CN103205891A - Preparation method of negative oxygen ion and chitosan finishing agent, and cloth finishing method using negative oxygen ion and chitosan finishing agent - Google Patents
Preparation method of negative oxygen ion and chitosan finishing agent, and cloth finishing method using negative oxygen ion and chitosan finishing agent Download PDFInfo
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- CN103205891A CN103205891A CN2013100955111A CN201310095511A CN103205891A CN 103205891 A CN103205891 A CN 103205891A CN 2013100955111 A CN2013100955111 A CN 2013100955111A CN 201310095511 A CN201310095511 A CN 201310095511A CN 103205891 A CN103205891 A CN 103205891A
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- oxygen ion
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- negative oxygen
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Abstract
The invention discloses a preparation method of negative oxygen ion and chitosan finishing agent, and a cloth finishing method using the negative oxygen ion and chitosan finishing agent. The preparation method includes the steps of using 5000-mesh natural tourmaline superfine powder as the powder to be milled, milling the powder into 12500-mesh powder by a high-pressure jet mill, mixing the components, and well mixing at 25-90 DEG C for 30-60 minutes to obtain homogeneous negative oxygen ion and chitosan finishing agent. The components include, by weight, 1-5 parts of tourmaline powder to be milled, and 0.3-5 parts of chitosan with 4.5-400,000 molecular weight and 3-5 pH value. The preparation method is convenient to operate, the concentration of produced negative ions is high, and the negative oxygen ion and chitosan finishing agent is well antibacterial.
Description
Technical field
The present invention relates to a kind of finishing agent, be specifically related to a kind of preparation method and fabric finishing method for negative oxygen ion and shitosan health care antibacterial environment protection fabric finishing agent.
Background technology
Raising along with people's living standard, people require more and more higher to security performance and the environmental-protecting performance of fabric, anionic finishing agent is widely applied in the fabric because having anti-microbial property, and shitosan is a kind of compound of polycation type, under acid condition, have higher positive charge, fiber there is good affinity, molecular weight is that shitosan content about 1% in fabric of 4.5-40 ten thousand just has the excellent antibiotic effect, it is the natural antibacterial agent of environmental protection, and shitosan can also be as surface coating, adhesive tightly is combined in fabric face by the anion nanometer material, has strengthened washable and lasting effect, thereby gives fabric higher anti-microbial property.
Summary of the invention
Goal of the invention: the present invention is in order to solve the deficiencies in the prior art, provides a kind of and can produce negative oxygen ion that a large amount of anions again can be antibiotic and the preparation method of shitosan finishing agent, and another object of the present invention has provided corresponding fabric finishing method.
Technical scheme: the preparation method of a kind of negative oxygen ion and shitosan finishing agent, comprise the following steps: natural Tourmaline powder 5000 order superfines to treating the powder powder, be crushed to 12500 orders with the high pressure draught pulverizer, following component is mixed according to parts by weight: the Tourmaline powder 1-5 part after the pulverizing, molecular weight is that the shitosan pH value of 4.5-40 ten thousand is 3-5,0.3-5 part, be under 25-90 ℃ in reaction temperature, evenly stir negative oxygen ion and shitosan finishing agent that 30-60min obtains homogeneous.
In order to realize another object of the present invention, provide following technical scheme: the fabric finishing method of a kind of negative oxygen ion and shitosan finishing agent, fabric to be put in order and described finishing agent bath raio are that 1:10-50 puts in order, fabric after the arrangement is put into the alkali lye that PH is 10-12, make fabric reach neutral.
As preferably, the fabric of handling well is dried under 90-130 ℃ temperature, get final product.
As preferably, the particle diameter of the Tourmaline powder after the pulverizing is less than 1 micron.
Beneficial effect: the present invention compares with existing technology, Tourmaline powder and shitosan is used, and wraps up film coating technique with shitosan, and made finishing agent is easy to operate, and the negative oxygen ion concentration of generation is big, has excellent antibiotic performance and washability.
The specific embodiment
The present invention will be described in detail below in conjunction with specific embodiment.
