CN103315386A - Method for preparing extracting solution of papermaking reconstituted tobacco raw materials - Google Patents
Method for preparing extracting solution of papermaking reconstituted tobacco raw materials Download PDFInfo
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Abstract
The invention discloses a method for preparing the extracting solution of papermaking reconstituted tobacco raw materials. The method includes adding tobacco materials and enzyme preparation into the water and performing mixing and extracting, wherein the enzyme preparation comprises pectinase, cellulose and hemicellulose compound enzyme, cellulase, beta-glucanase and xylanase. By adding a certain amount of the enzyme preparation which can be used for the enzymatic hydrolysis of water-insoluble macromolecular compound such as pectin, cellulose and protein in the tobacco raw material extraction process, the using amount of the water and the extraction temperature can be reduced and the extraction time can be shortened under the condition of the same extracting solution yield, so that industrial energy saving is achieved and the production efficiency can be improved. The extracting solution obtained through the preparation method capable of improving the extracting solution yield of papermaking reconstituted tobacco raw materials can be used for manufacturing cigarettes, and the product quality can be improved effectively.
Description
Technical field
The present invention relates to the tobacco manufacture field, specifically relate to a kind of preparation method of papermaking-method reconstituted tobaccos raw material extract.
Background technology
Reconstituted tobacco refers to utilize the Discarded Tobacco materials in the cigarette process such as offal, offal, tobacco cut to make sheet or thread reconstituted product for raw material, as cigarette filler.Reconstituted tobacco originates from the 1950's, its development experience roll-in method-3 stages of thick slurry method-paper process.Papermaking-method reconstituted tobaccos is compared with the roll-in method of present production, thick slurry method reconstituted tobacco has advantages of uniqueness, comprises that density is little, the filling value is high; Anti-machining property is good, becomes the silk rate high; Burning velocity is fast, releasing content of coke tar is low; Product plasticity is good etc.Late 1970s, foreign tobacco merchant begins system research paper process thin slice technology, and has carried out applying on a large scale in the eighties in 20th century.China just began papermaking-method reconstituted tobaccos is carried out systematic research at the end of the nineties in last century, had reached so far more than 10 year.Mainly be divided into two stages: first stage is the research starting stage (1998-2004), and this stage outstanding feature is that domestic successful has been developed 3000 ton/years of pilot production lines, has realized the transformation that domestic reconstituted tobacco grows out of nothing.Second stage is Rapid development stage (2005-2010), and this stage outstanding feature is that domestic successful has been developed 10,000 ton/years of production lines, has realized the amplification of domestic reconstituted tobacco output and from having to good transformation.Be at present the phase III, will realize " cigarette packs mark tar is not higher than 10mg/ and props up, and cigarette harmfulness index is not higher than 9.0 " target by 2015, further promoted the application of papermaking-method reconstituted tobaccos.
Chinese patent application CN200610027245.9 discloses a kind of semi-countercurrent multi-stage extracting process for reproducing tobacco leaves by paper-making method, will be through 20～50% extractants as the next stage extraction in the one-level extract that obtains after the extraction process, remaining 50～80% products as extraction.The method reduces solvent load under the prerequisite that guarantees certain extraction yield, improve extract concentration, reduces the water consumption of extraction process, and further reduces the energy consumption of enrichment process.Chinese patent application CN200610035619.1 discloses a kind of method that adopts the ultrasonic-leaching technology to make the reconstituted tobacco thin slice, utilize hyperacoustic cavitation, strengthen the solvability of solable matter in offal and the offal, accelerate and increase a kind of leach extraction method of offal and offal extracts active ingredients, the extraction that can improve tobacco active ingredient.Chinese patent application CN201110267955.X discloses a kind of two-step microbial fermentation method for preparing the tobacco leachate, process by microorganism enzymolysis and microorganism flavouring two-step microbial fermentation, macromolecular substances in the tobacco material is degraded into small-molecule substance soluble in water, obtain containing a large amount of water-soluble components, high-quality tobacco leachate, higher than existing paper process tobacco leachate water-soluble low molecular weight material total recovery.But also come with some shortcomings: (1) processing procedure is very loaded down with trivial details, has greatly limited industrial applications; (2) although some method is simple, can not reach the set goal by physical means extraction yield.Therefore, the control technique by simple and stable improves tobacco material extract yield, has important Research Significance and huge market value.
Summary of the invention
The invention provides a kind of preparation method of papermaking-method reconstituted tobaccos raw material extract, by in tobacco material, adding enzyme preparation, improve the extract yield of raw tobacco material with the technique of simple and stable.
