CN103288347B - Super flat high-penetration high-brightness once-firing drenches throws frit and methods for making and using same thereof - Google Patents
Super flat high-penetration high-brightness once-firing drenches throws frit and methods for making and using same thereof Download PDFInfo
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- CN103288347B CN103288347B CN201310241465.1A CN201310241465A CN103288347B CN 103288347 B CN103288347 B CN 103288347B CN 201310241465 A CN201310241465 A CN 201310241465A CN 103288347 B CN103288347 B CN 103288347B
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- 238000010304 firing Methods 0.000 title claims abstract description 22
- 238000000034 method Methods 0.000 title claims abstract description 19
- 239000000919 ceramic Substances 0.000 claims abstract description 26
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 19
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 208000002682 Hyperkalemia Diseases 0.000 claims abstract description 5
- 206010021036 Hyponatraemia Diseases 0.000 claims abstract description 5
- 239000011787 zinc oxide Substances 0.000 claims abstract description 5
- 239000002002 slurry Substances 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 238000005498 polishing Methods 0.000 claims description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 6
- 239000002689 soil Substances 0.000 claims description 6
- 238000002844 melting Methods 0.000 claims description 5
- 230000008018 melting Effects 0.000 claims description 5
- 239000000758 substrate Substances 0.000 claims description 5
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 4
- 239000004327 boric acid Substances 0.000 claims description 4
- 229910052681 coesite Inorganic materials 0.000 claims description 4
- 229910052593 corundum Inorganic materials 0.000 claims description 4
- 229910052906 cristobalite Inorganic materials 0.000 claims description 4
- 239000010459 dolomite Substances 0.000 claims description 4
- 229910000514 dolomite Inorganic materials 0.000 claims description 4
- 239000010433 feldspar Substances 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000000377 silicon dioxide Substances 0.000 claims description 4
- 238000004513 sizing Methods 0.000 claims description 4
- 229910052682 stishovite Inorganic materials 0.000 claims description 4
- 229910052905 tridymite Inorganic materials 0.000 claims description 4
- 229910001845 yogo sapphire Inorganic materials 0.000 claims description 4
- 239000005995 Aluminium silicate Substances 0.000 claims description 3
- 235000019738 Limestone Nutrition 0.000 claims description 3
- 235000012211 aluminium silicate Nutrition 0.000 claims description 3
- 239000002537 cosmetic Substances 0.000 claims description 3
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 3
- 239000006028 limestone Substances 0.000 claims description 3
- 239000010453 quartz Substances 0.000 claims description 3
- 239000011230 binding agent Substances 0.000 claims description 2
- 239000004615 ingredient Substances 0.000 claims description 2
- 238000009413 insulation Methods 0.000 claims description 2
- 230000014759 maintenance of location Effects 0.000 claims description 2
- 239000002245 particle Substances 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 6
- 239000011449 brick Substances 0.000 description 7
- 238000000498 ball milling Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000001488 sodium phosphate Substances 0.000 description 4
- 229910000162 sodium phosphate Inorganic materials 0.000 description 4
- 239000013638 trimer Substances 0.000 description 4
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 229920000609 methyl cellulose Polymers 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 239000001923 methylcellulose Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
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Abstract
The invention discloses a kind of super flat high-penetration high-brightness once-firing and drench throwing frit and methods for making and using same thereof, belong to ceramic glaze technical field. The method adopts hyperkalemia hyponatremia formula, adjusts the ratio of aluminium oxide and zinc oxide in frit composition simultaneously, to produce highlighted transparent effect, meets under ceramic glaze and decorates, surface finish condition. Compared with the frit used with traditional glaze pouring, this product and technique have improved the class of ceramic greatly, and compared with the brilliant dry granular of secondary burning throwing, this product has not only ensured the quality of ceramic, and having greatly reduced the consumption of frit, production cost can reduce by 30～50%.
Description
Technical field
The invention belongs to ceramic glaze technical field, be specifically related to a kind of super flat high-penetration high-brightness once-firing drench throw frit andIts methods for making and using same.
