CN103142425B - Mineral mud nutritional emulsion and preparation method thereof - Google Patents
Mineral mud nutritional emulsion and preparation method thereof Download PDFInfo
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Abstract
A mineral mud nutrition emulsion and a preparation method thereof relate to an emulsion and a preparation method thereof. The invention aims to solve the problem that the existing emulsion can not provide more nutrition because the water for preparing the emulsion is deionized water. The invention relates to a mineral mud nutritional emulsion which is prepared by emulsifying stearic acid, octadecanol, monoglyceride, isopropyl palmitate, lanolin, water-soluble silicone oil, mineral mud oil-soluble extracting solution, alkyl phosphate, triethanolamine, propylene glycol, glycerol, propylparaben, methylparaben, essence and mineral mud water-soluble extracting solution. The preparation method comprises the following steps: firstly, weighing each component; secondly, preparing an oil phase mixture; thirdly, preparing a water phase mixture; fourthly, emulsification; obtaining the mineral mud nutritional emulsion. The invention can be used for preparing the mineral mud nutritional emulsion.
Description
Technical field
The present invention relates to a kind of emulsion and preparation method thereof.
Background technology
The formation of Wudalianchi Volcanic sludge is very long, and since 300,000 years, the old and new are repeatedly broken out in phase volcano constantly volcano particle matter deposition, and is formed by underground mineral water soaking.Forming process is natural volcanic slurry through high temperature, high pressure, naturally calmness, containing various trace elements and organic acid, there is higher medical function and health value, after testing, in multiple to human body beneficial element and mineral etc. containing calcium, magnesium, potassium, zinc, ferrum, copper etc., be that the desirable mineral of human body supplements source.
Containing higher metasilicic acid in Wudalianchi Volcanic sludge, mineral water, salinity is also higher, element silicon in metasilicic acid is mainly distributed on the aorta wall of human vas, it is the necessary trace element of human body, the biosynthesis of human connective tissue, epithelial tissue, osseous tissue, ossein can be participated in, promote that growth in humans grows, can strengthen the permeability of blood vessel wall and elasticity, raising skin elasticity, play the effect of beauty and skin care; Zinc is indispensable trace element in body, it participates in the various physiological activities of human body, and in the trace element of skin, the content of zinc is the highest, it decides the smooth of skin and extent of elasticity, participate in B16 cell, prevent and treat acne, maintain gloss and the slickness of skin, there is lipoid peroxidization resistant, remove interior free yl, make skin from lipid peroxidation injury, make skin emolliency, lubricious, smooth away wrinkles; Ferrum is the main component forming hemoglobin in blood, the ruddy blood needing supply sufficient of the gloss of skin, and complexion changed ruddy gloss in opposite is very useful; Copper is relevant with the metabolism of protein, nucleic acid, skin exquisiteness, hair can be made shiny black, make people full of vigour, keep vigorous and graceful.Normal human can by balancing various meals, and obtain the good complement of mineral, but due to a variety of causes, some people also mineral deficiency can occur, mineral can not synthesize in vivo, can only be drunk water, breathes or skin acquisition by food.Emulsion is the product that protection skin is the most basic, consumption is maximum, and the preparation water of most emulsion is deionized water, can not provide more nutrition.
Summary of the invention
The present invention is the preparation water that will solve existing emulsion is deionized water, can not provide more polyauxotrophic problem, and provide a kind of mineral mud nutrition emulsion and preparation method thereof.
A kind of mineral mud nutrition emulsion of the present invention is by mass percentage by 3% ~ 3.5% stearic acid, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 2% ~ 4% lanoline, 5% ~ 7% water-soluble silicon oil, 5% ~ 7% sludge oil-soluble extracting solution, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben, 0.1% ~ 0.3% methyl hydroxybenzoate, 0.01% ~ 0.05% essence and surplus are that sludge water-soluble extracting liquid forms through emulsifying.
