CN103293417B - The detection method of transformer degree of aging - Google Patents

The detection method of transformer degree of aging Download PDF

Info

Publication number
CN103293417B
CN103293417B CN201310203944.4A CN201310203944A CN103293417B CN 103293417 B CN103293417 B CN 103293417B CN 201310203944 A CN201310203944 A CN 201310203944A CN 103293417 B CN103293417 B CN 103293417B
Authority
CN
China
Prior art keywords
gas
oil
concentration
sample
component
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201310203944.4A
Other languages
Chinese (zh)
Other versions
CN103293417A (en
Inventor
梁轩伟
安晨光
杜小琴
欧林军
邢升
陆思伊
曹建
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beijing Huadian Yuntong Power Technology Co Ltd
Original Assignee
Beijing Huadian Yuntong Power Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Beijing Huadian Yuntong Power Technology Co Ltd filed Critical Beijing Huadian Yuntong Power Technology Co Ltd
Priority to CN201310203944.4A priority Critical patent/CN103293417B/en
Publication of CN103293417A publication Critical patent/CN103293417A/en
Application granted granted Critical
Publication of CN103293417B publication Critical patent/CN103293417B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Housings And Mounting Of Transformers (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The detection method that the invention discloses a kind of transformer degree of aging, the method comprises the steps: 1) be V to volumeoil-sampleTransformer insulation oil oil sample vacuumize, the mist that makes to be dissolved in insulating oil separates with oily, after separating, the cumulative volume of mist place air chamber is Vgas; 2) from isolated mist, extract the sample gas of certain volume; 3) gas mixing in described sample gas is separated, isolate H2、CO、CH4、C2H4、C2H6、C2H2Gas; 4) measure respectively H by gas sensor2、CO、CH4、C2H4、C2H6、C2H2The concentration C of gasgas-i-detect; 5), according to formula<maths num="0001"></maths>Calculate the concentration C of gas component i in tested oil samplei-in-oil, wherein, η is stripping factor; Step 5), according to the concentration C of gas component ii-in-oil, according to known method analysis with judge transformer degree of aging and fault type.