Background technology
It is mainly to obtain different surface effects for the ceramic after making to burn till that frit is applied to Ceramic glaze. In recent yearsOccurred that a kind of floor tile throws brilliant brick, a kind of ceramic tile production process that utilizes exactly the transparency of frit to form, specifically makesLow temperature frit (750～900 DEG C of beginning fusing points), thick after oven dry powder process (3mm left and right) is sprinkling upon and is decorated specific effect of decorative patternsAnd on floor tile after burning till, then easy fired, polishing afterwards, makes secondary and burns and throw brilliant dry granular brick. Throw brilliant brick smooth, smooth, highBright, decorative pattern rich texture, third dimension are strong, and owing to being that underglaze colour decorative pattern is not easy to wear. Due to this height of twice firing, developCan be suitable for the brilliant frit of the throwing of once burning, adopt the direct fired ceramic of firing technique one time, then polishing, not only provide cost savings but also canMake goods reach secondary and burn the brilliant effect of throwing, have very large market value.
Throwing brilliant dry granular is, after frit is pulverized by special installation, to carry out as required the one that rational gradation composition obtainsDry granular.
Application number is in 201110320534.9 Chinese invention patent application file, to have recorded a kind of once-firing to throw brilliantDry granular and application thereof for brick. This invention dry granular is made up of at least one in high potassium, high barium, three kinds of dry granulars of high zinc, of the present inventionDry granular initial melting temperature is high, and the grain composition that high temperature viscosity is little and good both can ensure that base substrate exhaust was good, again can be at heightThe lower eliminating bubble as far as possible of temperature; The brilliant brick of throwing that uses the brilliant brick of throwing of the present invention to make with dry granular, once-firing, can save high temperatureBiscuiting process, greatly reduces energy consumption, has effectively reduced pollution, can reduce production costs compared with secondary firing technique nearly 15%,Greatly improve productivity effect. The brilliant brick of throwing that production obtains, glaze transparency is high, and bubble is few.
Cannot compare although throw the prepared ceramic of brilliant dry granular traditional glaze pouring on class, due to throwingThe production process of brilliant dry granular is too complicated, and required management and equipment cost are all very high, add that its consumption is large, cause the cost of productMake manufacturer beyond affordability.
Summary of the invention
The technical problem to be solved in the present invention is: overcome the deficiencies in the prior art, provide a kind of super flat high-penetration high-brightness onceBurn till to drench and throw frit and methods for making and using same thereof. Under the prerequisite that reaches the brilliant dry granular effect of throwing, reduce production costs.
The technical solution adopted for the present invention to solve the technical problems is: super flat high-penetration high-brightness once-firing drenches throws frit,The relative weight percentage of described frit based on oxide gross weight meter is:
SiO250～55%
Al2O315～20%
K2O3～5%
CaO9～13%
MgO0～1%
B2O37～11%
ZnO6～9%
Other are 0～1% years old.
Preferably, the relative weight percentage of described frit based on oxide gross weight meter is:
SiO251～52%
Al2O317～18%
K2O3.5～4.5%
CaO10～11%
MgO0.5～1%
B2O38～9%
ZnO7～8%
Other are 0～1% years old.
Preferably, have the following ingredients as parent material, the gross weight of described composition based on these compositions is with weightCount:
Quartz 15～20%
Hyperkalemia hyponatremia feldspar 30～43%
Lime stone 12～17%
Dolomite 2～6%
Zinc oxide 5～8%
Boric acid 11～20%
Aluminium oxide 9～13%.
Super flat high-penetration high-brightness once-firing drenches the preparation method who throws frit, comprises the step of described parent material heating and meltingSuddenly, described melt temperature is 1500～1700 DEG C.
Preferably, also comprise the step that the raw material of described melting is incubated at described temperature, temperature retention time is 2～4 littleTime.
Preferably, also comprise the step of the parent material after described heating and thermal insulation being carried out to shrend, shrend water usedMiddle interpolation antisludging agent.