A kind of preparation method of papermaking-method reconstituted tobaccos raw material extract comprises:
Tobacco material is added to the water, and adds enzyme preparation, mixing extracts, and described enzyme preparation comprises pectase, cellulose hemicellulose complex enzyme, cellulase, 1,4 beta-glucanase and zytase.
Come the organic macromolecule material in the mixed liquor of degrading tobacco and water by adding enzyme preparation, such as pectin, protein etc., the raising extraction efficiency.
In the tobacco material leaching process, add a certain amount of enzyme preparation, can be with pectin, cellulose, the macromolecular compound enzymolysis that protein and pectin etc. are difficult water-soluble, in the situation that possess identical extract yield, can reduce the consumption of water and the temperature of extraction, and shorten extraction time, thus energy-conservation and enhance productivity in industrial realization.
Described enzyme preparation addition calculates according to enzyme activity, raw material use amount ratio and the extract yield effect of enzyme preparation self respectively.As preferably, each composition of described enzyme preparation accounts for consisting of of tobacco material gross mass:
Pectase 0.1%-1%;
Cellulose hemicellulose complex enzyme 0.1%-1%;
Cellulase 0.1%-1%;
1,4 beta-glucanase 0.1%-1%;
Zytase 0.1%-1%.
More preferred, each composition of described enzyme preparation accounts for consisting of of tobacco material gross mass:
Pectase 0.1%-1%;
Cellulose hemicellulose complex enzyme 0.5-1%;
Cellulase 0.1%-1%;
1,4 beta-glucanase 0.1%-1%;
Zytase 0.1%-1%.
Cellulose hemicellulose complex enzyme can be used for decomposing the cellulose in the tobacco material, is decomposed into the materials such as glucose, when cellulose hemicellulose complex enzyme adds with top described addition, can improve greatly the extract yield that tobacco material extracts.
More preferred, each composition of described enzyme preparation accounts for consisting of of tobacco material gross mass:
Pectase 0.1%-1%;
Cellulose hemicellulose complex enzyme 0.5-1%;
Cellulase 0.1%-1%;
1,4 beta-glucanase 0.5-1%;
Zytase 0.1%-1%.
1,4 beta-glucanase and cellulose hemicellulose complex enzyme unite use, macromolecular decomposition in the tobacco material is played a driving role, more be conducive to water-fast macromolecular accelerated decomposition, become water-soluble inorganic molecules, stay the mouthfeel that inorganic molecules in the extract also can obviously improve cigarette, make it comfortable natural again.
The most preferred, each composition of described enzyme preparation accounts for consisting of of tobacco material gross mass:
Pectase 0.1%-1%;
Cellulose hemicellulose complex enzyme 0.8%;
Cellulase 0.1%-1%;
1,4 beta-glucanase 0.8%;
Zytase 0.1%-1%.
The addition of described cellulose hemicellulose complex enzyme and 1,4 beta-glucanase be respectively account for the tobacco material gross mass 0.8% the time, can greatly improve extraction efficiency, the extract yield can reach 77.2%, relatively the amplification directly extracted of water reaches 47%.
The blending manner of described tobacco material and enzyme preparation is: tobacco material is added in the beaker, and tobacco material and water proportioning are 1:6, and then pH4～6 add enzyme preparation in 40～50 ℃ water, and mixing is mixed well.
The process conditions of described extraction are: extract 40～50 ℃ of temperature, extraction time 2～3h.
The step of described extraction is: tobacco material and the enzyme preparation of mixing are extracted 3 times extraction time 2h for the first time, rear extracted twice each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction; The each extraction dewatered with centrifugal dehydrator.
After extracting end, insoluble residue is dried by the fire 2h to weight at 125 ℃ of baking ovens, and to extract the over dry re-computation extract yield of front and back material.
The over dry anharmonic ratio of material before and after extract efficient refers to extract.
In leaching process, add enzyme preparation, make that DDGS is effectively extracted in the tobacco material, improved greatly tobacco and extracted yield; And because the stripping of macromolecular substances in the tobacco material is more favourable in the process of manufacturing paper with pulp so that the slurry after the tobacco material extraction is cleaner, particularly reduced the sticking cylinder effect of substrate, improved greatly the speed of a motor vehicle and production efficiency and yield.