Specific embodiment 1:
The preparation method of a kind of negative oxygen ion and shitosan finishing agent, comprise the following steps: natural Tourmaline powder 5000 order superfines to treating the powder powder, be crushed to 12500 orders with the high pressure draught pulverizer, Tourmaline powder footpath after feasible the pulverizing is less than 1 micron, following component is mixed according to parts by weight: 1 part in the Tourmaline powder after the pulverizing, pH value is 3, molecular weight is 0.3 part of the shitosan of 4.5-40 ten thousand, be under 25 ℃ in reaction temperature, evenly stir negative oxygen ion and shitosan finishing agent that 30min obtains homogeneous.
The fabric finishing method of negative oxygen ion and shitosan finishing agent among the present invention, fabric to be put in order and described finishing agent bath raio are that 1:10 puts in order, fabric after the arrangement is put into the alkali lye that PH is 10-12, make fabric reach neutral, then the fabric of handling well is dried under 90 ℃ temperature, get final product.
Specific embodiment 2:
The preparation method of a kind of negative oxygen ion and shitosan finishing agent, comprise the following steps: natural Tourmaline powder 5000 order superfines to treating the powder powder, be crushed to 12500 orders with the high pressure draught pulverizer, Tourmaline powder footpath after feasible the pulverizing is less than 1 micron, following component is mixed according to parts by weight: 4 parts in the Tourmaline powder after the pulverizing, pH value is 4, molecular weight is 4 parts of the shitosans of 4.5-40 ten thousand, be under 70 ℃ in reaction temperature, evenly stir negative oxygen ion and shitosan finishing agent that 40min obtains homogeneous.
The fabric finishing method of negative oxygen ion and shitosan finishing agent among the present invention, fabric to be put in order and described finishing agent bath raio are that 1:30 puts in order, it is 11 alkali lye that fabric after the arrangement is put into PH, make fabric reach neutral, then the fabric of handling well is dried under 100 ℃ temperature, get final product.
Specific embodiment 3:
The preparation method of a kind of negative oxygen ion and shitosan finishing agent, comprise the following steps: natural Tourmaline powder 5000 order superfines to treating the powder powder, be crushed to 12500 orders with the high pressure draught pulverizer, Tourmaline powder footpath after feasible the pulverizing is less than 1 micron, following component is mixed according to parts by weight: 5 parts in the Tourmaline powder after the pulverizing, pH value is 5, molecular weight is 5 parts of the shitosans of 4.5-40 ten thousand, be under 90 ℃ in reaction temperature, evenly stir negative oxygen ion and shitosan finishing agent that 60min obtains homogeneous.
The fabric finishing method of negative oxygen ion and shitosan finishing agent among the present invention, fabric to be put in order and described finishing agent bath raio are that 1:50 puts in order, it is 12 alkali lye that fabric after the arrangement is put into PH, make fabric reach neutral, then the fabric of handling well is dried under 130 ℃ temperature, get final product.
Claims (4)
1. the preparation method of a negative oxygen ion and shitosan finishing agent, comprise the following steps: natural Tourmaline powder 5000 order superfines to treating the powder powder, be crushed to 12500 orders with the high pressure draught pulverizer, it is characterized in that: following component is mixed according to parts by weight: the Tourmaline powder 1-5 part after the pulverizing, molecular weight is that the shitosan pH value of 4.5-40 ten thousand is 3-5,0.3-5 part, be under 25-90 ℃ in reaction temperature, evenly stir negative oxygen ion and shitosan finishing agent that 30-60min obtains homogeneous.
2. the fabric finishing method of a negative oxygen ion and shitosan finishing agent, it is characterized in that: fabric to be put in order and described finishing agent bath raio are that 1:10-50 puts in order, and the fabric after the arrangement is put into the alkali lye that PH is 10-12, make fabric reach neutral.
3. the fabric finishing method of negative oxygen ion as claimed in claim 2 and shitosan finishing agent is characterized in that: the fabric of handling well is dried under 90-130 ℃ temperature, get final product.
