CN103276437A - Method for electrolytic polishing of inner wall of kettle - Google Patents

Method for electrolytic polishing of inner wall of kettle Download PDF

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Publication number
CN103276437A
CN103276437A CN2013101485113A CN201310148511A CN103276437A CN 103276437 A CN103276437 A CN 103276437A CN 2013101485113 A CN2013101485113 A CN 2013101485113A CN 201310148511 A CN201310148511 A CN 201310148511A CN 103276437 A CN103276437 A CN 103276437A
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Prior art keywords
kettle
electrolytic solution
wall
electrolytic
storage tank
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CN2013101485113A
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CN103276437B (en
Inventor
杨春辉
李勇
赵振钢
罗忠新
张艳秋
张涛
陆晓峰
闫玉良
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Huludao Huayuan Chemical Machinery Equipment Co Ltd
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Huludao Huayuan Chemical Machinery Equipment Co Ltd
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Abstract

The invention provides a method for electrolytic polishing of an inner wall of a kettle. The method is characterized in that electrodes are arranged in a kettle and an electrolyte is added into the kettle; and under the action of a power supply, an electrolyte-based polishing process is carried out so that electrolytic polishing of an inner wall of the kettle is realized. The method can improve efficiency of electrolytic polishing of the inner wall of the kettle, realize good flatness and high surface glossiness and reduces a cost. The method is suitable for electrolytic polishing of an inner surface of a kettle.

Description

A kind of inner wall of kettle electrolytic polishing method
Technical field
The present invention is to provide the inner wall of kettle finishing method of oil, chemical industry, chemical fertilizer, field of medicaments use, specifically a kind of inner wall of kettle electrolytic polishing method.
Background technology
Electropolishing is that applied metal surface selectivity anode in electrolytic solution melts and reaches polishing and a kind for the treatment of process of smooth appearance.When handling, by the control to current density, electrolytic solution viscosity and electrolyte temperature, metal is melted in electrolytic solution, pocket enters passive state and melts, and the boss activity melts, and finally reaches certain balance, by adding light agent and anodic polarization effect in the electrolytic solution, reach the purpose of leveling polishing, surface brightness can reach extreme value.Main electropolishing mechanism has the theoretical and passive film theory of mucous membrane.The smoothness of metallic surface electropolishing and thick liquid film are closely related, and luminance brightness and solid passive film are closely related.The metallic surface electropolishing can be subdivided into macroscopic view leveling and two processes of microcosmic leveling, and the variation of these two processes and anode potential is closely related, and when it reached a kind of dynamic balance state, surface brightness can reach extreme value.Compare with mechanical polishing, electropolishing can reduce the stress on metal inside and surface, and the smooth finish behind the electropolishing and planeness keep more for a long time than mechanical polishing.
At present, along with the continuous development of domestic and international electropolishing technology, the research of domestic electropolishing technology to metal works is more and more ripe, but can't realize the disposable integral electropolishing of cylindrical kettle and ellipsoidal head, especially main equipment does not have correlation technique at home as yet.
Summary of the invention
In order to realize the inner wall of kettle polishing, the present invention proposes a kind of inner wall of kettle electrolytic polishing method.This method be by will electrolytic solution pumping in the kettle after the heating, and feed direct current between pole plate and electrode axis, by the effect of electric current and the electrolytic reaction between pole plate and the electrode axis, solve the technical problem of inner wall of kettle electropolishing.
The scheme that technical solution problem of the present invention adopts is:
Electropolishing equipment: kettle is installed on the carrying roller of the commentaries on classics jar machine that drive-motor is housed, and the kettle rotation axis is installed on the support at kettle two ends; Insulcrete is housed in kettle, at insulcrete pole plate is arranged fixedly, in the kettle centre electrode axis is arranged fixedly; Kettle one end is provided with the electrolytic solution storage tank, in a side of electrolytic solution storage tank temperature control unit is housed, and is provided with transferpump in a side of electrolytic solution storage tank, and transferpump is communicated with second mouth of pipe by pipeline, at pipeline under meter is housed; Be provided with first mouth of pipe at the kettle opposite side; Be provided with housing at the kettle opposite side, housing is connected with direct supply by lead, and direct supply is connected with electrode axis with pole plate respectively by first mouth of pipe, constitutes the electrolysis loop.
Electrolytic polishing method: the electrolytic solution for preparing is poured in the electrolytic solution storage tank, starting temperature control unit heats electrolytic solution, after electrolyte temperature reaches the design temperature scope, starting transferpump pumps into electrolytic solution in the electrolytic solution storage tank, start housing and power supply, change the drive-motor of jar machine and start working, rotate kettle and make electrolytic solution in still, carry out the electropolishing reaction.
Electrolytic solution is formed: phosphoric acid quality mark 56%, sulfuric acid massfraction 40%, glycerine additive 4%, solution density 1.76-1.82 g/cm 3
Electrolyte temperature: 55~65 ℃;
Kettle rotating speed: 〉=0.05~0.1RPM;
Direct supply voltage: 8V;
Direct supply electric current: 15~50 amperes/square decimeter;
Plate material: stereotype;
Electrode axis material: stainless steel or tetrafluoroethylene.
Positively effect, method of the present invention can be realized electropolishing in the kettle, and the efficient height, and planeness is good, and the surface smoothness height reduces cost.Suitable method as still class implements internal surface electropolishing is used.
Description of drawings
Fig. 1 is structure iron of the present invention
Among the figure, 1. electrolytic solution storage tank, 2. transferpump, 3. under meter, 4. kettle, 5. insulcrete, 6. pole plate, 7. electrode axis, 8. direct supply, 9. housing, 10. support, 11. change jar machines, 12. drive-motor, 13. first mouths of pipe, 14. second mouths of pipe, 15. temperature control units.
Embodiment
Electropolishing equipment: as shown in the figure, kettle 4 is installed on the carrying roller of the commentaries on classics jar machine 11 that drive-motor 12 is housed, and the kettle rotation axis is installed on the support 10 at kettle two ends; Insulcrete 5 is housed in kettle, at insulcrete pole plate 6 is arranged fixedly, in the kettle centre electrode axis 7 is arranged fixedly; Kettle one end is provided with electrolytic solution storage tank 1, in a side of electrolytic solution storage tank temperature control unit 15 is housed, and is provided with transferpump 2 in a side of electrolytic solution storage tank, and transferpump is communicated with second mouth of pipe 14 by pipeline, at pipeline under meter 3 is housed; Be provided with first mouth of pipe 13 at the kettle opposite side; Be provided with housing 9 at the kettle opposite side, housing is connected with direct supply 8 by lead, and direct supply is connected with electrode axis with pole plate respectively by first mouth of pipe, constitutes the electrolysis loop.
Electrolytic polishing method: the electrolytic solution for preparing is poured in the electrolytic solution storage tank, starting temperature control unit heats electrolytic solution, after electrolyte temperature reaches the design temperature scope, starting transferpump pumps into electrolytic solution in the electrolytic solution storage tank, start housing and power supply, change the drive-motor of jar machine and start working, rotate kettle and make electrolytic solution in still, carry out the electropolishing reaction.
Electrolytic solution is formed: phosphoric acid quality mark 56%, sulfuric acid massfraction 40%, glycerine additive 4%, solution density 1.76-1.82 g/cm 3
Electrolyte temperature: 55~65 ℃;
Kettle rotating speed: 〉=0.05~0.1RPM;
Direct supply voltage: 8V;
Direct supply electric current: 15~50 amperes/square decimeter;
Plate material: stereotype;
Electrode axis material: stainless steel or tetrafluoroethylene.
Characteristics:
The present invention is by carrying out electropolishing to kettle right cylinder and two ends elipse head internal surface, can realize the disposable electropolishing of main equipment or complicated inner surface, have high-level efficiency, high-precision advantage, and electrolytic solution can repeated multiple times use, reduce cost and labour intensity, enhance productivity and quality of finish, reduce pollution emissions.

Claims (5)

