CN103173298B - Quick oil stain detergent and preparation method - Google Patents
Quick oil stain detergent and preparation method Download PDFInfo
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- CN103173298B CN103173298B CN201110435723.0A CN201110435723A CN103173298B CN 103173298 B CN103173298 B CN 103173298B CN 201110435723 A CN201110435723 A CN 201110435723A CN 103173298 B CN103173298 B CN 103173298B
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Abstract
The invention discloses Quick oil stain detergent and preparation method, Quick oil stain detergent is that raw material is made by following component by weight percentage: Sodium dodecylbenzene sulfonate, C14-17 Seconary Alkane Sulphonate Sodium, C9-11 Pareth-3, cocotrimonium chloride, trolamine, methylchloroisothiazandnone, methylisothiazolinone, lemon yellow pigment, essence, all the other are water.Experiment proves: washing composition of the present invention, heavy oil stain successful in cleaning kitchen, utilize the additive that the synergistic function between tensio-active agent is suitable in addition, effectively can remove various greasy dirt in kitchen, clean environment firendly, nontoxic, harmless, without phosphorus, cleaning process neither corrodes kitchen utilities, also do not injure skin, for the cleaning of kitchen oil stain, oily waste degradation rate can reach more than 99.4%.Low cost of raw materials, easily purchases and is easy to get, and economic benefit is good, is applicable to suitability for industrialized production.
Description
Technical field
The invention belongs to articles for washing field, relating to a kind of washing composition for cleaning heavy oil stain in kitchen and preparation method.
Background technology
The formation of kitchen dirt mainly edible oil drippage and heated portion is evaporated and pollutes on apparatus, adds dust, accumulates over a long period and just define the extremely strong grease of one deck thickness sticking power.The clean-out system that this grease is general is difficult to removing, so be badly in need of the clean-out system of a kind of easy, quick, environmental protection of research and development.
At present, conventional kitchen oil stain cleaning is main adopts strong basicity cleaning and solvent-borne type cleaning technique, although the two has higher oily waste degradation rate, safety in utilization is poor, has larger corrosion and disoperation to human body skin and kitchen utilities.Therefore, efficiently, the development of the kitchen oil stain clean-out system of safety, environmental protection has larger using value and development prospect.
Summary of the invention
The object of the present invention is to provide a kind of Quick oil stain detergent that can be used for cleaning heavy oil stain in kitchen.
Second object of the present invention is to provide a kind of preparation method of Quick oil stain detergent.
Technical scheme of the present invention is summarized as follows:
Quick oil stain detergent is that raw material is made by following component by weight percentage:
Sodium dodecylbenzene sulfonate 18-30%; C14-17 Seconary Alkane Sulphonate Sodium 7-10%; C9-11 Pareth-3 1.5-2%; Cocotrimonium chloride 1.5-3%; Trolamine 2-5%; Methylchloroisothiazandnone 0.01-0.03%; Methylisothiazolinone 0.01-0.03%; Lemon yellow pigment 0.0001-0.0004%; Essence 0.2-0.4%; All the other are water.
The weight percent of described Sodium dodecylbenzene sulfonate is 22%.
Described essence is ice orange essence, flavoring pineapple essence, strawberry flavour, osmanthus flower fragrance or Hami melon essence.
The preparation method of Quick oil stain detergent, comprises the steps:
(1) raw material is taken by weight percentage: Sodium dodecylbenzene sulfonate 18-30%; C14-17 Seconary Alkane Sulphonate Sodium 7-10%; C9-11 Pareth-3 1.5-2%; Cocotrimonium chloride 1.5-3%; Trolamine 2-5%; Methylchloroisothiazandnone 0.01-0.03%; Methylisothiazolinone 0.01-0.03%; Lemon yellow pigment 0.0001-0.0004%; Essence 0.2-0.4%; All the other are water;
(2) in ingredients pot, add a certain amount of water, stir and be warming up to 75-80 DEG C, add Sodium dodecylbenzene sulfonate, to be to be dissolvedly uniformly dispersed, continue to stir 5-15 minute;
(3) ingredients pot temperature is down to 55-60 DEG C, adds C14-17 Seconary Alkane Sulphonate Sodium, stir;
(4) ingredients pot temperature is down to 45-50 DEG C, the mode stirred while adding adds C9-11 Pareth-3, cocotrimonium chloride, trolamine successively; By often adding a kind of raw material interval 5-7 minute;
(5) regulate pH to 8-9 with sodium hydroxide, then add methylchloroisothiazandnone, methylisothiazolinone, essence and lemon yellow pigment, often add a kind of raw material interval 5-7 minute, stir while adding, add water to 100%, stir, be i.e. obtained Quick oil stain detergent.
