, anti-condensation glass pot bottom is also provided with the pipeline three be connected with air duct, the pressure balance inside and outside anti-condensation glass tank can be ensured after whole system is quit work.
Adopt the reactor system a kind of capable of circulation of technical solution of the present invention, surge tank can be entered by gaseous material in realization response still, anti-condensation glass tank is being entered into from surge tank, carry out liquefying in anti-condensation glass tank or being back in reactor, react, realize the circulation of just the flowing of material in circular response still system, condensation and backflow.
Above-mentionedly by reference to the accompanying drawings invention to be exemplarily described; obvious specific implementation of the present invention is not subject to the restrictions described above; as long as have employed this insubstantial that method of the present invention is conceived and technical scheme is carried out to improve; or the design of invention and technical scheme directly applied to other occasions, all within protection scope of the present invention without to improve.
Claims (3)
1. a reactor system capable of circulation, the condensation circulating device comprising reactor and be connected with reactor, is characterized in that: described condensation circulating device comprises the surge tank and anti-condensation glass tank that are connected with reactor, is connected between described surge tank with anti-condensation glass tank;
Described surge tank position is higher than anti-condensation glass tank, and described anti-condensation glass tank position is higher than reactor;
Described surge tank top is connected with anti-condensation glass tank top by pipeline one;
Described pipeline one sets up pipeline two separately, and described pipeline two is connected with return water pipe;
Described anti-condensation glass pot bottom is connected with reactor top by glass tube one;
Described glass tube one sets up glass tube two separately, and described glass tube two is connected with return water pipe.
2. a kind of reactor system capable of circulation according to claim 1, is characterized in that: be provided with pump between described reactor and surge tank.
3. a kind of reactor system capable of circulation according to claim 1, is characterized in that: described anti-condensation glass pot bottom is also provided with the pipeline three be connected with air duct.
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CN201310276264.5A CN103386286B (en) | 2013-07-01 | 2013-07-01 | Recyclable reaction vessel system |
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CN201310276264.5A CN103386286B (en) | 2013-07-01 | 2013-07-01 | Recyclable reaction vessel system |
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CN103386286B true CN103386286B (en) | 2015-04-01 |
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CN106552554A (en) * | 2015-09-30 | 2017-04-05 | 江苏创新石化有限公司 | A kind of amine liquid recovery system of compounding neutralization corrosion inhibiter |
CN110818579B (en) * | 2018-08-08 | 2022-09-16 | 青岛海湾精细化工有限公司 | Cooling crystallization method and device for N-acetoacetanilide compound |
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CN201610417U (en) * | 2009-12-25 | 2010-10-20 | 潍坊中业油脂有限公司 | Chlorination reaction device for chloroactic acid production |
CN102489233A (en) * | 2011-12-16 | 2012-06-13 | 中国石油化工股份有限公司 | Novel production equipment of propionic acid peroxide as well as safety protection method and application thereof |
CN202398358U (en) * | 2011-12-20 | 2012-08-29 | 迈克斯(如东)化工有限公司 | Terbacil material punching prevention system |
CN203525678U (en) * | 2013-07-01 | 2014-04-09 | 安徽省旌德县天益医药化工厂 | Circulatory reaction kettle system |
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Effective date of registration: 20180611 Address after: 043100 Shanxi Xinjiang County Coal Chemical Industrial Park, Yuncheng (Shanxi Heng Qiang Chemical Co., Ltd.) Patentee after: Shanxi Kai Li Fine Chemicals Technology Co., Ltd. Address before: 242000 Guanyin Pavilion, Jingyang Town, Jingde County, Xuancheng, Anhui, China Patentee before: Anhui Province Shengde County Tianyi Pharmaceutical Chemical Factory |
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