The preparation method of above-mentioned mineral mud nutrition emulsion, carry out according to the following steps:
One, take each component: take 3% ~ 3.5% stearic acid by mass percentage, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 2% ~ 4% lanoline, 5% ~ 7% water-soluble silicon oil, 5% ~ 7% sludge oil-soluble extracting solution, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben, 0.1% ~ 0.3% methyl hydroxybenzoate, 0.01% ~ 0.05% essence and surplus are sludge water-soluble extracting liquid, two, oil mixture is prepared: low whipping speed is under the condition of 80r/min ~ 100r/min, 3% ~ 3.5% stearic acid step one taken, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 0.1% ~ 0.3% methyl hydroxybenzoate, 2% ~ 4% lanoline, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine and 5% ~ 7% sludge oil-soluble extracting solution mixing and stirring are also heated to 70 DEG C ~ 85 DEG C from room temperature, obtain oil mixture, three, aqueous mixture is prepared: low whipping speed is under the condition of 100r/min ~ 150r/min, 5% ~ 7% water-soluble silicon oil step one taken, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben and surplus are sludge water-soluble extracting liquid mixing and stirring and are heated to 80 DEG C ~ 90 DEG C from room temperature, then continue to stir 20min ~ 30min, obtain aqueous mixture, four, emulsifying: oil mixture step 2 obtained joins in the aqueous mixture that step 3 obtains, at the emulsified homogenizing 5min ~ 10min of condition that speed is 2500r/min ~ 3000r/min, be cooled to 30 DEG C ~ 50 DEG C, obtain water oil mixture, then 0.01% ~ 0.05% essence step one taken joins in water oil mixture, continue to stir 10min ~ 20min, be cooled to room temperature, namely obtain mineral mud nutrition emulsion.
Advantage of the present invention: one, utilize Wudalianchi Volcanic sludge extracting solution and Wudalianchi natural mineral water to manufacture mineral mud nutrition emulsion, abundant nutritional labeling can be provided to skin, make skin gloss, softness, high resilience; Two, the mineral mud nutrition emulsion that prepared by the present invention can meet people's demand in delay skin aging, alleviation outside stimulus, climate change, environmental effect etc.; Three, the preparation method technique of mineral mud nutrition emulsion of the present invention is simple, easy to operate; Four, the sludge extracting solution with looks improving and the skin nourishing effect is applied in product emulsion by the present invention, by the comprehensive function of various beneficial element, promotes skin to the absorption of nutritional labeling, and effectively pins moisture, make skin obtain basic nursing.
Detailed description of the invention
Detailed description of the invention one: a kind of mineral mud nutrition emulsion of present embodiment is by mass percentage by 3% ~ 3.5% stearic acid, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 2% ~ 4% lanoline, 5% ~ 7% water-soluble silicon oil, 5% ~ 7% sludge oil-soluble extracting solution, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben, 0.1% ~ 0.3% methyl hydroxybenzoate, 0.01% ~ 0.05% essence and surplus are that sludge water-soluble extracting liquid forms through emulsifying.
Mineral mud nutrition emulsion described in present embodiment can provide abundant nutritional labeling to skin, makes skin gloss, softness, high resilience.
Detailed description of the invention two: present embodiment and detailed description of the invention one unlike: described sludge water-soluble extracting liquid is prepared according to the following steps: one, prepare sludge powder: low whipping speed is under the condition of 20r/min ~ 50r/min, be the Wudalianchi Volcanic sludge of 25% ~ 30% and the mass ratio of mineral water by moisture content being 1:(2 ~ 3.5) mineral water to be joined moisture content be stir in the Wudalianchi Volcanic sludge of 25% ~ 30%, obtain slime water, at room temperature, the slime water obtained is crossed 700 mesh sieves, be removed the slime water of volcanic pisolite and root system of plant, then at room temperature dry 15 days ~ 20 days, finally pulverized 600 mesh sieves, obtain the sludge powder of moisture content < 1%, two, Centrifugical extraction: low whipping speed is under the condition of 20r/min ~ 50r/min, be that mineral water to join in the sludge powder of moisture content < 1% and stirs 24h ~ 30h by 10:1 by the mass ratio of the sludge powder of mineral water and moisture content < 1%, obtain the mud mixture stirred, then be centrifugal 10min ~ 15min under the condition of 3000r/min ~ 4000r/min at rotating speed by the mud mixture stirred, obtain clear liquor and deposit, then be extractant Centrifugical extraction 2 times ~ 3 times again with mineral water by the deposit obtained, merge the clear liquor of gained, namely sludge water-soluble extracting liquid is obtained, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that mineral water joins in deposit by 3:1 by mineral water and sedimental mass ratio, be centrifugal 8min ~ 10min under the condition of 3000r/min ~ 4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.Other is identical with detailed description of the invention one.
Mineral water described in present embodiment is through pipeline disinfection by ultraviolet light, the Wudalianchi metasilicic acid mineral water filtered by filtering with microporous membrane device, not containing oxidizable ferrum, manganese in the metasilicic acid mineral water of Wudalianchi.