Described essence is ice orange essence, flavoring pineapple essence, strawberry flavour, osmanthus flower fragrance or Hami melon essence.
Experiment proves: washing composition of the present invention, heavy oil stain successful in cleaning kitchen, utilize the additive that the synergistic function between tensio-active agent is suitable in addition, effectively can remove various greasy dirt in kitchen, clean environment firendly, nontoxic, harmless, without phosphorus, cleaning process neither corrodes kitchen utilities, also do not injure skin, for the cleaning of kitchen oil stain, oily waste degradation rate can reach more than 99.4%.Low cost of raw materials, easily purchases and is easy to get, and economic benefit is good, is applicable to suitability for industrialized production.
Embodiment
Below in conjunction with specific embodiment, set forth the present invention further.Should be understood that these embodiments are only not used in for illustration of the present invention to limit the scope of the invention.In addition should be understood that those skilled in the art can change the present invention or revise, and these equivalent form of values fall within the application's claims limited range equally after the content of having read the present invention's instruction.
Table 1 be classified as embodiment 1-embodiment 4 composition by weight percentage:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | |
| Sodium dodecylbenzene sulfonate | 22 | 25 | 18 | 30 |
| C14-17 Seconary Alkane Sulphonate Sodium | 8 | 7 | 9 | 10 |
| C9-11 Pareth-3 | 1 | 2 | 1.5 | 1 |
| Cocotrimonium chloride | 2 | 1 | 3 | 1.5 |
| Trolamine | 3 | 2 | 3 | 5 |
| Methylchloroisothiazandnone | 0.02 | 0.03 | 0.01 | 0.02 |
| Methylisothiazolinone | 0.02 | 0.02 | 0.03 | 0.01 |
| Lemon yellow pigment | 0.0002 | 0.0001 | 0.0002 | 0.0004 |
| Essence | 0.3 (ice orange essence) | 0.4 (flavoring pineapple essence) | 0.1 (strawberry flavour) | 0.2 (osmanthus flower fragrance) |
| All the other are water; | Add water to 100 parts | Add water to 100 parts | Add water to 100 parts | Add water to 100 parts |
Embodiment 5
The preparation method of Quick oil stain detergent, comprises the steps:
(1) material is taken by embodiment 1:
(2) in ingredients pot, add a certain amount of water, stir and be warming up to 78 DEG C, add Sodium dodecylbenzene sulfonate, to be to be dissolvedly uniformly dispersed, continue stirring 10 minutes;
(3) ingredients pot temperature is down to 58 DEG C, adds C14-17 Seconary Alkane Sulphonate Sodium, stir;
(4) ingredients pot temperature is down to 48 DEG C, the mode stirred while adding adds C9-11 Pareth-3, cocotrimonium chloride, trolamine successively; By often adding 6 minutes, a kind of raw material interval;
(5) regulate pH to 8 with sodium hydroxide, then add methylchloroisothiazandnone, methylisothiazolinone, essence and lemon yellow pigment, often add 6 minutes, a kind of raw material interval, stir while adding, add water to 100%, stir, be i.e. obtained Quick oil stain detergent.
Embodiment 6
The preparation method of Quick oil stain detergent, comprises the steps:
(1) material is taken by embodiment 2:
(2) in ingredients pot, add a certain amount of water, stir and be warming up to 75 DEG C, add Sodium dodecylbenzene sulfonate, to be to be dissolvedly uniformly dispersed, continue stirring 15 minutes;
(3) ingredients pot temperature is down to 60 DEG C, adds C14-17 Seconary Alkane Sulphonate Sodium, stir;
(4) ingredients pot temperature is down to 48 DEG C, the mode stirred while adding adds C9-11 Pareth-3, cocotrimonium chloride, trolamine successively; By often adding 5 minutes, a kind of raw material interval;
(5) regulate pH to 9 with sodium hydroxide, then add methylchloroisothiazandnone, methylisothiazolinone, essence and lemon yellow pigment, often add 5 minutes, a kind of raw material interval, stir while adding, add water to 100%, stir, be i.e. obtained Quick oil stain detergent.
