CN103172350A - Production technology of live crystal porcelain - Google Patents
Production technology of live crystal porcelain Download PDFInfo
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- CN103172350A CN103172350A CN2013100986321A CN201310098632A CN103172350A CN 103172350 A CN103172350 A CN 103172350A CN 2013100986321 A CN2013100986321 A CN 2013100986321A CN 201310098632 A CN201310098632 A CN 201310098632A CN 103172350 A CN103172350 A CN 103172350A
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Abstract
The invention relates to the field of ceramic, and particularly relates to a production technology of live crystal porcelain. The production technology comprises the following production steps of burning, cooling, grinding, and sieving potash feldspar and the like; burning, cooling, grinding and sieving periclase and the like; respectively burning, cooling, grinding and sieving kaoline and the like; taking petuntse raw material to grind and stew, and preparing into petuntse; taking porcelain glaze raw material to grind, stew and prepare into porcelain glaze; molding, drying, biscuiting and cooling the petuntse to obtain the biscuit product; and glazing the biscuit product by porcelain glaze, and then putting into a kiln to sinter. The live crystal porcelain product prepared by the production technology is natural, free of poison, harm or odor, energy-saving and environment-friendly; daily drinking water is changed into small-molecule water (commonly known as 'running water'); and the small-molecule water enters a cell water channel of a human body, so as to improve the physiological efficacy and health benefit of water on the human body.
Description
Technical field
The present invention relates to ceramic field, in particular to a kind of production technique of the brilliant porcelain of living.
Background technology
At present, ceramic product is only the effect of playing decoration or storage, and wherein, earthenware porcelain receptacle does not play any beneficial effect to the object that is held within it, only has the function that holds of container.
Summary of the invention
The object of the present invention is to provide a kind of production technique of the brilliant porcelain of living, to solve the above problems.
A kind of production technique of the brilliant porcelain of living is provided in an embodiment of the present invention, has comprised following production stage:
Steps A: respectively potassium felspar sand, albite, sodium aluminum fluoride, spinel, mullite, trichroite are calcined 5.5-6.5h under 940-960 ℃, and grind after being cooled to normal temperature, cross the 90-120 mesh sieve, standby;
Respectively periclasite, calcite, fluorite, quartzite, medical stone, tourmalinite are calcined 5.5-6.5h under 840-860 ℃, and grind after being cooled to normal temperature, cross the 90-120 mesh sieve, standby;
Respectively kaolin, wilkinite, clay are calcined 5.5-6.5h respectively under 590-610 ℃, and grind after being cooled to normal temperature, cross the 90-120 mesh sieve, standby;
step B: by weight, get kaolin 21-23%, clay 21-23%, quartzite 11-13%, albite 7-9%, bone meal 4-6%, mullite 4-4.5%, trichroite 3-3.5%, tourmalinite 3-3.5%, medical stone 3-3.5%, spinel 3-3.5%, borax 2.8-3.2%, rare earth element 4.8-5.2%, wilkinite 5-7% is as porcelain mud raw material, knock down ball mill, the water that adds the 80-100% of porcelain mud raw material gross weight, grind 24-28h, standing 36 hours again, remove the water float thing, adopt again the magnet removal of impurities, then except hydraulic pressure mud, pugging to pug weight in wet base per-cent is 19-25%, make porcelain mud,
step C: by weight, get kaolin 2-2.5%, wilkinite 9-11%, potassium felspar sand 36-40%, calcite 3.5-4.5%, zinc oxide 10-12%, barium carbonate 2-3%, titanium trioxide 0.2-1.4%, quartzite 4.5-5.5%, sodium aluminum fluoride 2.5-3.5%, Quilonum Retard 2.5-3.5%, fluorite 2.5-3.5%, rare earth element 4.8-5.2%, periclasite 2.8-3.2%, tourmalinite 4.8-5.2%, medical stone 4.8-5.2% is as the enamel raw material, knock down ball mill, the water that adds the 80-100% of enamel raw material gross weight, grind 24-28h, standing 36 hours again, remove the water float thing, adopt again the magnet removal of impurities, then except hydraulic pressure mud, pugging to pug weight in wet base per-cent is 19-25%, make enamel,
Step D: described porcelain mud is carried out moulding by the traditional ceramics production method, drying, then at 880-920 ℃ of lower biscuiting 3.5-4.5h, and naturally cool to normal temperature, obtain the biscuiting product;
Step e: press the traditional ceramics production method, adopt described enamel to carry out glazing to described biscuiting product, then be placed in kiln and burn till;
Described method of burning till is:
First controlling in kiln is reducing atmosphere, and makes the temperature in kiln be warming up to 850-900 ℃ in 3-4h, then is warming up to 1215-1225 ℃ in 5-6h; Controlling in kiln is oxidizing atmosphere again, and makes the temperature of kiln keep 2h under 1215-1225 ℃; Controlling kiln is neutral atmosphere again, kiln temperature is cooled to 1160-1170 ℃ in 3min; With the speed of 50-65 ℃ per hour, kiln temperature is warming up to 1280-1300 ℃ again in 100-120min, and in keeping 25-35min, after come out of the stove, then naturally cool to normal temperature, obtain product;
Relate to the raw material identical with described steps A in described porcelain mud raw material and described enamel raw material and all adopt raw material through described processing of step A.