The extract that said method is obtained is coated on the thin slice substrate of manufacturing paper with pulp as lotion, the dry maintenance and the silky moisture content of cigarette, subsequently chopping rolls into cigarette sample and smokes panel test, and result's demonstration is satisfied with to the improvement of assorted gas very much, has effectively improved the quality of product.
The invention has the beneficial effects as follows:
Enzyme preparation of the present invention is pectase, cellulose hemicellulose complex enzyme, cellulase, 1,4 beta-glucanase and zytase, and it has facilitation to papermaking-method reconstituted tobaccos tobacco material extract yield.Especially when the addition of enzyme preparation be above-mentioned when mentioning preferred addition, tobacco material extract yield is had remarkable facilitation, compare when extracting with direct water, tobacco material extract yield can improve 21.7%-47.0%.
The inventive method, treatment process is simple, can satisfy well the requirement of reconstituted tobacco production technology, and saves the energy, can directly amplify production, has good industrial applications prospect.
The specific embodiment
Below in conjunction with specific embodiment the present invention is described in further detail.
Embodiment 1
Raw material sources:
Pectase, the food-grade pectase of Ningxia jade of the He family Bioisystech Co., Ltd (enzyme activity is 500,000);
Cellulase, the food-grade cellulase of Ningxia jade of the He family Bioisystech Co., Ltd; The enzyme scope of living is CMC2 ten thousand u/g-150,000 u/g;
1,4 beta-glucanase, Jinan Jigang Design Inst.'s solid Type B, enzyme activity 5000IU/g;
Zytase, Henan navigator's chemical products Co., Ltd, enzyme is lived: 1,000 ten thousand～6,000 ten thousand u/g;
Cellulose hemicellulose complex enzyme, the food-grade cellulose hemicellulose complex enzyme of Ningxia jade of the He family Bioisystech Co., Ltd, enzyme activity: 〉=2200IU/g.
Getting each 2 parts of offal 50g adds in 2 beakers, the water intaking 300ml each 2 parts heat to 50 ℃, label 1,2, No. 1 is blank, it is that quality take offal is as 100% to add pectase, cellulose hemicellulose complex enzyme, cellulase, 1,4 beta-glucanase and each 0.1%(of zytase in No. 2) fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 1:
Table 1 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 63.9% | 21.7% |
The relative blank test of extract yield of processing through enzyme has increased by 21.7%, has obviously improved extraction efficiency.
Embodiment 2
Getting each 2 parts of offal 50g adds in 2 beakers, the water intaking 300ml each 2 parts heat to 50 ℃, label 1,2, No. 1 is blank, it is that quality take offal is as 100% to add pectase 0.5%, cellulose hemicellulose complex enzyme 0.8%, cellulase 0.1%, 1,4 beta-glucanase 0.8% and zytase 0.5%(in No. 2), fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 2:
Table 2 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 77.2% | 47.0% |
The relative blank test of extract yield of processing through enzyme has increased by 47.0%, has obviously improved extraction efficiency.
Embodiment 3
Getting each 2 parts of offal 50g adds in 2 beakers, the water intaking 300ml each 2 parts heat to 50 ℃, label 1,2, No. 1 is blank, it is that quality take offal is as 100% to add 1,4 beta-glucanase 0.1%, pectase, cellulose hemicellulose complex enzyme, cellulase and each 0.5%(of zytase in No. 2), fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 3:
Table 3 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 71.9% | 37.0% |
The relative blank test of extract yield of processing through enzyme has increased by 37.0%, has obviously improved extraction efficiency.
Embodiment 4
Getting each 2 parts of offal 50g adds in 2 beakers, the water intaking 300ml each 2 parts heat to 50 ℃, label 1,2, No. 1 is blank, in No. 2, add pectase, cellulose hemicellulose complex enzyme each 1.0%, 1,4 beta-glucanase 0.5%, cellulase and each 0.1%(of zytase its be that quality take offal is as 100%), fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 4:
Table 4 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 75.6% | 44.0% |
The relative blank test of extract yield of processing through enzyme has increased by 44.0%, has obviously improved extraction efficiency.
Embodiment 5
Getting each 2 parts of offal 50g adds in 2 beakers, the water intaking 300ml each 2 parts heat to 50 ℃, label 1,2, No. 1 is blank, it is that quality take offal is as 100% to add 1,4 beta-glucanase 0.1%(in No. 2), pectase, cellulose hemicellulose complex enzyme, cellulase and zytase each 1.0%, fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 5:
Table 5 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 76.6% | 45.9% |
The relative blank test of extract yield of processing through enzyme has increased by 45.9%, has obviously improved extraction efficiency.