Embodiment 7
The preparation method of Quick oil stain detergent, comprises the steps:
(1) material is taken by embodiment 3:
(2) in ingredients pot, add a certain amount of water, stir and be warming up to 76 DEG C, add Sodium dodecylbenzene sulfonate, to be to be dissolvedly uniformly dispersed, continue stirring 5 minutes;
(3) ingredients pot temperature is down to 55 DEG C, adds C14-17 Seconary Alkane Sulphonate Sodium, stir;
(4) ingredients pot temperature is down to 50 DEG C, the mode stirred while adding adds C9-11 Pareth-3, cocotrimonium chloride, trolamine successively; By often adding 6 minutes, a kind of raw material interval;
(5) regulate pH to 8 with sodium hydroxide, then add methylchloroisothiazandnone, methylisothiazolinone, essence and lemon yellow pigment, often add 6 minutes, a kind of raw material interval, stir while adding, add water to 100%, stir, be i.e. obtained Quick oil stain detergent.
Embodiment 8
The preparation method of Quick oil stain detergent, comprises the steps:
(1) material is taken by embodiment 4:
(2) in ingredients pot, add a certain amount of water, stir and be warming up to 80 DEG C, add Sodium dodecylbenzene sulfonate, to be to be dissolvedly uniformly dispersed, continue stirring 10 minutes;
(3) ingredients pot temperature is down to 58 DEG C, adds C14-17 Seconary Alkane Sulphonate Sodium, stir;
(4) ingredients pot temperature is down to 45 DEG C, the mode stirred while adding adds C9-11 Pareth-3, cocotrimonium chloride, trolamine successively; By often adding 7 minutes, a kind of raw material interval;
(5) regulate pH to 9 with sodium hydroxide, then add methylchloroisothiazandnone, methylisothiazolinone, essence and lemon yellow pigment, often add 7 minutes, a kind of raw material interval, stir while adding, add water to 100%, stir, be i.e. obtained Quick oil stain detergent.
Experiment proves: Quick oil stain detergent of the present invention effectively can remove all kinds of obstinate oil stain dirt on the surfaces such as kitchen range in kitchen, door, window, ground, cupboard, exhaust fan, smoke exhaust ventilator fast; Diffuse is strong, and the obstinate grease of decomposable asymmetric choice net, by being arranged on the nozzle on bottle, makes liquid can be atomized spray, for cleaning large-area greasy dirt; Also liquid can be made to be linear injection, to can be used for cleaning heavy oil stain, easy to use, be the essential product in household kitchen.
Main component
C14-17 Seconary Alkane Sulphonate Sodium has unique physicochemical property, and biological degradation is splendid; Solvability is strong, and wetting power is good, has fabulous cleaning and degreasing performance; Splendid joining property of association is had to skin; Within the scope of whole PH, have chemical stability, be a kind of novel surfactant, and have good decontamination, dissolving and resist water hardness tolerance, pungency is low.
C9-11 Pareth-3 is a kind of emulsifying agents, can be biodegradable, the spatter property had within the scope of alkaline PH, has resistance to hard water, soft water, static electricity resistance and anti-deposition properties; But must with tensio-active agent with the use of, just there is the degreasing that level is good.
Experiment proves: washing composition of the present invention can in 3min within effective remove various greasy dirt in kitchen, oily waste degradation rate can reach more than 99.4%.