The production technique of a kind of brilliant porcelain of living of the above embodiment of the present invention, in sintering process, two steps of burning till in the kiln of reducing atmosphere and oxidizing atmosphere have been completed the crystal melting, and when being neutral atmosphere in kiln, kiln temperature are cooled to 1160-1170 ℃ in 3min; This moment, temperature sharply descended, impel a kind of natural pulling force of host crystal self-assembling formation when quench, other low-melting crystal is attracted around host crystal, thus form a kind of polynary combination the type well-regulated brilliant flower of eternal live body that can discharge infrared energy in order arranged; Thereby make the product of making except having the function of holding, also have the brilliant characteristic of following work:
Crystal shape is different from ordinary porcelain, and its crystal is macrocrystal cover small-crystalline, and small-crystalline cover macrocrystal seems to seem active pure;
Intrinsic heat electrically and piezoelectricity, it can make its polarity ion in the equilibrium theory of tide vibration and cause dipole
Square change to produce the electromagnetic radiation of far infrared band and generate energy also claims the anion far infrared rays energy;
Inspection center is detected through national far infrared, and its far infrared rays wavelength is 11 μ m, and emittance reaches 92%, and the full emission of normal direction reaches 84%;
In addition, through detecting proof, the product that the present invention makes has the brilliant function of following work:
Can make the macromolecular mass water of tap water become small-micelle water, detect through " national drug and Methanogenesis research centre ", record spectrum peak width NMR and reach 57.43Hz;
Through " national general Buddhist nun examines " center " and detects, potential of hydrogen that can the equilibrium water;
Through " Beijing public health tap water institute " check, can reach 20.09% except the free chlorine residual in anhydrating;
Through " Beijing public health tap water institute " check, bacteriostasis rate reaches 75.76%.
Description of drawings
Fig. 1 shows the brilliant porcelain of work of test example preparation of the present invention at the crystal shape of microscopically.
Embodiment
Also by reference to the accompanying drawings the present invention is described in further detail below by specific embodiment.
