CN103349632A - Preparation process of fragrance beads - Google Patents
Preparation process of fragrance beads Download PDFInfo
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- CN103349632A CN103349632A CN2013102547973A CN201310254797A CN103349632A CN 103349632 A CN103349632 A CN 103349632A CN 2013102547973 A CN2013102547973 A CN 2013102547973A CN 201310254797 A CN201310254797 A CN 201310254797A CN 103349632 A CN103349632 A CN 103349632A
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- fragrance
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- perfume
- gelatin
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Abstract
The invention provides a preparation process of fragrance beads. The preparation process comprises the following steps of: adding 8-10% of gelatin, 4-7% of glycerol, 0.5-1.0% of polyethylene glycol 400 and 0.5-1.5% of sorbitol into a glue-melting tank, then putting in 1.5-2 times the amount of the gelatin of water, performing cold soaking for 30min, gradually heating to 75 DEG C, performing heat preservation, stirring for 5h, performing vacuum degassing, filtering, loading into a glue material barrel of a capsule machine, and performing heat preservation at 65 DEG C for later use; and loading fragrance components into a medical material barrel for capsules, adjusting the loading quantity, pressing pills and drying to obtain the fragrance beads. The preparation process provided by the invention adopts a preparation method of the soft capsules to prepare the fragrance beads, and the obtained fragrance beads have the advantages of sparkling and clear appearance and lasting fragrance diffusion. In addition, the fragrance beads can be directly bottled and boxed for placing in indoor spaces of automobiles, families, guest houses and the like; and a certain proportion of water and perfume solvent can also be added into a bottle for slow release and spraying on human bodies, and the fragrance is lasting. The preparation process has the advantages of economy, practicality and wide range of application.
Description
Technical field
The present invention relates to a kind of perfume technique, relate in particular to the preparation technology of a kind of perfume pearl.
Background technology
Along with improving constantly of living standard, people are also more and more exquisite to the living space quality, improve surrounding air environment and taked a lot of methods and measure, for example people put the spice Fragrant box in the room, vehicle-used perfume etc., the effect of perfume does not act on merely human body yet, with it being sprayed on, also can be used for various public places and improve air quality, general perfume major part is liquid, and standing time, slightly length will be apt to deteriorate, and then affect ambient air quality, if employing solid perfume not only can be easy to use, and standing time is long, is not easy to go bad.For the scope of application that makes perfume is more and more wider, numerous scientific research personnel are also constantly exploring and research.
200610035798.9 the manufacture method of perfume cards, the directly method of screen printed pattern in absorbent paper has been adopted in this invention, directly perfume is added in the absorbent paper, perfume can be diffused into rapidly in the whole absorbent paper, make absorbent paper improve the effect of air quality, although the method process is simple, perfume component volatilization more, the perfume taste is not lasting, and sphere of action can only be used for site surrounding.
Summary of the invention
Be more sufficient above-mentioned deficiency, the invention provides the perfume pearl preparation method that a kind of technique is simple, easy to use, fragrance is lasting, the perfume pearl of the method preparation can not only directly be put in public environment, discharge fragrance, and can be dissolved in the perfume solvent, be sprayed on health, the pleasant aroma, lasting is lasting.
The process of preparing of a kind of perfume pearl is,
1) changes adding 8-10%1 gelatin in the glue tank, 4-7% glycerol, the 0.5-1.0% PEG400, then the 0.5-1.5% sorbitol drops into the water of 1.5～2 times of gelatin amounts, is warming up to gradually 75 ℃ behind the merceration 30min, insulated and stirred 5h vacuum outgas, filtration incapsulates in the machine sizing material bucket, is incubated 65 ℃, and is for subsequent use.
2) perfume composition is incapsulated in the spice bucket of agent, adjust loading amount, pelleting is drying to obtain the perfume pearl.
Wherein in the pellet press, 50～52 ℃ of gelatin box temperature controls, mould rotating speed 3.2 r/min are rolled in 42～45 ℃ of sprinkler body temperature controls, rubber thickness 0.75～0.8 mm.Indoor temperature is 18～25 ℃ simultaneously, relative humidity＜40%.The sphere diameter of perfume pearl is 1～2cm approximately.
Perfume composition of the present invention can be single fragrance component, also can be the spice blending ingredients.
The present invention selects soft capsule component, gelatin: glycerol: PEG400: the sorbitol mass ratio is 10:4:0.5:1.5.
The present invention adopts the method for preparing soft capsule to prepare the perfume pearl, and not only outward appearance is glittering and translucent for the perfume pearl that obtains, and fragrance emission is lasting.In addition, the mounted box of not only can directly bottling is put into the interior spaces such as automobile, family, hotel and is put, and also can add a certain proportion of water and perfume solvent and pack into and allow its slow release in the bottle, sprays on the human body lasting fragrance.This invention is economical and practical, applied widely.