Claims (5)
1., for cleaning the washing composition of heavy oil stain in kitchen, it is characterized in that being made up of following method:
(1) raw material is taken by weight percentage: Sodium dodecylbenzene sulfonate 18-30%; C
14-17seconary Alkane Sulphonate Sodium 7-10%; C
9-11pareth-3 1.5-2%; Cocotrimonium chloride 1.5-3%; Trolamine 2-5%; Methylchloroisothiazandnone 0.01-0.03%; Methylisothiazolinone 0.01-0.03%; Lemon yellow pigment 0.0001-0.0004%; Essence 0.2-0.4%; All the other are water;
(2) in ingredients pot, add a certain amount of water, stir and be warming up to 75-80 DEG C, add Sodium dodecylbenzene sulfonate, to be to be dissolvedly uniformly dispersed, continue to stir 5-15 minute;
(3) ingredients pot temperature is down to 55-60 DEG C, adds C
14-17seconary Alkane Sulphonate Sodium, stirs;
(4) ingredients pot temperature is down to 45-50 DEG C, the mode stirred while adding adds C successively
9-11pareth-3, cocotrimonium chloride, trolamine; Often add a kind of raw material interval 5-7 minute;
(5) regulate pH to 8-9 with sodium hydroxide, then add methylchloroisothiazandnone, methylisothiazolinone, essence and lemon yellow pigment, often add a kind of raw material interval 5-7 minute, stir while adding, add water to 100%, stir, be i.e. obtained Quick oil stain detergent.
2. the washing composition for cleaning heavy oil stain in kitchen according to claim 1, is characterized in that: the weight percent of described Sodium dodecylbenzene sulfonate is 22%.
3. the washing composition for cleaning heavy oil stain in kitchen according to claim 1, is characterized in that: described essence is ice orange essence, flavoring pineapple essence, strawberry flavour, osmanthus flower fragrance or Hami melon essence.
4. the preparation method of the washing composition for cleaning heavy oil stain in kitchen according to claim 1, is characterized in that comprising the steps: that (1) takes raw material by weight percentage: Sodium dodecylbenzene sulfonate 18-30%; C
14-17seconary Alkane Sulphonate Sodium 7-10%; C
9-11pareth-3 1.5-2%; Cocotrimonium chloride 1.5-3%; Trolamine 2-5%; Methylchloroisothiazandnone 0.01-0.03%; Methylisothiazolinone 0.01-0.03%; Lemon yellow pigment 0.0001-0.0004%; Essence 0.2-0.4%; All the other are water;
(2) in ingredients pot, add a certain amount of water, stir and be warming up to 75-80 DEG C, add Sodium dodecylbenzene sulfonate, to be to be dissolvedly uniformly dispersed, continue to stir 5-15 minute;
(3) ingredients pot temperature is down to 55-60 DEG C, adds C
14-17seconary Alkane Sulphonate Sodium, stirs;
(4) ingredients pot temperature is down to 45-50 DEG C, the mode stirred while adding adds C successively
9-11pareth-3, cocotrimonium chloride, trolamine; Often add a kind of raw material interval 5-7 minute;
(5) regulate pH to 8-9 with sodium hydroxide, then add methylchloroisothiazandnone, methylisothiazolinone, essence and lemon yellow pigment, often add a kind of raw material interval 5-7 minute, stir while adding, add water to 100%, stir, be i.e. obtained Quick oil stain detergent.
5. the preparation method of the washing composition for cleaning heavy oil stain in kitchen according to claim 4, is characterized in that described essence is ice orange essence, flavoring pineapple essence, strawberry flavour, osmanthus flower fragrance or Hami melon essence.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110435723.0A CN103173298B (en) | 2011-12-22 | 2011-12-22 | Quick oil stain detergent and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110435723.0A CN103173298B (en) | 2011-12-22 | 2011-12-22 | Quick oil stain detergent and preparation method |
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| Publication Number | Publication Date |
|---|---|
| CN103173298A CN103173298A (en) | 2013-06-26 |
| CN103173298B true CN103173298B (en) | 2015-10-28 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201110435723.0A Expired - Fee Related CN103173298B (en) | 2011-12-22 | 2011-12-22 | Quick oil stain detergent and preparation method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103710012B (en) * | 2013-12-04 | 2016-01-13 | 天津大港油田滨港集团博弘石油化工有限公司 | A kind of sewage whipping agent |
| CN110129145A (en) * | 2018-02-08 | 2019-08-16 | 黄瑞金 | A kind of degreasing agent and production method |
| CN113801740A (en) * | 2020-06-14 | 2021-12-17 | 金华市金东区嘉良日用品厂 | Oil stain purifying condensation bead |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1191890A (en) * | 1997-02-27 | 1998-09-02 | Lg化学株式会社 | Compositions of dishwashing detergent |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1191890A (en) * | 1997-02-27 | 1998-09-02 | Lg化学株式会社 | Compositions of dishwashing detergent |
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Granted publication date: 20151028 Termination date: 20211222 |