Super flat high-penetration high-brightness once-firing drenches the application process of throwing frit, comprises following processing step:
1) will in frit, add a small amount of water, kaolin and degumming agent and binding agent to wear into the slurry of desired particle size;
2) slurry making in step 1) being imposed on the ceramic body of cosmetic soil, described usage of sizing agent is 0.3～0.7g/cm2；
3) base substrate of executing slurry is burnt till, then carry out polishing, make super flat high-penetration high-brightness ceramic.
Compared with prior art, the invention has the beneficial effects as follows:
Adjust and the super flat high-penetration high-brightness once-firing pouring throwing frit of technology controlling and process making by formula, can adopt " pouring glaze-Burn till-polishing " technology generations is for existing " executing dry granular-burn till-polishing " technique, can save 20～30% frit consumption, with throwingBrilliant dry granular is compared, and production cost can reduce by 30～50%.
After using the ceramic of this kind of frit to burn till, there is super flat, high saturating, highlighted visual effect, have as jadewareTexture.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further. Wherein, parent material used and oxide composition thereofIn table 1.
Table 1 parent material and oxide composition thereof
Parent material control fineness used is as follows:
1) quartz, lime stone and dolomite, 200 mesh screen residues are less than 5%;
2) hyperkalemia hyponatremia feldspar, 80 mesh screen residues are less than 3%;
3) zinc oxide, boric acid and aluminium oxide pulverize.
Embodiment 1
The oxide that super flat high-penetration high-brightness once-firing in this embodiment drenches throwing frit forms in table 2.
The oxide weight percentage of table 2 frit
In each embodiment, supply 100% surplus and formed by impurity.
The preparation method of this kind of frit mainly divides following three steps:
1) configuration of compound: take respectively quartzy 17.5Kg in small, broken bits, hyperkalemia hyponatremia feldspar 34.5Kg, lime stone14Kg, dolomite 3.5Kg, zinc oxide 6.5Kg, boric acid 13Kg and aluminium oxide 11Kg, above-mentioned parent material all required 80 mesh sieves,Then in batch mixer, mix;
2) melting of compound: calcar is warming up to after 1580 DEG C, the compound mixing in step 1) is addedIn calcar, and be incubated 2.5 hours at this temperature, make liquation;
3) open the stove plug of calcar bottom, make step 2) in the liquation that makes flow in water-cooled pond, wherein, fused solution streamOutlet is 1～1.5 meter with the liquid level distance in water-cooled pond. Wherein, water quenching pool at least should carry out dirty removing processing every month, and shrend waterMiddle interpolation antisludging agent.
Liquation is quenched into granular frit after entering water-cooled pond. After dry, make super flat high-penetration high-brightness once-firing and drench throwingFrit.
The application process of this kind of frit is as follows:
Take dried frit 190g, kaolin 10g, water 80g, sodium phosphate trimer 0.5g, methylcellulose 0.3g, addEnter in ball mill, ball milling 15 minutes, makes slurry fast, and slurry is crossed 100 mesh sieves, is defined as slurry No. 1.
No. 1 slurry is drenched to glaze to the ceramic tile blank that has cosmetic soil of flower out of the press, and usage of sizing agent is 0.5g/cm2(,Sizing material 0.5g on every square centimeter of base substrate). The base substrate drenching after glaze is burnt till in the roller kilns of 1130 DEG C of left and right, cooling afterPolishing on polishing machine.
The surface quality of ceramic tile that the present embodiment is fired is in table 3, and wherein, surperficial pore is 1 meter of vertical ceramic tile surfaceDistance obtains by visually observing, and glossiness adopts vancometer UG60 test.
The surface quality of the different embodiment gained of table 3 ceramic tile
Embodiment 2～7
Adopt parent material and condition in table 4, according to the method preparation of embodiment 1. The obtained frit of embodiment 2～7Oxide weight percentage in table 2. The surface quality of ceramic tile that each embodiment fires is in table 3, and wherein, surperficial pore is to hang downThe distance that straight ceramic tile surface is 1 meter is by visually observing, and glossiness adopts vancometer UG60 test.
The different embodiment of table 4 parent material used consumption and technological parameter by weight
Comparative example 1
Take large great 1415# interior wall clear frit 190g, water 80g, Datong District soil 10g, sodium phosphate trimer 0.5g, methyl fiberElement 0.3g. Add in Quick ball grinder, ball milling 15 minutes, glaze slip is crossed 100 mesh sieves, is defined as slurry No. 2.