Description

The detection method of transformer degree of aging
Technical field
The present invention relates to a kind of detection method of transformer degree of aging, especially utilize and be dissolved inGas content in transformer insulation oil judges the method for transformer degree of aging.
Background technology
Component and the content of analyzing oil dissolved gas are to monitor oil-filled electric equipment safe operationOne of effective measures, utilize gc analysis oil dissolved gas to monitor oil-filled electricEquipment safety operation has had the use experience of more than 40 year in China. According to " GB/7252-2001Gases Dissolved in Transformer Oil is analyzed and is judged directive/guide " regulation, this measuring method need throughCross sampling, from oil, deviate from dissolved gas, gas sampling, gas separate, gas detects, knowSeven links such as calculation peak, peak, quantitative calculating, each link very important person, for participating in, easily causes mistakePoor, bring very big impact to test repeatability and accuracy.
The release of Dissolved Gases in Transformer Oil on-line monitoring method is several years only, from electric power areSystem operation department feedback obtains message, several thousand Gases Dissolved in Transformer Oils installing at homeThe ruuning situation of on-Line Monitor Device is also pessimistic, and problem is mainly that measure error is bigger than normal.
Summary of the invention
For problems of the prior art, the detection method of transformer degree of aging of the present inventionCarrying out a large amount of actual measurements, accumulating on a large amount of operating experience bases, working outA whole set of separates link from Oil-gas Separation link, mist quantitative sample injection link, mistCalculate the comprehensive study analyses such as link with tested gasometry, obtained a kind of based on chromatographic techniqueThe online of operating transformer insulating oil dissolved gas quantitatively detected and calculated, and then draw transformationThe method of device degree of aging.
To achieve these goals, the detection method of transformer degree of aging of the present invention, the methodComprise the steps:
Step 1) is V to volumeoil-sampleTransformer insulation oil oil sample vacuumize, makeThe mist being dissolved in insulating oil separates with oily, and after separating, mist place air chamber is totalVolume is Vgas
Step 2), from isolated mist, extract the sample gas of certain volume;
Step 3), separates the gas mixing in described sample gas, isolates H2、CO、CH4、C2H4、C2H6、C2H2Gas;
Step 4), measures respectively H by gas sensor2、CO、CH4、C2H4、C2H6、C2H2The concentration C of gasgas-i-detect
Step 5), according to formula
C i - in - oil = C gas - i - det ect * V gas ( 1 - &eta; ) * V oil - sample
Calculate the concentration C of gas component i in tested oil samplei-in-oil, wherein, η is degassed systemNumber;
Step 5), according to the concentration C of gas component ii-in-oil, according to known method analysis andJudge transformer degree of aging and fault type.
Further, described in described step 4), gas sensor is measured H as follows2、CO、CH4、C2H4、C2H6、C2H2The concentration C of gasgas-i-detect
1. step, is used the H of several variable concentrations2、CO、CH4、C2H4、C2H6、C2H2Calibrating gas carries out C to gas sensori-xConcentration calibration, wherein, i is gas component, xBe in x kind concentration;
2. step, demarcates the H of rear variable concentrations2、CO、CH4、C2H4、C2H6、C2H2Gas pairThe peak height of answering is Hi-x
3. step, carries out Mathematical Fitting to the gas of each component respectively with Lagrangian method:Cgas-i-detect=f(Hi), and calculate the concentration value C of gas igas-i-detect
Wherein, i is gas component, and x is x kind concentration.
Further, to described Ci-xWith described Hi-xSet up respectively ID table, every group of standard divided gasBody be divided into 10 grades by concentration, in described ID table, be arranged in order from low to high.
Detailed description of the invention
Below the specific embodiment of the present invention is elaborated.
Insulating oil dissolved gas of the present invention detects metering method online, and the method comprises the steps:
Step 1) is V to volumeoil-sampleTransformer insulation oil oil sample vacuumize, makeThe mist being dissolved in insulating oil separates with oily, and after separating, mist place air chamber is totalVolume is Vgas
Step 2), from isolated mist, extract the sample gas of certain volume.
Step 3), separates the gas mixing in described sample gas, isolates H2、CO、CH4、C2H4、C2H6、C2H2Gas.
Step 4), measures respectively H by gas sensor2、CO、CH4、C2H4、C2H6、C2H2The concentration C of gasgas-i-detect, concrete detecting step is: the H that 1. uses 10 kinds of variable concentrations2、CO、CH4、C2H4、C2H6、C2H2Calibrating gas carries out C to gas sensori-xConcentration calibration,Set up concentration ID table from low to high, in table 1; 2. the H of variable concentrations after demarcating2、CO、CH4、C2H4、C2H6、C2H2The peak height that gas is corresponding is Hi-x, set up Hi-xID table, seeTable 2, wherein, i is gas component, x is in x kind concentration; 3. use Lagrangian methodRespectively the gas of each component is carried out to Mathematical Fitting: Cgas-i-detect=f(Hi), and calculateDraw the concentration value C of gas igas-i-detect
Step 5), according to formula
C i - in - oil = C gas - i - det ect * V gas ( 1 - &eta; ) * V oil - sample
Calculate the concentration C of gas component i in tested oil samplei-in-oil, wherein, η is degassed systemNumber.
Step 5), according to the concentration C of gas component ii-in-oil, according to State Grid's standardThe event of the proposition in GBT7252-2001 " Gases Dissolved in Transformer Oil analysis and judge directive/guide "Barrier type judgement method, analyzes and judges transformer degree of aging and fault type.
The corresponding concentration of table 1 gas with various component (unit: ppm)
Gas H2 CO CH4 C2H4 C2H6 C2H2
1 2.07 4.78 0.5 0.5 0.51 0.51
2 8.28 19.10 2.00 2.00 2.02 20.2
3 18.97 40.65 6.97 5.48 4.98 5.13
4 59.28 127.03 21.78 17.13 15.58 16.03