Detailed description of the invention three: present embodiment and detailed description of the invention one or two unlike: described sludge oil-soluble extracting solution is prepared according to the following steps: one, prepare sludge powder: low whipping speed is under the condition of 20r/min ~ 50r/min, be the Wudalianchi Volcanic sludge of 25% ~ 30% and the mass ratio of mineral water by moisture content being 1:(2 ~ 3.5) mineral water to be joined moisture content be stir in the Wudalianchi Volcanic sludge of 25% ~ 30%, obtain slime water, at room temperature, the slime water obtained is crossed 700 mesh sieves, be removed the slime water of volcanic pisolite and root system of plant, then at room temperature dry 15 days ~ 20 days, finally pulverized 600 mesh sieves, obtain the sludge powder of moisture content < 1%, two, Centrifugical extraction: low whipping speed is under the condition of 10r/min ~ 30r/min, be that squalane to join in the sludge powder of moisture content < 1% and stirs 24h ~ 30h by 5:1 by the mass ratio of the sludge powder of squalane and moisture content < 1%, obtain the mixture of mud and the squalane stirred, then be centrifugal 10min ~ 15min under the condition of 3000r/min ~ 4000r/min at rotating speed by the mixture of the mud stirred and squalane, obtain clear liquor and deposit, then be extractant Centrifugical extraction 2 times ~ 3 times again with squalane by the deposit obtained, merge the clear liquor of gained, namely sludge oil-soluble extracting solution is obtained, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that squalane joins in deposit by 3:1 by squalane and sedimental mass ratio, be centrifugal 8min ~ 10min under the condition of 3000r/min ~ 4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.Other is identical with detailed description of the invention one or two.
Mineral water described in present embodiment is through pipeline disinfection by ultraviolet light, the Wudalianchi metasilicic acid mineral water filtered by filtering with microporous membrane device, not containing oxidizable ferrum, manganese in the metasilicic acid mineral water of Wudalianchi.
Detailed description of the invention four: the preparation method of a kind of mineral mud nutrition emulsion of present embodiment, carry out according to the following steps:
One, take each component: take 3% ~ 3.5% stearic acid by mass percentage, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 2% ~ 4% lanoline, 5% ~ 7% water-soluble silicon oil, 5% ~ 7% sludge oil-soluble extracting solution, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben, 0.1% ~ 0.3% methyl hydroxybenzoate, 0.01% ~ 0.05% essence and surplus are sludge water-soluble extracting liquid, two, oil mixture is prepared: low whipping speed is under the condition of 80r/min ~ 100r/min, 3% ~ 3.5% stearic acid step one taken, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 0.1% ~ 0.3% methyl hydroxybenzoate, 2% ~ 4% lanoline, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine and 5% ~ 7% sludge oil-soluble extracting solution mixing and stirring are also heated to 70 DEG C ~ 85 DEG C from room temperature, obtain oil mixture, three, aqueous mixture is prepared: low whipping speed is under the condition of 100r/min ~ 150r/min, 5% ~ 7% water-soluble silicon oil step one taken, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben and surplus are sludge water-soluble extracting liquid mixing and stirring and are heated to 80 DEG C ~ 90 DEG C from room temperature, then continue to stir 20min ~ 30min, obtain aqueous mixture, four, emulsifying: oil mixture step 2 obtained joins in the aqueous mixture that step 3 obtains, at the emulsified homogenizing 5min ~ 10min of condition that speed is 2500r/min ~ 3000r/min, be cooled to 30 DEG C ~ 50 DEG C, obtain water oil mixture, then 0.01% ~ 0.05% essence step one taken joins in water oil mixture, continue to stir 10min ~ 20min, be cooled to room temperature, namely obtain mineral mud nutrition emulsion.
Mineral mud nutrition emulsion prepared by present embodiment can provide abundant nutritional labeling to skin, makes skin gloss, softness, high resilience.
The preparation method technique of present embodiment is simple, easy to operate.
Detailed description of the invention five: present embodiment and detailed description of the invention four unlike: the sludge water-soluble extracting liquid described in step one is prepared according to the following steps: one, prepare sludge powder: low whipping speed is under the condition of 20r/min ~ 50r/min, be the Wudalianchi Volcanic sludge of 25% ~ 30% and the mass ratio of mineral water by moisture content being 1:(2 ~ 3.5) mineral water to be joined moisture content be stir in the Wudalianchi Volcanic sludge of 25% ~ 30%, obtain slime water, at room temperature, the slime water obtained is crossed 700 mesh sieves, be removed the slime water of volcanic pisolite and root system of plant, then at room temperature dry 15 days ~ 20 days, finally pulverized 600 mesh sieves, obtain the sludge powder of moisture content < 1%, two, Centrifugical extraction: low whipping speed is under the condition of 20r/min ~ 50r/min, be that mineral water to join in the sludge powder of moisture content < 1% and stirs 24h ~ 30h by 10:1 by the mass ratio of the sludge powder of mineral water and moisture content < 1%, obtain the mud mixture stirred, then be centrifugal 10min ~ 15min under the condition of 3000r/min ~ 4000r/min at rotating speed by the mud mixture stirred, obtain clear liquor and deposit, then be extractant Centrifugical extraction 2 times ~ 3 times again with mineral water by the deposit obtained, merge the clear liquor of gained, namely sludge water-soluble extracting liquid is obtained, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that mineral water joins in deposit by 3:1 by mineral water and sedimental mass ratio, be centrifugal 8min ~ 10min under the condition of 3000r/min ~ 4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.Other and detailed description of the invention four.