Embodiment 1
Change and to add the 10g gelatin in the glue tank, 40g glycerol, the 5g PEG400, then the 15g sorbitol drops into the water of 160g, is warming up to gradually 75 ℃ behind the merceration 30min, and insulated and stirred 5h vacuum outgas is filtered and incapsulated in the machine sizing material bucket, is incubated 65 ℃, and is for subsequent use.Jasmin essence is distributed in the spice bucket of capsule, adjusts loading amount, pelleting is drying to obtain the perfume pearl.The bottling of perfume pearl is namely got product.Fragrance remaining time 15 days.
Embodiment 2
Change and to add the 10g gelatin in the glue tank, 40g glycerol, the 5g PEG400, then the 15g sorbitol drops into the water of 160g, is warming up to gradually 75 ℃ behind the merceration 30min, and insulated and stirred 5h vacuum outgas is filtered and incapsulated in the machine sizing material bucket, is incubated 65 ℃, and is for subsequent use.Jasmin essence is distributed in the spice bucket of capsule, adjusts loading amount, pelleting is drying to obtain the perfume pearl.20g perfume pearl is dissolved in 80g 95% ethanol, and the dissolving mixing namely gets product.Fragrance remaining time 24 hours.
Claims (2)
1. the preparation technology of a perfume pearl is characterized in that step is as follows:
1) changes adding 8-10%1 gelatin in the glue tank, 4-7% glycerol, the 0.5-1.0% PEG400, then the 0.5-1.5% sorbitol drops into the water of 1.5～2 times of quality of gelatin, is warming up to gradually 75 ℃ behind the merceration 30min, insulated and stirred 5h vacuum outgas, filtration incapsulates in the machine sizing material bucket, is incubated 65 ℃, and is for subsequent use;
2) perfume composition is incapsulated in the spice bucket of agent, adjust loading amount, pelleting is drying to obtain the perfume pearl.
2. described according to claim 1, its technical characterictic is that the present invention selects soft capsule component, gelatin: glycerol: PEG400: the sorbitol mass ratio is 10:4:0.5:1.5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013102547973A CN103349632A (en) | 2013-06-25 | 2013-06-25 | Preparation process of fragrance beads |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013102547973A CN103349632A (en) | 2013-06-25 | 2013-06-25 | Preparation process of fragrance beads |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103349632A true CN103349632A (en) | 2013-10-16 |
Family
ID=49306117
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2013102547973A Withdrawn CN103349632A (en) | 2013-06-25 | 2013-06-25 | Preparation process of fragrance beads |
Country Status (1)
| Country | Link |
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| CN (1) | CN103349632A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104383551A (en) * | 2014-12-09 | 2015-03-04 | 山西黄河中医药研究所（有限公司） | Traditional Chinese medicine soft capsule auxiliary material with universality and method for preparing traditional Chinese medicine soft capsules |
| CN104490612A (en) * | 2014-12-16 | 2015-04-08 | 重庆小丸科贸有限公司 | Hydrogel-microcapsule-type perfume |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101032624A (en) * | 2007-04-24 | 2007-09-12 | 辽宁大生药业有限公司 | Novel soft capsule peel composition |
-
2013
- 2013-06-25 CN CN2013102547973A patent/CN103349632A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101032624A (en) * | 2007-04-24 | 2007-09-12 | 辽宁大生药业有限公司 | Novel soft capsule peel composition |
Non-Patent Citations (3)
| Title |
|---|
| 吴克刚等: "《食品微胶囊技术》", 31 July 2006, article "香精香料微胶囊技术", pages: 194-197 * |
| 陆彬: "《药剂学》", 31 January 2003, article "胶囊剂", pages: 153 * |
| 韩瑞亭: "《药物技术技术》", 31 March 2009, article "药物及辅料的填充", pages: 108-109 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104383551A (en) * | 2014-12-09 | 2015-03-04 | 山西黄河中医药研究所（有限公司） | Traditional Chinese medicine soft capsule auxiliary material with universality and method for preparing traditional Chinese medicine soft capsules |
| CN104490612A (en) * | 2014-12-16 | 2015-04-08 | 重庆小丸科贸有限公司 | Hydrogel-microcapsule-type perfume |
| CN104490612B (en) * | 2014-12-16 | 2017-11-10 | 重庆小丸科贸有限公司 | A kind of hydrogel microcapsule type perfume |
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Legal Events
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C04 | Withdrawal of patent application after publication (patent law 2001) | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20131016 |