5 128.03 274.37 47.03 36.99 33.64 34.61
6 237.10 508.10 87.10 68.50 62.30 64.10
7 809.37 1502.24 289.70 229.11 208.83 256.36
8 1380.69 2562.64 494.19 390.83 356.24 437.32
9 2332.89 4329.98 835.01 660.37 601.92 738.92
10 3856.41 7157.73 1380.32 1091.64 995.64 1221.48
The corresponding peak height of table 2 variable concentrations gas component (unit: uv)
Embodiment 1
The transformer insulation oil oil sample that step 1) is 45ml to volume vacuumizes, and makes moltenThe mist of solution in insulating oil separates with oily, and after separating, mist place air chamber is overallAmass as 18.47ml.
Step 2), from isolated mist, extract the sample gas of certain volume.
Step 3), separates the gas mixing in described sample gas, isolates H2、CO、CH4、C2H4、C2H6、C2H2Gas.
Step 4), measures respectively H by gas sensor2、CO、CH4、C2H4、C2H6、C2H2The concentration C of gasgas-i-detectConcrete detecting step is: the H that 1. uses 10 kinds of variable concentrations2、CO、CH4、C2H4、C2H6、C2H2Calibrating gas carries out C to gas sensori-xConcentration calibration,Set up concentration ID table from low to high, in table 1; 2. the H of variable concentrations after demarcating2、CO、CH4、C2H4、C2H6、C2H2The peak height that gas is corresponding is Hi-x, set up Hi-xID table, seeTable 2, wherein, i is gas component, x is in x kind concentration; 3. use Lagrangian methodRespectively the gas of each component is carried out to Mathematical Fitting: Cgas-i-detect=f(Hi), and calculateDraw the concentration value C of gas igas-i-detect, in table 3.
Step 5), according to formula
C i - in - oil = C gas - i - det ect * V gas ( 1 - &eta; ) * V oil - sample
Calculate the concentration C of gas component i in tested oil samplei-in-oil, in table 3, wherein, η isStripping factor.
Table 3
Step 5), by the concentration C of gas component ii-in-oilAccording to State Grid's standardThe event of the proposition in GBT7252-2001 " Gases Dissolved in Transformer Oil analysis and judge directive/guide "Barrier type judgement method, knows C2H2/C2H4,CH4/H2,C2H4/C2H6Ratio be 0.48,0.13,7.33, be encoded to 1,0,2, can judge measurand is the aging of transformerDegree and fault type are low energy electric discharge.
Embodiment 2
The transformer insulation oil oil sample that step 1) is 45ml to volume vacuumizes, and makes moltenThe mist of solution in insulating oil separates with oily, and after separating, mist place air chamber is overallAmass as 18.47ml.
Step 2), from isolated mist, extract the sample gas of certain volume.
Step 3), separates the gas mixing in described sample gas, isolates H2、CO、CH4、C2H4、C2H6、C2H2Gas.
Step 4), measures respectively H by gas sensor2、CO、CH4、C2H4、C2H6、C2H2The concentration C of gasgas-H2-detect-concrete detecting step is: the H that 1. uses 10 kinds of variable concentrations2、CO、CH4、C2H4、C2H6、C2H2Calibrating gas carries out C to gas sensori-xConcentration calibration,Set up concentration ID table from low to high, in table 1; 2. the H of variable concentrations after demarcating2、CO、CH4、C2H4、C2H6、C2H2The peak height that gas is corresponding is Hi-x, set up Hi-xID table, seeTable 2, wherein, i is gas component, x is in x kind concentration; 3. use Lagrangian methodRespectively the gas of each component is carried out to Mathematical Fitting: Cgas-i-detect=f(Hi), and calculateDraw the concentration value C of gas igas-i-detect, in table 4.
Step 5), according to formula
C i - in - oil = C gas - i - det ect * V gas ( 1 - &eta; ) * V oil - sample
Calculate the concentration C of gas component i in tested oil samplei-in-oil, as table 4 shows, wherein,η is stripping factor.
Table 4
Step 5), by the concentration C of gas component ii-in-oilAccording to State Grid's standardThe event of the proposition in GBT7252-2001 " Gases Dissolved in Transformer Oil analysis and judge directive/guide "Barrier type judgement method, knows C2H2/C2H4,CH4/H2,C2H4/C2H6Ratio be 0.20,3.63,9.85, be encoded to 1,2,2, can judge measurand is the aging of transformerDegree and fault type are that low energy electric discharge is double overheated.
Embodiment 3
The transformer insulation oil oil sample that step 1) is 45ml to volume vacuumizes, and makes moltenThe mist of solution in insulating oil separates with oily, and after separating, mist place air chamber is overallAmass as 18.47ml.
Step 2), from isolated mist, extract the sample gas of certain volume.
Step 3), separates the gas mixing in described sample gas, isolates H2、CO、CH4、C2H4、C2H6、C2H2Gas.
Step 4), measures respectively H by gas sensor2、CO、CH4、C2H4、C2H6、C2H2The concentration C of gasgas-H2-detect-concrete detecting step is: the H that 1. uses 10 kinds of variable concentrations2、CO、CH4、C2H4、C2H6、C2H2Calibrating gas carries out C to gas sensori-xConcentration calibration,Set up concentration ID table from low to high, in table 1; 2. the H of variable concentrations after demarcating2、CO、CH4、C2H4、C2H6、C2H2The peak height that gas is corresponding is Hi-x, set up Hi-xID table, seeTable 2, wherein, i is gas component, x is in x kind concentration; 3. use Lagrangian methodRespectively the gas of each component is carried out to Mathematical Fitting: Cgas-i-detect=f(Hi), and calculateDraw the concentration value C of gas igas-i-detect, in table 5.
Step 5), according to formula
C i - in - oil = C gas - i - det ect * V gas ( 1 - &eta; ) * V oil - sample
Calculate the concentration C of gas component i in tested oil samplei-in-oil, as table 5 shows, wherein,η is stripping factor.
Table 5
Step 5), by the concentration C of gas component ii-in-oilAccording to State Grid's standardThe event of the proposition in GBT7252-2001 " Gases Dissolved in Transformer Oil analysis and judge directive/guide "Barrier type judgement method, knows C2H2/C2H4,CH4/H2,C2H4/C2H6Ratio be 0.49,6.21,0.82, be encoded to 1,2,0, can judge measurand is the aging of transformerDegree and fault type are that low energy electric discharge is double overheated.
Above-mentioned example is just for illustrating the present invention, and embodiments of the present invention are not limited to theseExample, the various detailed description of the invention of inventive concept that what those skilled in the art made meetAll within protection scope of the present invention.