Embodiment one
Embodiments of the invention one provide a kind of production technique of the brilliant porcelain of living, and comprise the following steps:
The first step: respectively potassium felspar sand, albite, sodium aluminum fluoride, spinel, mullite, trichroite are calcined 5.5-6.5h under 940-960 ℃, and grind after being cooled to normal temperature, cross the 90-120 mesh sieve, standby;
Respectively periclasite, calcite, fluorite, quartzite, medical stone, tourmalinite are calcined 5.5-6.5h under 840-860 ℃, and grind after being cooled to normal temperature, cross the 90-120 mesh sieve, standby;
Respectively kaolin, wilkinite, clay are calcined 5.5-6.5h respectively under 590-610 ℃, and grind after being cooled to normal temperature, cross the 90-120 mesh sieve, standby;
second step: by weight, get kaolin 21-23%, clay 21-23%, quartzite 11-13%, albite 7-9%, bone meal 4-6%, mullite 4-4.5%, trichroite 3-3.5%, tourmalinite 3-3.5%, medical stone 3-3.5%, spinel 3-3.5%, borax 2.8-3.2%, rare earth element 4.8-5.2%, wilkinite 5-7% is as porcelain mud raw material, knock down ball mill, the water that adds the 80-100% of porcelain mud raw material gross weight, grind 24-28h, standing 36 hours again, remove the water float thing, adopt again the magnet removal of impurities, then except hydraulic pressure mud, pugging to pug weight in wet base per-cent is 19-25%, make porcelain mud,
the 3rd step: by weight, get kaolin 2-2.5%, wilkinite 9-11%, potassium felspar sand 36-40%, calcite 3.5-4.5%, zinc oxide 10-12%, barium carbonate 2-3%, titanium trioxide 0.2-1.4%, quartzite 4.5-5.5%, sodium aluminum fluoride 2.5-3.5%, Quilonum Retard 2.5-3.5%, fluorite 2.5-3.5%, rare earth element 4.8-5.2%, periclasite 2.8-3.2%, tourmalinite 4.8-5.2%, medical stone 4.8-5.2% is as the enamel raw material, knock down ball mill, the water that adds the 80-100% of enamel raw material gross weight, grind 24-28h, standing 36 hours again, remove the water float thing, adopt again the magnet removal of impurities, then except hydraulic pressure mud, pugging to pug weight in wet base per-cent is 19-25%, make enamel,
The 4th step: described porcelain mud is carried out moulding by the traditional ceramics production method, drying, then at 880-920 ℃ of lower biscuiting 3.5-4.5h, and naturally cool to normal temperature, obtain the biscuiting product;
The 5th step: press the traditional ceramics production method, adopt described enamel to carry out glazing to described biscuiting product, then be placed in kiln and burn till;
Described method of burning till is:
First controlling in kiln is reducing atmosphere, and makes the temperature in kiln be warming up to 850-900 ℃ in 3-4h, then is warming up to 1215-1225 ℃ in 5-6h; Controlling in kiln is oxidizing atmosphere again, and makes the temperature of kiln keep 2h under 1215-1225 ℃; Controlling kiln is neutral atmosphere again, kiln temperature is cooled to 1160-1170 ℃ in 3min; With the speed of 50-65 ℃ per hour, kiln temperature is warming up to 1280-1300 ℃ again in 100-120min, and in keeping 25-35min, after come out of the stove, then naturally cool to normal temperature, obtain product;
Relate to the raw material identical with the first step in described porcelain mud raw material and described enamel raw material and all adopt the raw material of processing through the described the first step.
Described normal temperature is 20-35 ℃.
Above-mentioned production technique, two steps of burning till in the kiln of reducing atmosphere and oxidizing atmosphere have been completed the crystal melting, and when being neutral atmosphere in kiln, kiln temperature are cooled to 1160-1170 ℃ in 3min; This moment, temperature sharply descended, impel a kind of natural pulling force of host crystal self-assembling formation when quench, other low-melting crystal is attracted around host crystal, thus form a kind of polynary combination the type well-regulated brilliant flower of eternal live body that can discharge infrared energy in order arranged; Thereby make the product of making have the brilliant characteristic of following work:
Crystal shape is different from ordinary porcelain, and its crystal is macrocrystal cover small-crystalline, and small-crystalline cover macrocrystal seems to seem active pure;
Intrinsic heat electrically and piezoelectricity, it can make its polarity ion in the equilibrium theory of tide vibration and cause dipole
Square change to produce the electromagnetic radiation of far infrared band and generate energy also claims the anion far infrared rays energy;
Inspection center is detected through national far infrared, and its far infrared rays wavelength is 11 μ m, and emittance reaches 92%, and the full emission of normal direction reaches 84%;
In addition, through detecting proof, the product that the present invention makes has the brilliant function of following work:
Can make the macromolecular mass water of tap water become small-micelle water, detect through " national drug and Methanogenesis research centre ", record spectrum peak width NMR and reach 57.43Hz;
Through " national general Buddhist nun examines " center " and detects, potential of hydrogen that can the equilibrium water;
Through " Beijing public health tap water institute " check, can reach 20.09% except the free chlorine residual in anhydrating;
Through " Beijing public health tap water institute " check, bacteriostasis rate reaches 75.76%.