4. the preparation method of negative oxygen ion as claimed in claim 1 and shitosan finishing agent, it is characterized in that: the particle diameter of the Tourmaline powder after the pulverizing is less than 1 micron.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310095511.1A CN103205891B (en) | 2013-03-25 | 2013-03-25 | Preparation method of negative oxygen ion and chitosan finishing agent, and cloth finishing method using negative oxygen ion and chitosan finishing agent |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310095511.1A CN103205891B (en) | 2013-03-25 | 2013-03-25 | Preparation method of negative oxygen ion and chitosan finishing agent, and cloth finishing method using negative oxygen ion and chitosan finishing agent |
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| CN103205891A true CN103205891A (en) | 2013-07-17 |
| CN103205891B CN103205891B (en) | 2015-03-04 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103572587A (en) * | 2013-11-13 | 2014-02-12 | 新疆大学 | Antibacterial health-care lambsdown tourmaline sleep bedding and health-care product |
| CN103590237A (en) * | 2013-11-11 | 2014-02-19 | 新疆大学 | Tourmaline antibacterial health-care heat-bonded wadding |
| CN106012569A (en) * | 2016-06-13 | 2016-10-12 | 浙江鑫龙彩印包装有限公司 | Canvas with slow negative ion releasing function and manufacturing method thereof |
| CN109576988A (en) * | 2018-11-22 | 2019-04-05 | 辽东学院 | A kind of negative oxygen-ion, far infrared silk tussah fibre finishing fluid, negative oxygen-ion, far infrared silk tussah fibre and preparation method thereof |
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| CN101476240A (en) * | 2008-01-03 | 2009-07-08 | 深圳宝利时尚科技有限公司 | Textile finishing agent with thermal protecting, antibacterial and moisture-keeping functions, and health socks using the same |
| CN101871139A (en) * | 2010-06-25 | 2010-10-27 | 上海心动材料科技有限公司 | Far infrared anionic magnetic fiber and manufacturing method thereof |
| CN102273742A (en) * | 2011-09-01 | 2011-12-14 | 丁一 | Nano chitin element anionic far-infrared antibacterial, anti-mite and electromagnetic wave preventing student's wear |
| CN102808328A (en) * | 2012-08-29 | 2012-12-05 | 紫罗兰家纺科技股份有限公司 | Anion finishing agent and preparation method thereof |
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2013
- 2013-03-25 CN CN201310095511.1A patent/CN103205891B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101476240A (en) * | 2008-01-03 | 2009-07-08 | 深圳宝利时尚科技有限公司 | Textile finishing agent with thermal protecting, antibacterial and moisture-keeping functions, and health socks using the same |
| CN101871139A (en) * | 2010-06-25 | 2010-10-27 | 上海心动材料科技有限公司 | Far infrared anionic magnetic fiber and manufacturing method thereof |
| CN102273742A (en) * | 2011-09-01 | 2011-12-14 | 丁一 | Nano chitin element anionic far-infrared antibacterial, anti-mite and electromagnetic wave preventing student's wear |
| CN102808328A (en) * | 2012-08-29 | 2012-12-05 | 紫罗兰家纺科技股份有限公司 | Anion finishing agent and preparation method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103590237A (en) * | 2013-11-11 | 2014-02-19 | 新疆大学 | Tourmaline antibacterial health-care heat-bonded wadding |
| CN103590237B (en) * | 2013-11-11 | 2018-09-18 | 新疆大学 | Tourmaline antibiotic health care heats flocculus |
| CN103572587A (en) * | 2013-11-13 | 2014-02-12 | 新疆大学 | Antibacterial health-care lambsdown tourmaline sleep bedding and health-care product |
| CN103572587B (en) * | 2013-11-13 | 2018-09-18 | 新疆大学 | Tourmaline antibiotic health care camel's hair sleeps bedroom and healthy shield product |
| CN106012569A (en) * | 2016-06-13 | 2016-10-12 | 浙江鑫龙彩印包装有限公司 | Canvas with slow negative ion releasing function and manufacturing method thereof |
| CN109576988A (en) * | 2018-11-22 | 2019-04-05 | 辽东学院 | A kind of negative oxygen-ion, far infrared silk tussah fibre finishing fluid, negative oxygen-ion, far infrared silk tussah fibre and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103205891B (en) | 2015-03-04 |
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