Claims (2)

1. the detection method of transformer degree of aging, is characterized in that, the method comprises the steps:
Step 1), be V to volumeoil-sampleTransformer insulation oil oil sample vacuumize, the mist that makes to be dissolved in insulating oil separates with oily, after separating, the cumulative volume of mist place air chamber is Vgas
Step 2), from isolated mist, extract the sample gas of certain volume;
Step 3), the gas mixing in described sample gas is separated, isolate H2、CO、CH4、C2H4、C2H6、C2H2Gas;
Step 4), measure respectively H by gas sensor2、CO、CH4、C2H4、C2H6、C2H2The concentration C of gasgas-i-detect
Step 5), according to formula
Calculate the concentration C of gas component i in tested oil samplei-in-oil, wherein, η is stripping factor;
Step 6), according to the concentration C of gas component ii-in-oil, according to the fault type determination methods of the proposition in the standard GBT7252-2001 of State Grid " Gases Dissolved in Transformer Oil analysis and judge directive/guide ", analyze and judge transformer degree of aging and fault type;
Wherein, described step 4) described in gas sensor measure as follows H2、CO、CH4、C2H4、C2H6、C2H2The concentration C of gasgas-i-detect
1. step, is used the H of several variable concentrations2、CO、CH4、C2H4、C2H6、C2H2Calibrating gas carries out C to gas sensori-xConcentration calibration, wherein, i is gas component, x is x kind concentration;
2. step, demarcates the H of rear variable concentrations2、CO、CH4、C2H4、C2H6、C2H2The peak height that gas is corresponding is Hi-x
3. step, carries out Mathematical Fitting: C to the gas of each component respectively with Lagrangian methodgas-i-detect=f(Hi), and calculate the concentration value C of gas igas-i-detect
Wherein, i is gas component, and x is x kind concentration.
2. the detection method of transformer degree of aging as claimed in claim 1, is characterized in that, to described Ci-xWith described Hi-xSet up respectively ID table, the calibrating gas of every component is divided into 10 grades by concentration, in described ID table, is arranged in order from low to high.
CN201310203944.4A 2013-05-28 2013-05-28 The detection method of transformer degree of aging Active CN103293417B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310203944.4A CN103293417B (en) 2013-05-28 2013-05-28 The detection method of transformer degree of aging