Adopt slurry No. 2, fire ceramic tile according to the method in embodiment 1, record fired ceramic tile surface quality in table 4.
Comparative example 2
Take the Kunlun enamel frit makeing 876# interior wall clear frit 190g, water 80g, Datong District soil 10g, sodium phosphate trimer 0.5g, methylCellulose 0.3g. Add in Quick ball grinder, ball milling 15 minutes, glaze slip is crossed 100 mesh sieves, is defined as slurry No. 3.
Adopt slurry No. 2, fire ceramic tile according to the method in embodiment 1, record fired ceramic tile surface quality in table 4.
Comparative example 3
Take the 1710# of our company interior wall clear frit 190g, water 80g, Datong District soil 10g, sodium phosphate trimer 0.5g, methyl fibreTie up plain 0.3g. Add in Quick ball grinder, ball milling 15 minutes, glaze slip is crossed 100 mesh sieves, records fired ceramic tile surface quality in Table4。
The above, be only preferred embodiment of the present invention, is not the restriction of the present invention being made to other form, appointsThe equivalence what those skilled in the art may utilize the technology contents of above-mentioned announcement to be changed to equivalent variations is implementedExample. But every technical solution of the present invention content that do not depart from, that according to technical spirit of the present invention, above embodiment is done appointsWhat simple modification, equivalent variations, still belong to the protection domain of technical solution of the present invention.
Claims (7)
1. super flat high-penetration high-brightness once-firing drenches and throws frit, it is characterized in that the phase of described frit based on oxide gross weight meterTo percentage by weight be:
SiO250～55%
Al2O315～20%
K2O3～5%
CaO9～13%
MgO0～1%
B2O37～11%
ZnO6～9%
Other are 0～1% years old.
2. super flat high-penetration high-brightness once-firing according to claim 1 drenches and throws frit, it is characterized in that, described frit based onThe relative weight percentage of oxide gross weight meter is:
SiO251～52%
Al2O317～18%
K2O3.5～4.5%
CaO10～11%
MgO0.5～1%
B2O38～9%
ZnO7～8%
Other are 0～1% years old.
3. super flat high-penetration high-brightness once-firing according to claim 1 and 2 drenches and throws frit, it is characterized in that, existence is used asThe following ingredients of parent material, the gross weight of described composition based on these compositions is by weight:
Quartz 15～20%
Hyperkalemia hyponatremia feldspar 30～43%
Lime stone 12～17%
Dolomite 2～6%
Zinc oxide 5～8%
Boric acid 11～20%
Aluminium oxide 9～13%.
4. super flat high-penetration high-brightness once-firing according to claim 3 drenches a preparation method who throws frit, and its feature existsIn: comprise the step of described parent material heating and melting, melt temperature is 1500～1700 DEG C.
5. super flat high-penetration high-brightness once-firing according to claim 4 drenches the preparation method who throws frit, it is characterized in that: alsoComprise the step that the raw material of described melting is incubated at described temperature, temperature retention time is 2～4 hours.
6. super flat high-penetration high-brightness once-firing according to claim 5 drenches the preparation method who throws frit, it is characterized in that: alsoComprise the step of the parent material after described heating and thermal insulation being carried out to shrend, in shrend water used, add antisludging agent.
7. super flat high-penetration high-brightness once-firing according to claim 3 drenches an application process of throwing frit, and its feature existsIn, comprise following processing step:
1) will in frit, add a small amount of water, kaolin and degumming agent and binding agent to wear into the slurry of desired particle size;
2) slurry making in step 1) is imposed on the ceramic body of cosmetic soil, described usage of sizing agent is 0.3～0.7g/cm2；
3) base substrate of executing slurry is burnt till, then carry out polishing, make super flat high-penetration high-brightness ceramic.