As seen, production technique provided by the invention can obtain a kind of multi-functional pottery, namely has the brilliant dual-use function that holds and live.In a word, the brilliant porcelain products of the work that the present invention makes are not only natural, nontoxic, tasteless, energy-conservation and environmental protection, it can become daily tap water small-micelle water (being commonly called as " running water "), small-micelle water can enter the cellular water channel of human body, thereby improves water to physiological function and the health efficacy of human body.Science proves, ordering and structurized small-micelle water are easily absorbed by human body cell, can better participate in substance metabolism, energy metabolism, the information metabolism of human body, thereby reach the effect that promotes health and improve quality of life.
In addition, the described rare earth element in above-mentioned production technique is by 1 part of yttrium, 1 part of lanthanum, 2 parts of praseodymiums and 1 part of neodymium is mixed forms (by weight), perhaps other etc.
" by the traditional ceramics production method " in above-mentioned the 4th step refers to porcelain mud is broken into mud, the mould that reinjects, more naturally dry, then demoulding ejection.
" by the traditional ceramics production method " in described the 5th step refers to the method for " soaking glaze ", is about to base substrate and immerses in enamel, takes out in a moment, utilizes the water-absorbent of base substrate, makes enamel be attached to equably billet surface.
The beneficial effect that reaches in order to illustrate further production technique of the present invention, the present invention also provides concrete test example.
Test example
Test method:
The first step: get and grind after potassium felspar sand, albite, sodium aluminum fluoride, spinel, mullite, trichroite are cooled to normal temperature after respectively at 950 ℃ of calcining 6h, cross 120 mesh sieves standby;
Get and grind after periclasite, calcite, lustrous and transparent spar, quartzite, medical stone, tourmalinite are cooled to normal temperature respectively at 850 ℃ of calcining 6h, cross 120 mesh sieves standby;
Get and grind after kaolin, wilkinite, clay are cooled to normal temperature after respectively at 600 ℃ of calcining 6h, cross 120 mesh sieves standby;
second step: by weight percentage, get kaolin 22%, clay 22%, quartzite 12%, albite 8%, bone meal 5%, mullite 4.2%, trichroite 3.2%, tourmalinite 3.2%, medical stone 3.2%, spinel 3.2%, borax 3%, yttrium 1%, lanthanum 1%, praseodymium 2%, neodymium 1%, wilkinite 6% is as porcelain mud raw material, knock down ball mill, 100% the water that adds porcelain mud raw material gross weight, grind 24h, standing 36 hours again, remove the water float thing, adopt again the magnet removal of impurities, (i.e. " old dirt ") is then except hydraulic pressure mud, pugging is to pug water content 20%(weight percent), make porcelain mud standby.
the 3rd step: get by weight percentage kaolin 2.2%, wilkinite 10%, potassium felspar sand 38%, calcite 4%, zinc oxide 11%, barium carbonate 2.5%, titanium trioxide 0.3%, quartzite 5%, sodium aluminum fluoride 3%, Quilonum Retard 3%, fluorite 3%, yttrium 1%, lanthanum 1%, praseodymium 2%, neodymium 1%, periclasite 3%, tourmalinite 5%, medical stone 5% is as the enamel raw material, knock down ball mill, 80% the water that adds enamel raw material gross weight ground 28 hours, standing 36 hours again, remove the water float thing, adopt again the magnet removal of impurities, then except hydraulic pressure mud, pugging is to pug water content 24%(weight percent), make enamel standby.
All raw materials that relate in above-mentioned porcelain mud and enamel preparation process all adopt the raw material of processing through the first step.
The 4th the step: get standby porcelain mud and carry out shaping and drying by the traditional ceramics production method, then with moulding product after 900 ℃ of biscuiting 4h, naturally cool to normal temperature standby;
The 5th step: get the product of standby enamel after to biscuiting by the traditional ceramics production method and carry out glazing, then be placed in kiln and burn till, this moment, kiln was reducing atmosphere, prior to being warming up to 900 ℃ in 4h, then was warming up to 1220 ℃ in 5h; Controlling kiln is oxidizing atmosphere again, keeps kiln temperature 2h in 1220 ℃; The adjustment kiln is neutral atmosphere, kiln temperature is cooled to 1160 ℃ in 3min; With the speed of 60 ℃ per hour, kiln temperature is warming up to 1280 ℃ in 120 minutes, and comes out of the stove after keeping constant temperature 30min in 1280 ℃ and naturally cool to normal temperature, make the product of test example.