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310203944.4A CN103293417B (en) 2013-05-28 2013-05-28 The detection method of transformer degree of aging

Publications (2)

Publication Number Publication Date
CN103293417A CN103293417A (en) 2013-09-11
CN103293417B true CN103293417B (en) 2016-05-25

Family

ID=49094627

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310203944.4A Active CN103293417B (en) 2013-05-28 2013-05-28 The detection method of transformer degree of aging

Country Status (1)

Country Link
CN (1) CN103293417B (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110068530B (en) * 2019-05-09 2022-06-24 苏州市职业大学 PVC pipe aging detection device
CN111308286B (en) * 2020-03-06 2021-01-12 西南交通大学 Method for estimating service life of traction transformer under multi-parameter empowerment combination
CN111579948A (en) * 2020-05-26 2020-08-25 重庆大学 Method for analyzing fault of mixed insulating oil transformer based on dissolved gas in oil

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5659126A (en) * 1996-04-19 1997-08-19 Farber; Milton Gas chromatograph techniques for on-line testing of transformer faults
CN1779471A (en) * 2004-11-17 2006-05-31 上海神源电气有限公司 Frequency-converter ageing tester
CN101408578B (en) * 2008-11-21 2011-12-14 重庆大学 Multiple factors accelerated aging test apparatus and method for oil paper insulation of transformer
CN102033118B (en) * 2009-09-25 2012-11-14 上海宝钢工业检测公司 Method for testing aging degree of transformer oil

Also Published As

Publication number Publication date
CN103293417A (en) 2013-09-11

Similar Documents

Publication Publication Date Title
CN106645531B (en) A kind of modification method of Gases Dissolved in Transformer Oil detection data
CN111307984B (en) On-site calibration system for dissolved gas on-line monitoring device in insulating oil
CN103293417B (en) The detection method of transformer degree of aging
CN101887051A (en) Online chromatographic analysis method
CN105021732A (en) Method for fast determination of oxygen isotope composition of water in beverage wine
CN101915821A (en) Check method and system of SF6 gas catabolite detecting instrument
CN105158356A (en) Method for separating helium and hydrogen in oil chromatography of converter transformer
CN102967671B (en) Device and method for detecting sulfur hexafluoride gas in oil immersed transformer
CN101451982A (en) Parameter regulation means for on-line gas chromatographic analysis device
CN109781809A (en) A kind of concentration of formaldehyde artificial intelligence measuring method
CN112461944A (en) Calibration method of online monitoring device for dissolved gas in transformer oil
CN106525998A (en) Method of measuring content of benzene series ingredients in stationary pollution source waste gas
CN102565241B (en) Preparation method of gas sample in vinyl gas chromatography analysis of 110 methylvinyl silicone rubber
CN105717006A (en) Method for evaluating uncertainty of measuring result of laser particle size analyzer
CN105136917A (en) Qualitative and quantitative analytic method of multiple sulfides in transformer oil
US9976985B2 (en) Field asymmetric ion mobility spectrometry system
Li et al. Estimation of dissolved gas concentrations in transformer oil from membranes
CN110879222A (en) Construction method of quantitative analysis curve of furfural in transformer oil and detection method of furfural content
CN105572279A (en) Method for determining naphthalene content of coal tar through gas chromatography
CN111024828B (en) Online detection device and detection method for nitrogen content of air foam flooding oil well
CN114034776A (en) Device and method for measuring distribution coefficient of dissolved gas in insulating oil
CN107796886A (en) A kind of method of propylene content in measure insulating oil
CN108120744B (en) Method for measuring oxidation induction time of vegetable oil in aqueous medium
CN202676655U (en) Device for measuring gas concentration by using electrochemical sensor
JP2777304B2 (en) Abnormality diagnosis apparatus and diagnosis method for perfluorocarbon input device

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant