CN103214170A - Method for toughening 4.0mm toughened glass - Google Patents

Method for toughening 4.0mm toughened glass Download PDF

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Publication number
CN103214170A
CN103214170A CN2013101209185A CN201310120918A CN103214170A CN 103214170 A CN103214170 A CN 103214170A CN 2013101209185 A CN2013101209185 A CN 2013101209185A CN 201310120918 A CN201310120918 A CN 201310120918A CN 103214170 A CN103214170 A CN 103214170A
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CN
China
Prior art keywords
glass
temperature
minute
toughened
interval
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2013101209185A
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Chinese (zh)
Inventor
张百庆
韩立平
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HEFEI CHENGXIN GLASS CO Ltd
Original Assignee
HEFEI CHENGXIN GLASS CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HEFEI CHENGXIN GLASS CO Ltd filed Critical HEFEI CHENGXIN GLASS CO Ltd
Priority to CN2013101209185A priority Critical patent/CN103214170A/en
Publication of CN103214170A publication Critical patent/CN103214170A/en
Pending legal-status Critical Current

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/50Glass production, e.g. reusing waste heat during processing or shaping
    • Y02P40/57Improving the yield, e-g- reduction of reject rates

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  • Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
  • Surface Treatment Of Glass (AREA)

Abstract

The invention discloses a method for toughening a piece of 4.0mm toughened glass. The method comprises the following steps of horizontally placing the glass to be processed onto a roller bed, delivering the glass into a passage-type toughening furnace through the roller bed, sequentially conducting heat treatment on the glass at intervals, and cooling the glass through high-pressure air until the surface temperature of the glass reaches 310 to 330 DEG C; placing the glass into 18 to 25 percent potassium nitrate glycerol solution at the temperature of 150 to 160 DEG C to be cooled for 4 to 5 minutes; reheating the glass to the temperature of 260 to 290 DEG C for 4 to 5 minutes; and taking out the glass to be slowly cooled in the air. Through the interval heating and cold treatment, the stress distribution on the surface of the glass is adjusted, and the flatness of the toughened glass is guaranteed; and through treatment of the potassium nitrate glycerol solution, reheating and slow cooling, the toughened degree of the glass surface is increased, the self cracking possibility of the glass in the cooling process is reduced, the yield of finished product of the toughened glass is increased, and the performance index requirement of the toughened glass can be met.

Description

4.0mm the tempering processing method of toughened glass
Technical field
The invention belongs to the glass preparation field, be specifically related to the preparation technology of toughened glass.
Technical background
Toughened glass makes it be widely used owing to have higher mechanical strength, good heatproof acute degeneration, good advantages such as security.It is the steel process of heat-eliminating medium that existing toughened glass production process adopts mostly with the air, makes to be heated glass and to carry out Quench at short notice by a large amount of air and handle, thereby finishes the tempering process.In order to guarantee the performance of toughened glass, the air of very big flow need be provided in very short time usually, especially more obvious when tempering approaches glass, select for use the high-power blower of high blast, big flow to dry simultaneously usually.
At present the mode of glass tempering also has the chemical tempering mode, and chemically toughened glass intensity and physical toughened glass are approaching, but overlong time, the low and production cost height of efficient.
Summary of the invention
The tempering processing method that the purpose of this invention is to provide a kind of 4.0mm toughened glass, glass surface stress are evenly, sinuousness, fragment, degree of the temper all meet the requirements.
Technical solution of the present invention is as follows:
4.0 the tempering processing method of mm toughened glass is characterized in that may further comprise the steps:
(1), just the bath of glass placing flat is delivered in the channel-type annealing furnace by roller-way to roller-way, heat-treat successively by the interval:
First interval: temperature 250-300 ℃, time 3-4 minute; Second interval: temperature 400-450 ℃, time 4-5 minute; The 3rd interval: temperature 250-300 ℃, time 4-5 minute; The 4th interval: temperature 550-600 ℃, time 3-4 minute; The 5th interval: temperature 650-700 ℃, time 5-6 minute;
(2), adopt high-pressure blast to be cooled to 310-330 ℃ of glass surface temperature;
(3), glass was added 150-160 ℃, the cooling of the saltpetre glycerine solution of 18-25% 4-5 minute;
(4), glass is reheated to 260-290 ℃ time 4-5 minute;
(5), take out in the glass air slow cooling but.
The present invention is by adopting by stages heating, deepfreeze, regulate the glass surface stress distribution, guaranteed the planeness of toughened glass, by the saltpetre glycerine solution, reheat, slow cooling handles, increased the degree of the temper of glass surface, reduce the probability that glass is revealed in process of cooling, improved the yield rate of toughened glass, satisfied the performance index requirement of toughened glass.
Embodiment
4.0 the tempering processing method of mm toughened glass comprises and carries out following steps successively:
(1), just the bath of glass placing flat is delivered in the channel-type annealing furnace by roller-way to roller-way, heat-treat successively by the interval:
First interval: temperature 280-300 ℃, time 3-4 minute; Second interval: temperature 430-450 ℃, time 4-5 minute; The 3rd interval: temperature 280-300 ℃, time 4-5 minute; The 4th interval: temperature 580-600 ℃, time 3-4 minute; The 5th interval: temperature 670-700 ℃, time 5-6 minute;
(2), adopt high-pressure blast to be cooled to 320-330 ℃ of glass surface temperature;
(3), glass was added 150-160 ℃, the cooling of 18% saltpetre glycerine solution 5 minutes;
(4), glass is reheated to 280-290 ℃ soaking time 4-5 minute;
(5), take out in the glass air slow cooling but.
The toughened glass that processes is detected, and its sinuousness reaches 0.8 ‰, 55 of 50 * 50mm internal fragments, conformance with standard; Degree of the temper=3.5N/cm, the self-destruction rate is 1 ~ 3 ‰.