This test example formed product is good, and the rate of burning till reaches 99%, at the microscopically crystal shape as shown in Figure 1.After testing, its far infrared rays wavelength is 11mn, and emittance reaches 92%, and the full emission of normal direction reaches 84%, and it is 57.43Hz that the spectrum peak width reaches NMR, can reach 20.09% except the free chlorine residual in anhydrating, and bacteriostasis rate reaches 75.76%.
For further outstanding beneficial effect of the present invention, also provide following Comparative Examples.
Comparative Examples 1: different from test example is, omits the first step " part material low temperature calcination ", makes the product of Comparative Examples 1.The technique of Comparative Examples 1 makes raw material have the organism residue, and the carbide that produces can affect flowing of crystal in sintering process, can't form uniform crystal, and the formed product qualification rate is low.
Comparative Examples 2: different from test example is that the first step " raw material calcining " all adopts 800 ℃ of calcining 6h, makes the product of Comparative Examples 2.The technique of Comparative Examples 2 produces the surface interruptions thing around making crystal, and the product crystal size of making is inhomogeneous.
Comparative Examples 3: different from test example is, the 5th step was revised as and gets the product of standby enamel after to biscuiting by the traditional ceramics production method and carry out glazing, then was placed in kiln and burnt till, and this moment, kiln was reducing atmosphere, be warming up to 900 ℃ in 4 hours, then be warming up to 1220 ℃ in 5h; Controlling kiln is oxidizing atmosphere again, keeps kiln temperature after 2.5h, directly to come out of the stove in 1220 ℃, naturally cools to normal temperature, makes the product of Comparative Examples 3.The formation of the technogenic influence crystal of Comparative Examples 3, the crystal of the product of making are irregular or half of crystal block, affect the radiation quantity of far infrared rays.
Contrast 4: different from test example is that the 5th step all adopted neutral atmosphere to burn till, and made the product of Comparative Examples 4.The technique of Comparative Examples 4 is the formation of catalysis crystal effectively, and the product of making be can't see crystal at microscopically.
The above is only the preferred embodiments of the present invention, is not limited to the present invention, and for a person skilled in the art, the present invention can have various modifications and variations.Within the spirit and principles in the present invention all, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (3)
1. the production technique of the brilliant porcelain of living, is characterized in that, comprises following production stage:
Steps A: respectively potassium felspar sand, albite, sodium aluminum fluoride, spinel, mullite, trichroite are calcined 5.5-6.5h under 940-960 ℃, and grind after being cooled to normal temperature, cross the 90-120 mesh sieve, standby;
Respectively periclasite, calcite, fluorite, quartzite, medical stone, tourmalinite are calcined 5.5-6.5h under 840-860 ℃, and grind after being cooled to normal temperature, cross the 90-120 mesh sieve, standby;
Respectively kaolin, wilkinite, clay are calcined 5.5-6.5h respectively under 590-610 ℃, and grind after being cooled to normal temperature, cross the 90-120 mesh sieve, standby;
step B: by weight, get kaolin 21-23%, clay 21-23%, quartzite 11-13%, albite 7-9%, bone meal 4-6%, mullite 4-4.5%, trichroite 3-3.5%, tourmalinite 3-3.5%, medical stone 3-3.5%, spinel 3-3.5%, borax 2.8-3.2%, rare earth element 4.8-5.2%, wilkinite 5-7% is as porcelain mud raw material, knock down ball mill, the water that adds the 80-100% of porcelain mud raw material gross weight, grind 24-28h, standing 36 hours again, remove the water float thing, adopt again the magnet removal of impurities, then except hydraulic pressure mud, pugging to pug weight in wet base per-cent is 19-25%, make porcelain mud,