Embodiment 6
Getting each 2 parts of offal 50g adds in 2 beakers, the water intaking 300ml each 2 parts heat to 50 ℃, label 1,2, No. 1 is blank, in No. 2, add pectase, cellulose hemicellulose complex enzyme each 0.1%, cellulase, 1,4 beta-glucanase and each 0.5%(of zytase its be that quality take offal is as 100%), fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 6:
Table 6 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 67.6% | 28.8% |
The relative blank test of extract yield of processing through enzyme has increased by 28.8%, has obviously improved extraction efficiency.
Embodiment 7
Getting each 2 parts of offal 50g adds in 2 beakers, the water intaking 300ml each 2 parts heat to 50 ℃, label 1,2, No. 1 is blank, it is that quality take offal is as 100% to add pectase 0.5%, cellulase 1.0%, cellulose hemicellulose complex enzyme, 1,4 beta-glucanase and each 0.1%(of zytase in No. 2), fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 7:
Table 7 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 66.0% | 25.7% |
The relative blank test of extract yield of processing through enzyme has increased by 25.7%, has obviously improved extraction efficiency.
Embodiment 8
Getting each 2 parts of offal 50g adds in 2 beakers, the water intaking 300ml each 2 parts heat to 50 ℃, label 1,2, No. 1 is blank, in No. 2, add 1,4 beta-glucanase, cellulose hemicellulose complex enzyme each 0.5%, cellulase, pectase each 0.1%, zytase 1.0%(its be that quality take offal is as 100%), fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 8:
Table 8 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 70.7% | 34.7% |
The relative blank test of extract yield of processing through enzyme has increased by 34.7%, has obviously improved extraction efficiency.
Comparative Examples 1
Get each 2 parts of offal 50g and add in 2 beakers, each 2 parts of water intaking 300ml heat to 50 ℃ label 1,2, No. 1 is blank, in No. 2, add 0.5% cellulase, 0.1% pectase (it is that quality take offal is as 100%), fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 9:
Table 9 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 56.3% | 7.2% |
Comparative Examples 2
Get each 2 parts of offal 50g and add in 2 beakers, each 2 parts of water intaking 300ml heat to 50 ℃ label 1,2, No. 1 is blank, in No. 2, add respectively 0.5% 1,4 beta-glucanase and pectase (it is that quality take offal is as 100%), fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 10:
Table 10 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 56.4% | 7.4% |
Comparative Examples 3
Get each 2 parts of offal 50g and add in 2 beakers, each 2 parts of water intaking 300ml heat to 50 ℃ label 1,2, No. 1 is blank, in No. 2, add respectively 0.5% pectase, cellulose hemicellulose complex enzyme and cellulase (it is that quality take offal is as 100%), fully mix with offal, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 11:
Table 11 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 54.2% | 3.2% |
Comparative Examples 4
Get each 2 parts of offal 50g and add in 2 beakers, each 2 parts of water intaking 300ml heat to 50 ℃ label 1,2, No. 1 is blank, in No. 2, add 1% cellulase, 0.5% 1,4 beta-glucanase and 0.5% pectase (it is that quality take offal is as 100%), fully mix with offal respectively, extract 3 times, extraction time 2h for the first time, rear 2 times each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction, the each extraction with the centrifugal dehydrator dehydration obtains extract.
Compare with No. 1 blank (directly water extracts) data, have preferably extraction effect after the employing processing with enzyme preparation, the results are shown in following table 12:
Table 12 extraction effect
| ? | The extract yield | Amplification |
| Blank | 52.5% | - |
| Enzyme is processed | 58.5% | 11.4% |
Claims (8)
1. the preparation method of a papermaking-method reconstituted tobaccos raw material extract is characterized in that, comprising: tobacco material is added to the water, and adding enzyme preparation, mixing extracts, and described enzyme preparation comprises pectase, cellulose hemicellulose complex enzyme, cellulase, 1,4 beta-glucanase and zytase.
2. the preparation method of papermaking-method reconstituted tobaccos raw material extract according to claim 1 is characterized in that, each composition of described enzyme preparation accounts for consisting of of tobacco material gross mass:
Pectase 0.1%-1%;
Cellulose hemicellulose complex enzyme 0.1%-1%;
Cellulase 0.1%-1%;
1,4 beta-glucanase 0.1%-1%;
Zytase 0.1%-1%.
3. the preparation method of papermaking-method reconstituted tobaccos raw material extract according to claim 2 is characterized in that, each composition of described enzyme preparation accounts for consisting of of tobacco material gross mass:
Pectase 0.1%-1%;
Cellulose hemicellulose complex enzyme 0.5-1%;
Cellulase 0.1%-1%;
1,4 beta-glucanase 0.1%-1%;
Zytase 0.1%-1%.
4. the preparation method of papermaking-method reconstituted tobaccos raw material extract according to claim 3 is characterized in that, each composition of described enzyme preparation accounts for consisting of of tobacco material gross mass:
Pectase 0.1%-1%;
Cellulose hemicellulose complex enzyme 0.5-1%;
Cellulase 0.1%-1%;
1,4 beta-glucanase 0.5-1%;
Zytase 0.1%-1%.
5. the preparation method of papermaking-method reconstituted tobaccos raw material extract according to claim 4 is characterized in that, each composition of described enzyme preparation accounts for consisting of of tobacco material gross mass:
Pectase 0.1%-1%;
Cellulose hemicellulose complex enzyme 0.8%;
Cellulase 0.1%-1%;
1,4 beta-glucanase 0.8%;
Zytase 0.1%-1%.
6. the preparation method of papermaking-method reconstituted tobaccos raw material extract according to claim 1, it is characterized in that, the blending manner of described tobacco material and enzyme preparation is: tobacco material is added in the beaker, tobacco material and water proportioning are 1:6, pH4～6, then add respectively enzyme preparation in 40～50 ℃ water, mixing is mixed well.
7. the preparation method of papermaking-method reconstituted tobaccos raw material extract according to claim 1 is characterized in that, the process conditions of described extraction are: extract 40～50 ℃ of temperature, extraction time 2～3h.
8. the preparation method of papermaking-method reconstituted tobaccos raw material extract according to claim 7, it is characterized in that, the step of described extraction is: tobacco material and the enzyme preparation of mixing are extracted 3 times, extraction time 2h for the first time, rear extracted twice each 20 minutes, constant temperature in 50 ℃ thermostat water bath, agitation as appropriate during extraction; The each extraction dewatered with centrifugal dehydrator.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104305514A (en) * | 2014-11-06 | 2015-01-28 | 云南中烟工业有限责任公司 | Method for improving regenerated tobacco leaf quality through magnetic nano carrier enzyme |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1836589A (en) * | 2006-04-24 | 2006-09-27 | 中国烟草总公司郑州烟草研究院 | Paper method leaching and thickening process for remaking tobacco leaf |
| CN101204249A (en) * | 2007-12-11 | 2008-06-25 | 广东中烟工业公司 | Preparation method for tobacco extracting |
| CN101427846A (en) * | 2007-11-07 | 2009-05-13 | 武汉烟草(集团)有限公司 | Method for improving efficiency of slice raw material abstraction and quality of slice flue gas with complex enzyme |
| CN101637298A (en) * | 2009-08-18 | 2010-02-03 | 广东中烟工业有限责任公司 | Method for preparing tobacco sheet and application thereof |
| CN101695407A (en) * | 2009-10-21 | 2010-04-21 | 安徽中烟工业公司 | Method for producing tobacco sheets by paper making method |
-
2013
- 2013-06-25 CN CN201310258263.8A patent/CN103315386B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1836589A (en) * | 2006-04-24 | 2006-09-27 | 中国烟草总公司郑州烟草研究院 | Paper method leaching and thickening process for remaking tobacco leaf |
| CN101427846A (en) * | 2007-11-07 | 2009-05-13 | 武汉烟草(集团)有限公司 | Method for improving efficiency of slice raw material abstraction and quality of slice flue gas with complex enzyme |
| CN101204249A (en) * | 2007-12-11 | 2008-06-25 | 广东中烟工业公司 | Preparation method for tobacco extracting |
| CN101637298A (en) * | 2009-08-18 | 2010-02-03 | 广东中烟工业有限责任公司 | Method for preparing tobacco sheet and application thereof |
| CN101695407A (en) * | 2009-10-21 | 2010-04-21 | 安徽中烟工业公司 | Method for producing tobacco sheets by paper making method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104305514A (en) * | 2014-11-06 | 2015-01-28 | 云南中烟工业有限责任公司 | Method for improving regenerated tobacco leaf quality through magnetic nano carrier enzyme |
| CN104305514B (en) * | 2014-11-06 | 2016-04-20 | 云南中烟工业有限责任公司 | A kind of method utilizing magnetic nano-carrier enzyme to promote reconstituted tobacco quality |
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