CN103224565B - 利用秸秆制备印花糊料用的羧甲基纤维素的方法 - Google Patents
利用秸秆制备印花糊料用的羧甲基纤维素的方法 Download PDFInfo
- Publication number
- CN103224565B CN103224565B CN201310152152.9A CN201310152152A CN103224565B CN 103224565 B CN103224565 B CN 103224565B CN 201310152152 A CN201310152152 A CN 201310152152A CN 103224565 B CN103224565 B CN 103224565B
- Authority
- CN
- China
- Prior art keywords
- carboxymethyl cellulose
- add
- printing gum
- straw
- stalk
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000007639 printing Methods 0.000 title claims abstract description 34
- 229920002134 Carboxymethyl cellulose Polymers 0.000 title claims abstract description 33
- 239000001768 carboxy methyl cellulose Substances 0.000 title claims abstract description 33
- 235000010948 carboxy methyl cellulose Nutrition 0.000 title claims abstract description 33
- 239000008112 carboxymethyl-cellulose Substances 0.000 title claims abstract description 33
- 239000010902 straw Substances 0.000 title claims abstract description 27
- 238000000034 method Methods 0.000 title claims abstract description 20
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 51
- 239000007787 solid Substances 0.000 claims abstract description 18
- 238000006243 chemical reaction Methods 0.000 claims abstract description 16
- FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical compound OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 claims abstract description 15
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 14
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000005406 washing Methods 0.000 claims abstract description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000005956 quaternization reaction Methods 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 229960000583 acetic acid Drugs 0.000 claims abstract description 7
- 239000012362 glacial acetic acid Substances 0.000 claims abstract description 7
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 7
- 239000000843 powder Substances 0.000 claims abstract description 7
- 238000010298 pulverizing process Methods 0.000 claims abstract description 7
- LRWZZZWJMFNZIK-UHFFFAOYSA-N 2-chloro-3-methyloxirane Chemical compound CC1OC1Cl LRWZZZWJMFNZIK-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 16
- 229940106681 chloroacetic acid Drugs 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 6
- 230000009467 reduction Effects 0.000 claims description 5
- 241000209140 Triticum Species 0.000 claims description 4
- 235000021307 Triticum Nutrition 0.000 claims description 4
- 240000007594 Oryza sativa Species 0.000 claims description 3
- 235000007164 Oryza sativa Nutrition 0.000 claims description 3
- 235000014676 Phragmites communis Nutrition 0.000 claims description 3
- 240000008042 Zea mays Species 0.000 claims description 3
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims description 3
- 235000009566 rice Nutrition 0.000 claims description 3
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims description 2
- 235000005822 corn Nutrition 0.000 claims description 2
- 238000006467 substitution reaction Methods 0.000 abstract description 5
- 238000006266 etherification reaction Methods 0.000 abstract description 2
- 239000008186 active pharmaceutical agent Substances 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical group CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 description 4
- 229920002678 cellulose Polymers 0.000 description 4
- 239000001913 cellulose Substances 0.000 description 4
- 239000000661 sodium alginate Substances 0.000 description 4
- 235000010413 sodium alginate Nutrition 0.000 description 4
- 229940005550 sodium alginate Drugs 0.000 description 4
- 239000002562 thickening agent Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 244000303965 Cyamopsis psoralioides Species 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 1
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 229920006321 anionic cellulose Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 description 1
- 230000007071 enzymatic hydrolysis Effects 0.000 description 1
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 235000009973 maize Nutrition 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Landscapes