Claims (1)

1.4.0 the tempering processing method of mm toughened glass is characterized in that may further comprise the steps:
(1), just the bath of glass placing flat is delivered in the channel-type annealing furnace by roller-way to roller-way, heat-treat successively by the interval:
First interval: temperature 250-300 ℃, time 3-4 minute; Second interval: temperature 400-450 ℃, time 4-5 minute; The 3rd interval: temperature 250-300 ℃, time 4-5 minute; The 4th interval: temperature 550-600 ℃, time 3-4 minute; The 5th interval: temperature 650-700 ℃, time 5-6 minute;
(2), adopt high-pressure blast to be cooled to 310-330 ℃ of glass surface temperature;
(3), glass was added 150-160 ℃, the cooling of the saltpetre glycerine solution of 18-25% 4-5 minute;
(4), glass is reheated to 260-290 ℃ time 4-5 minute;
(5), take out in the glass air slow cooling but.
CN2013101209185A 2013-04-09 2013-04-09 Method for toughening 4.0mm toughened glass Pending CN103214170A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2013101209185A CN103214170A (en) 2013-04-09 2013-04-09 Method for toughening 4.0mm toughened glass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2013101209185A CN103214170A (en) 2013-04-09 2013-04-09 Method for toughening 4.0mm toughened glass

Publications (1)

Publication Number Publication Date
CN103214170A true CN103214170A (en) 2013-07-24

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN2013101209185A Pending CN103214170A (en) 2013-04-09 2013-04-09 Method for toughening 4.0mm toughened glass

Country Status (1)

Country Link
CN (1) CN103214170A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104045229A (en) * 2014-07-01 2014-09-17 福建省港达玻璃制品有限公司 Preparation process of tempered glass

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1824619A (en) * 2006-03-17 2006-08-30 中国建筑材料科学研究院 Preparation method of air strengthened glass
US7367205B1 (en) * 2001-09-19 2008-05-06 Boaz Premakaran T System for simultaneously heating and cooling glass
CN102730952A (en) * 2012-06-29 2012-10-17 都匀开发区福田化工有限责任公司 Glass tempering furnace and glass tempering method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7367205B1 (en) * 2001-09-19 2008-05-06 Boaz Premakaran T System for simultaneously heating and cooling glass
CN1824619A (en) * 2006-03-17 2006-08-30 中国建筑材料科学研究院 Preparation method of air strengthened glass
CN102730952A (en) * 2012-06-29 2012-10-17 都匀开发区福田化工有限责任公司 Glass tempering furnace and glass tempering method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
上海市硅酸盐学会: "《玻璃译丛 第5辑》", 31 December 1964, article "玻璃的表面钢化" *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104045229A (en) * 2014-07-01 2014-09-17 福建省港达玻璃制品有限公司 Preparation process of tempered glass
CN104045229B (en) * 2014-07-01 2016-06-22 福建省港达玻璃制品有限公司 A kind of preparation technology of safety glass

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Application publication date: 20130724

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