step C: by weight, get kaolin 2-2.5%, wilkinite 9-11%, potassium felspar sand 36-40%, calcite 3.5-4.5%, zinc oxide 10-12%, barium carbonate 2-3%, titanium trioxide 0.2-1.4%, quartzite 4.5-5.5%, sodium aluminum fluoride 2.5-3.5%, Quilonum Retard 2.5-3.5%, fluorite 2.5-3.5%, rare earth element 4.8-5.2%, periclasite 2.8-3.2%, tourmalinite 4.8-5.2%, medical stone 4.8-5.2% is as the enamel raw material, knock down ball mill, the water that adds the 80-100% of enamel raw material gross weight, grind 24-28h, standing 36 hours again, remove the water float thing, adopt again the magnet removal of impurities, then except hydraulic pressure mud, pugging to pug weight in wet base per-cent is 19-25%, make enamel,
Step D: described porcelain mud is carried out moulding by the traditional ceramics production method, drying, then at 880-920 ℃ of lower biscuiting 3.5-4.5h, and naturally cool to normal temperature, obtain the biscuiting product;
Step e: press the traditional ceramics production method, adopt described enamel to carry out glazing to described biscuiting product, then be placed in kiln and burn till;
Described method of burning till is:
First controlling in kiln is reducing atmosphere, and makes the temperature in kiln be warming up to 850-900 ℃ in 3-4h, then is warming up to 1215-1225 ℃ in 5-6h; Controlling in kiln is oxidizing atmosphere again, and makes the temperature of kiln keep 2h under 1215-1225 ℃; Controlling kiln is neutral atmosphere again, kiln temperature is cooled to 1160-1170 ℃ in 3min; With the speed of 50-65 ℃ per hour, kiln temperature is warming up to 1280-1300 ℃ again in 100-120min, and in keeping 25-35min, after come out of the stove, then naturally cool to normal temperature, obtain product;
Relate to the raw material identical with described steps A in described porcelain mud raw material and described enamel raw material and all adopt raw material through described processing of step A.
2. the production technique of a kind of brilliant porcelain of living as claimed in claim 1, is characterized in that, described rare earth element comprises:
By weight, by 1 part of yttrium, 1 part of lanthanum, 2 parts of praseodymiums and 1 part of neodymium form.
3. the production technique of a kind of brilliant porcelain of living as claimed in claim 1 or 2, is characterized in that, described normal temperature is 20-35 ℃.
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| CN105016708A (en) * | 2015-08-11 | 2015-11-04 | 林俊生 | Functional live crystal porcelain and preparation method and application thereof |
| CN105669162A (en) * | 2016-02-18 | 2016-06-15 | *** | Preparation method of active ceramic and device where active ceramic acts to cause low-temperature nucleus melting reaction in water |
| CN108529882A (en) * | 2018-03-23 | 2018-09-14 | 俞骁飞 | A kind of explosion-proof porcelain coating and enamel utensil |
| CN110342918A (en) * | 2019-05-15 | 2019-10-18 | 中德道合科技有限公司 | A kind of crystallite new material and its application |
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| CN102617124A (en) * | 2012-03-27 | 2012-08-01 | 林俊生 | Active crystal ceramic production process |
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| CN102617124A (en) * | 2012-03-27 | 2012-08-01 | 林俊生 | Active crystal ceramic production process |
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| CN105016708A (en) * | 2015-08-11 | 2015-11-04 | 林俊生 | Functional live crystal porcelain and preparation method and application thereof |
| CN105669162A (en) * | 2016-02-18 | 2016-06-15 | *** | Preparation method of active ceramic and device where active ceramic acts to cause low-temperature nucleus melting reaction in water |
| CN108529882A (en) * | 2018-03-23 | 2018-09-14 | 俞骁飞 | A kind of explosion-proof porcelain coating and enamel utensil |
| CN108529882B (en) * | 2018-03-23 | 2023-12-22 | 俞骁飞 | Explosion-proof porcelain paint and enamel ware |
| CN110342918A (en) * | 2019-05-15 | 2019-10-18 | 中德道合科技有限公司 | A kind of crystallite new material and its application |
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| CN102617124A (en) | 2012-08-01 |
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