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310152152.9A CN103224565B (zh) | 2013-04-27 | 2013-04-27 | 利用秸秆制备印花糊料用的羧甲基纤维素的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310152152.9A CN103224565B (zh) | 2013-04-27 | 2013-04-27 | 利用秸秆制备印花糊料用的羧甲基纤维素的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103224565A CN103224565A (zh) | 2013-07-31 |
CN103224565B true CN103224565B (zh) | 2016-01-20 |
Family
ID=48835224
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310152152.9A Active CN103224565B (zh) | 2013-04-27 | 2013-04-27 | 利用秸秆制备印花糊料用的羧甲基纤维素的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103224565B (zh) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103788214B (zh) * | 2014-01-17 | 2015-12-30 | 甘肃高歌伟业新材料科技有限公司 | 以秸秆为原料制备耐电解质印花糊料的方法 |
CN103938469A (zh) * | 2014-04-17 | 2014-07-23 | 苏州润弘贸易有限公司 | 一种亚麻织物活性印染糊料的制备方法 |
CN105218686A (zh) * | 2015-10-20 | 2016-01-06 | 湖州博仁纺织品有限公司 | 一种新型活性染料印花用增稠剂的制备方法 |
CN110981975A (zh) * | 2019-11-28 | 2020-04-10 | 泸州北方纤维素有限公司 | 提高羟乙基纤维素粘度的方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2096417C1 (ru) * | 1991-12-02 | 1997-11-20 | Конструкторско-Технологическое Бюро Технических Средств Бурения Скважин | Способ получения натрийкарбоксиметилцеллюлозы |
CN101463091A (zh) * | 2009-01-16 | 2009-06-24 | 中国科学院过程工程研究所 | 秸秆羧甲基化组分分离及制备秸秆羧甲基纤维素的方法 |
CN101475696A (zh) * | 2008-12-09 | 2009-07-08 | 丹尼斯克(张家港)亲水胶体有限公司 | 特高粘羧甲基纤维素钠的制备方法 |
CN101985479A (zh) * | 2010-12-10 | 2011-03-16 | 西北师范大学 | 小麦秸秆羧甲基纤维素的制备和应用 |
CN102887956A (zh) * | 2012-10-22 | 2013-01-23 | 河北业之源化工有限公司 | 一种制备技术级高粘度高抗盐性羧甲基纤维素钠的方法 |
-
2013
- 2013-04-27 CN CN201310152152.9A patent/CN103224565B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2096417C1 (ru) * | 1991-12-02 | 1997-11-20 | Конструкторско-Технологическое Бюро Технических Средств Бурения Скважин | Способ получения натрийкарбоксиметилцеллюлозы |
CN101475696A (zh) * | 2008-12-09 | 2009-07-08 | 丹尼斯克(张家港)亲水胶体有限公司 | 特高粘羧甲基纤维素钠的制备方法 |
CN101463091A (zh) * | 2009-01-16 | 2009-06-24 | 中国科学院过程工程研究所 | 秸秆羧甲基化组分分离及制备秸秆羧甲基纤维素的方法 |
CN101985479A (zh) * | 2010-12-10 | 2011-03-16 | 西北师范大学 | 小麦秸秆羧甲基纤维素的制备和应用 |
CN102887956A (zh) * | 2012-10-22 | 2013-01-23 | 河北业之源化工有限公司 | 一种制备技术级高粘度高抗盐性羧甲基纤维素钠的方法 |
Also Published As
Publication number | Publication date |
---|---|
CN103224565A (zh) | 2013-07-31 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103410019B (zh) | 复合印花糊料的制备方法 | |
CN103224565B (zh) | 利用秸秆制备印花糊料用的羧甲基纤维素的方法 | |
CN103790038B (zh) | 以淀粉为原料制备活性印花糊料的方法 | |
CN102775506B (zh) | 一种采用亚糊化技术制备辛烯基琥珀酸木薯淀粉酯的方法 | |
CN1911966B (zh) | 一种淀粉预处理方法 | |
CN103755816B (zh) | 一种羧甲基纤维素钠的制备方法 | |
CN107142750A (zh) | 一种分散染料印花用复合糊料的制备方法 | |
CN101857639B (zh) | 用玉米秸秆生产生物丁醇的残渣制备羧甲基纤维素钠的方法 | |
CN103924457B (zh) | 一种印染糊料的生产工艺 | |
CN104831562A (zh) | 羟丙基羧甲基蜡质玉米淀粉酸性染料印花糊料及制备方法 | |
CN103554273B (zh) | 技术级羧甲基纤维素钠的生产方法 | |
CN107692001A (zh) | 一种吐浆率低且不易断的米粉条的制备方法 | |
CN104452345A (zh) | 一种仿蜡染用印花糊料 | |
CN105218686A (zh) | 一种新型活性染料印花用增稠剂的制备方法 | |
CN102964457A (zh) | 一种脱支交联预糊化淀粉及其制备方法 | |
CN109023998B (zh) | 一种安全环保的印花糊料及其制备方法 | |
CN103788214B (zh) | 以秸秆为原料制备耐电解质印花糊料的方法 | |
CN105693872B (zh) | 一种抗盐性羧甲基淀粉的制备方法 | |
CN103131350B (zh) | 一种熟胶粉及其制备方法 | |
CN103938469A (zh) | 一种亚麻织物活性印染糊料的制备方法 | |
CN105481987A (zh) | 一种利用小麦b淀粉制备预糊化淀粉的方法 | |
CN102690362B (zh) | 一种氧化交联-羧甲基复合变性淀粉的制备方法及氧化交联-羧甲基复合变性淀粉 | |
CN101974100B (zh) | 一种复合改性瓜尔胶及其制备方法 | |
CN1490337A (zh) | 超高粘度羧甲基淀粉钠及其制备方法 | |
CN102212142B (zh) | 一种三重变性淀粉的干法制备工艺 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Method for preparing carboxymethyl cellulose used in printing paste by using straws Effective date of registration: 20170427 Granted publication date: 20160120 Pledgee: Dingxi Anding Fengcheng Construction Management Co., Ltd. Pledgor: GANSU SHENGDAFANGZHOU POTATO MODIFIED STARCH Co.,Ltd. Registration number: 2017620000013 |
|
PP01 | Preservation of patent right |
Effective date of registration: 20200623 Granted publication date: 20160120 |
|
PP01 | Preservation of patent right | ||
PD01 | Discharge of preservation of patent |
Date of cancellation: 20230623 Granted publication date: 20160120 |
|
PD01 | Discharge of preservation of patent | ||
PP01 | Preservation of patent right |
Effective date of registration: 20230623 Granted publication date: 20160120 |
|
PP01 | Preservation of patent right |