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| CN104311155B (en) * | 2014-10-11 | 2019-04-19 | 杭州诺贝尔陶瓷有限公司 | A kind of crystallization vitreous brick and its production method |
| CN109928779B (en) * | 2019-05-17 | 2019-08-23 | 蒙娜丽莎集团股份有限公司 | A kind of wet process leaching sizing process dry-particle ceramic tile and preparation method thereof |
| CN110790510A (en) * | 2019-12-16 | 2020-02-14 | 黄奕雯 | Wear-resistant high-hardness ceramic glaze and preparation method thereof |
| CN111943512A (en) * | 2020-08-31 | 2020-11-17 | 重庆鸽牌电瓷有限公司 | High-performance glaze |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3804666A (en) * | 1971-12-13 | 1974-04-16 | Scm Corp | Glazed ceramic ware |
| CN100999415A (en) * | 2007-01-24 | 2007-07-18 | 唐山陶瓷股份有限公司 | Leadless molten block enamel for bone porcelain |
| CN102040398A (en) * | 2010-11-17 | 2011-05-04 | 广东道氏标准制釉股份有限公司 | Method for preparing polished crystal tile |
| CN102653476A (en) * | 2012-04-17 | 2012-09-05 | 陈满坚 | Three-dimensional hierarchical glazed ceramic brick and method for preparing same |
| CN102924126A (en) * | 2012-11-30 | 2013-02-13 | 山东炳坤腾泰陶瓷科技有限公司 | Milky-white frit for zirconium-free glaze and method for producing milky-white frit for zirconium-free glaze |
-
2013
- 2013-06-18 CN CN201310241465.1A patent/CN103288347B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3804666A (en) * | 1971-12-13 | 1974-04-16 | Scm Corp | Glazed ceramic ware |
| CN100999415A (en) * | 2007-01-24 | 2007-07-18 | 唐山陶瓷股份有限公司 | Leadless molten block enamel for bone porcelain |
| CN102040398A (en) * | 2010-11-17 | 2011-05-04 | 广东道氏标准制釉股份有限公司 | Method for preparing polished crystal tile |
| CN102653476A (en) * | 2012-04-17 | 2012-09-05 | 陈满坚 | Three-dimensional hierarchical glazed ceramic brick and method for preparing same |
| CN102924126A (en) * | 2012-11-30 | 2013-02-13 | 山东炳坤腾泰陶瓷科技有限公司 | Milky-white frit for zirconium-free glaze and method for producing milky-white frit for zirconium-free glaze |
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Address after: Wang Village Zhoucun District 255311 Shandong city of Zibo province Baoshan Industrial Park Shandong Bingkun tengtai ceramic Polytron Technologies Inc Applicant after: The bright female Tai-Tao porcelain Science and Technology Co., Ltd. of rising in Shandong Address before: Wang Village Zhoucun District 255311 Shandong city of Zibo province Baoshan Industrial Park Shandong Bingkun tengtai Ceramic Technology Co. Ltd. Applicant before: Shandong Bingkun Tengtai Ceramic Technology Co., Ltd. |
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Free format text: CORRECT: APPLICANT; FROM: SHANDONG BINGKUN TENGTAI CERAMICS TECHNOLOGY CO., LTD. TO: SHANDONG BINGKUN TENGTAI CERAMIC TECHNOLOGY CO., LTD. |
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Inventor after: Jiang Yuemin Inventor before: Song Fugui |
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Effective date of registration: 20180131 Address after: No. 295, government street of Yangjia temple, Wuqiao County, Cangzhou, Hebei Province Patentee after: Jiang Yuemin Address before: Wang Village Zhoucun District 255311 Shandong city of Zibo province Baoshan Industrial Park Shandong Bingkun tengtai ceramic Polytron Technologies Inc Patentee before: The bright female Tai-Tao porcelain Science and Technology Co., Ltd. of rising in Shandong |
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Effective date of registration: 20180425 Address after: 528000 Gaoming Town Industrial Park, Gaoming District, Foshan, Guangdong Patentee after: Foshan lidejia ceramic glaze Co. Ltd. Address before: 061000 No. 295 Government Street, Yangjia Temple Township, Wuqiao County, Cangzhou, Hebei Patentee before: Jiang Yuemin |
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