1. inner wall of kettle electrolytic polishing method is characterized in that:
Electropolishing equipment: kettle (4) is installed on the carrying roller of the commentaries on classics jar machine (11) that drive-motor (12) is housed, and the kettle rotation axis is installed on the support (10) at kettle two ends; Insulcrete (5) is housed in kettle, at insulcrete pole plate (6) is arranged fixedly, electrode axis (7) is fixedly arranged in the kettle centre; Kettle one end is provided with electrolytic solution storage tank (1), side at the electrolytic solution storage tank is equipped with temperature control unit (15), side at the electrolytic solution storage tank is provided with transferpump (2), and transferpump is communicated with second mouth of pipe (14) by pipeline, at pipeline under meter (3) is housed; Be provided with first mouth of pipe (13) at the reactor opposite side; Be provided with housing (9) at the reactor opposite side, housing is connected with direct supply (8) by lead, and direct supply is connected with electrode axis with pole plate respectively by first mouth of pipe, constitutes the electrolysis loop;
Electrolytic polishing method: the electrolytic solution for preparing is poured in the electrolytic solution storage tank, starting temperature control unit heats electrolytic solution, after electrolyte temperature reaches the design temperature scope, starting transferpump pumps into electrolytic solution in the electrolytic solution storage tank, start housing and power supply, change the drive-motor of jar machine and start working, rotate kettle and make electrolytic solution in still, carry out the electropolishing reaction.
2. a kind of inner wall of kettle electrolytic polishing method according to claim 1 is characterized in that: electrolytic solution composition: phosphoric acid quality mark 56%, sulfuric acid massfraction 40%, glycerine additive 4%, solution density 1.76-1.82 g/cm 3
3. a kind of inner wall of kettle electrolytic polishing method according to claim 1 is characterized in that: electrolyte temperature: 55~65 ℃; Reactor rotating speed: 〉=0.05~0.1rpm.
4. a kind of inner wall of kettle electrolytic polishing method according to claim 1 is characterized in that: electrolysis voltage: 8V; Electric current: 15~50 amperes/square decimeter.
5. a kind of inner wall of kettle electrolytic polishing method according to claim 1, it is characterized in that: the material of pole plate is stereotype; The electrode axis material is stainless steel or tetrafluoroethylene.
CN201310148511.3A 2013-04-26 2013-04-26 A kind of inner wall of kettle electrolytic polishing method Active CN103276437B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105297128A (en) * 2015-11-05 2016-02-03 佛山市南海区鑫恒力五金机械厂 Horizontal electrolytic decoating line production device
CN106048706A (en) * 2016-08-17 2016-10-26 沈阳航天新光集团有限公司 Electrochemical polishing tool for inner holes of stainless steel parts
CN106400100A (en) * 2016-10-18 2017-02-15 湖北帕尔森机电设备有限公司 Full-automatic electropolishing equipment
CN109056048A (en) * 2018-07-05 2018-12-21 刘素兰 Stainless steel pipe inner surface electrochemical polish system of processing and its application method

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4156637A (en) * 1977-03-15 1979-05-29 Jumer John F Method for electro-processing large vessels
JPS57198299A (en) * 1981-05-29 1982-12-04 Hitachi Ltd Electrolytic polishing method for inside surface of vessel
JP2003266246A (en) * 2002-03-12 2003-09-24 Kansan Corp Electrolytic composite polishing device, electrolytic composite polishing tool, and electrolytic composite polishing method
CN201581151U (en) * 2009-12-01 2010-09-15 广州中国科学院工业技术研究院 Electrochemical polishing treatment device for internal surface and external surface of metal workpiece
CN102586855A (en) * 2012-03-30 2012-07-18 河北省安装工程公司 Electrochemical and mechanical composite polishing device
CN102703963A (en) * 2011-03-28 2012-10-03 上海迈诺光洁工贸有限公司 Movable electrode (cathode) for stainless steel inner tube electropolishing
CN202572021U (en) * 2012-03-30 2012-12-05 河北省安装工程公司 Electrochemical and mechanical compound polishing device

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4156637A (en) * 1977-03-15 1979-05-29 Jumer John F Method for electro-processing large vessels
JPS57198299A (en) * 1981-05-29 1982-12-04 Hitachi Ltd Electrolytic polishing method for inside surface of vessel
JP2003266246A (en) * 2002-03-12 2003-09-24 Kansan Corp Electrolytic composite polishing device, electrolytic composite polishing tool, and electrolytic composite polishing method
CN201581151U (en) * 2009-12-01 2010-09-15 广州中国科学院工业技术研究院 Electrochemical polishing treatment device for internal surface and external surface of metal workpiece
CN102703963A (en) * 2011-03-28 2012-10-03 上海迈诺光洁工贸有限公司 Movable electrode (cathode) for stainless steel inner tube electropolishing
CN102586855A (en) * 2012-03-30 2012-07-18 河北省安装工程公司 Electrochemical and mechanical composite polishing device
CN202572021U (en) * 2012-03-30 2012-12-05 河北省安装工程公司 Electrochemical and mechanical compound polishing device

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
张允诚等: "《电镀手册》", 31 January 2007, 国防工业出版社 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105297128A (en) * 2015-11-05 2016-02-03 佛山市南海区鑫恒力五金机械厂 Horizontal electrolytic decoating line production device
CN106048706A (en) * 2016-08-17 2016-10-26 沈阳航天新光集团有限公司 Electrochemical polishing tool for inner holes of stainless steel parts
CN106400100A (en) * 2016-10-18 2017-02-15 湖北帕尔森机电设备有限公司 Full-automatic electropolishing equipment
CN109056048A (en) * 2018-07-05 2018-12-21 刘素兰 Stainless steel pipe inner surface electrochemical polish system of processing and its application method

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