CN103333210B - A kind of [Mn (L) (AcO)] in-situ synthetic method (HOAc) - Google Patents
A kind of [Mn (L) (AcO)] in-situ synthetic method (HOAc) Download PDFInfo
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- CN103333210B CN103333210B CN201310301196.3A CN201310301196A CN103333210B CN 103333210 B CN103333210 B CN 103333210B CN 201310301196 A CN201310301196 A CN 201310301196A CN 103333210 B CN103333210 B CN 103333210B
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- aco
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- hoac
- hac
- synthetic method
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- 238000010189 synthetic method Methods 0.000 title claims abstract description 7
- 238000011065 in-situ storage Methods 0.000 title claims description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 title claims description 5
- 229910004373 HOAc Inorganic materials 0.000 title claims description 5
- 239000011572 manganese Substances 0.000 claims abstract description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims abstract description 10
- 239000004810 polytetrafluoroethylene Substances 0.000 claims abstract description 10
- -1 polytetrafluoroethylene Polymers 0.000 claims abstract description 7
- 238000005406 washing Methods 0.000 claims abstract description 5
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims 1
- 229910052748 manganese Inorganic materials 0.000 claims 1
- 235000021419 vinegar Nutrition 0.000 claims 1
- 239000000052 vinegar Substances 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 6
- KTOXGWMDJYFBKK-UHFFFAOYSA-L manganese(2+);diacetate;dihydrate Chemical compound O.O.[Mn+2].CC([O-])=O.CC([O-])=O KTOXGWMDJYFBKK-UHFFFAOYSA-L 0.000 abstract description 4
- 239000002904 solvent Substances 0.000 abstract description 3
- 239000000470 constituent Substances 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 2
- YZCKVEUIGOORGS-IGMARMGPSA-N Protium Chemical compound [1H] YZCKVEUIGOORGS-IGMARMGPSA-N 0.000 description 1
- 206010070834 Sensitisation Diseases 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 150000004696 coordination complex Chemical class 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 230000008313 sensitization Effects 0.000 description 1
- 230000001052 transient effect Effects 0.000 description 1
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- Plural Heterocyclic Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
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CN201310301196.3A CN103333210B (en) | 2013-07-18 | 2013-07-18 | A kind of [Mn (L) (AcO)] in-situ synthetic method (HOAc) |
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CN201310301196.3A CN103333210B (en) | 2013-07-18 | 2013-07-18 | A kind of [Mn (L) (AcO)] in-situ synthetic method (HOAc) |
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CN103333210A CN103333210A (en) | 2013-10-02 |
CN103333210B true CN103333210B (en) | 2016-05-18 |
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CN201310301196.3A Active CN103333210B (en) | 2013-07-18 | 2013-07-18 | A kind of [Mn (L) (AcO)] in-situ synthetic method (HOAc) |
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Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106397487A (en) * | 2016-09-13 | 2017-02-15 | 桂林理工大学 | Complex [Mn2(HL<1>)2(<mu>2-Cl)2(Cl)2] and application of same to preparation of anti-cancer drug |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1519000A (en) * | 1974-09-05 | 1978-07-26 | Ciba Geigy Ag | Complexes of bis-hydrazones and a process for their manufacture |
CN102426894A (en) * | 2011-09-23 | 2012-04-25 | 桂林理工大学 | Preparation method for monomolecular magnet [Co4(hmb)4(mu3-OMe)4(MeOH)4] |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB9708487D0 (en) * | 1997-04-25 | 1997-06-18 | Bp Chem Int Ltd | Novel catalysts for olefin polymerisation |
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2013
- 2013-07-18 CN CN201310301196.3A patent/CN103333210B/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1519000A (en) * | 1974-09-05 | 1978-07-26 | Ciba Geigy Ag | Complexes of bis-hydrazones and a process for their manufacture |
CN102426894A (en) * | 2011-09-23 | 2012-04-25 | 桂林理工大学 | Preparation method for monomolecular magnet [Co4(hmb)4(mu3-OMe)4(MeOH)4] |
Non-Patent Citations (3)
Title |
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Ni(Ⅱ)–牛磺酸缩水杨醛席夫碱•2,2´-联吡啶三元配合物的合成及晶体结构;蒋毅民等,;《结 构 化 学》;20030131;第22卷(第1期);第89-92页 * |
Synthesis, crystal structure, computational study of 1-(6-chloro-pyridin-2-yl)-5-hydroxy-1H-pyrazole-3-carboxylic acid methyl ester and its 5-acetoxy analogs;Li-Qun Shen等,;《Journal of Molecular Structure》;20120404;第1021卷;第167-173页,尤其是168页方案2化合物2 * |
Triaqua[2-(2-pyridylmethyleneamino)ethanesulfonato-κ3N,Nˊ,O]nickel(II) perchlorate monohydrate;Jia-Ming Li等,;《Acta Cryst.》;20061231;第m447–m449页 * |
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Effective date of registration: 20201222 Address after: 11 / F, Jingang building, south of Lianyungang Road, Sheyang Economic Development Zone, Sheyang County, Yancheng City, Jiangsu Province 224300 Patentee after: Li Zaigao Address before: 541004 the Guangxi Zhuang Autonomous Region Guilin Construction Road No. 12 Patentee before: GUILIN University OF TECHNOLOGY |
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Effective date of registration: 20221226 Address after: Room 707, Administrative Committee of Tancheng Economic Development Zone, Linyi City, Shandong Province, 276100 Patentee after: Tancheng Economic Development Zone Pharmaceutical Development Co.,Ltd. Address before: 11 / F, Jingang building, south of Lianyungang Road, Sheyang Economic Development Zone, Sheyang County, Yancheng City, Jiangsu Province 224300 Patentee before: Li Zaigao |