Mineral water described in present embodiment is through pipeline disinfection by ultraviolet light, the Wudalianchi metasilicic acid mineral water filtered by filtering with microporous membrane device, not containing oxidizable ferrum, manganese in the metasilicic acid mineral water of Wudalianchi.
Detailed description of the invention six: present embodiment and detailed description of the invention four or five unlike: the sludge oil-soluble extracting solution described in step one is prepared according to the following steps: one, prepare sludge powder: low whipping speed is under the condition of 20r/min ~ 50r/min, be the Wudalianchi Volcanic sludge of 25% ~ 30% and the mass ratio of mineral water by moisture content being 1:(2 ~ 3.5) mineral water to be joined moisture content be stir in the Wudalianchi Volcanic sludge of 25% ~ 30%, obtain slime water, at room temperature, the slime water obtained is crossed 700 mesh sieves, be removed the slime water of volcanic pisolite and root system of plant, then at room temperature dry 15 days ~ 20 days, finally pulverized 600 mesh sieves, obtain the sludge powder of moisture content < 1%, two, Centrifugical extraction: low whipping speed is under the condition of 10r/min ~ 30r/min, be that squalane to join in the sludge powder of moisture content < 1% and stirs 24h ~ 30h by 5:1 by the mass ratio of the sludge powder of squalane and moisture content < 1%, obtain the mixture of mud and the squalane stirred, then be centrifugal 10min ~ 15min under the condition of 3000r/min ~ 4000r/min at rotating speed by the mixture of the mud stirred and squalane, obtain clear liquor and deposit, then be extractant Centrifugical extraction 2 times ~ 3 times again with squalane by the deposit obtained, merge the clear liquor of gained, namely sludge oil-soluble extracting solution is obtained, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that squalane joins in deposit by 3:1 by squalane and sedimental mass ratio, be centrifugal 8min ~ 10min under the condition of 3000r/min ~ 4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.Other is identical with detailed description of the invention four or five.
Mineral water described in present embodiment is through pipeline disinfection by ultraviolet light, the Wudalianchi metasilicic acid mineral water filtered by filtering with microporous membrane device, not containing oxidizable ferrum, manganese in the metasilicic acid mineral water of Wudalianchi.
Detailed description of the invention seven: one of present embodiment and detailed description of the invention four to six unlike: under in step 2, low whipping speed is the condition of 90r/min ~ 100r/min, 3% ~ 3.5% stearic acid step one taken, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 0.1% ~ 0.3% methyl hydroxybenzoate, 2% ~ 4% lanoline, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine and 5% ~ 7% sludge oil-soluble extracting solution mixing and stirring are also heated to 75 DEG C ~ 80 DEG C from room temperature, obtain oil mixture.Other is identical with one of detailed description of the invention four to six.
Detailed description of the invention eight: one of present embodiment and detailed description of the invention four to seven unlike: under in step 3, low whipping speed is the condition of 100r/min ~ 150r/min, 5% ~ 7% water-soluble silicon oil step one taken, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben and surplus are sludge water-soluble extracting liquid mixing and stirring and are heated to 80 DEG C ~ 85 DEG C from room temperature, then continue to stir 25min ~ 30min, obtain aqueous mixture.Other is identical with one of detailed description of the invention four to seven.
Detailed description of the invention nine: one of present embodiment and detailed description of the invention four to eight unlike: in step 4, the oil mixture that step 2 obtains is joined in the aqueous mixture that step 3 obtains, at the emulsified homogenizing 10min of condition that speed is 3000r/min, be cooled to 30 DEG C, obtain water oil mixture, then 0.01% ~ 0.05% essence step one taken joins in water oil mixture, continue to stir 20min, be cooled to room temperature, namely obtain mineral mud nutrition emulsion.Other is identical with one of detailed description of the invention four to eight.
Adopt following verification experimental verification effect of the present invention:
Test one: a kind of preparation method of mineral mud nutrition emulsion, carry out according to the following steps:
One, each component is taken: take 3.2g stearic acid, 4g octadecanol, 3g monoglyceride, 4g isopropyl palmitate, 3g lanoline, 6g water-soluble silicon oil, 5g sludge oil-soluble extracting solution, 4.5g alkyl phosphate, 1.5g triethanolamine, 5g propylene glycol, 9g glycerol, 0.2g propylparaben, 0.2g methyl hydroxybenzoate, 0.02g essence and 51.38g sludge water-soluble extracting liquid; Two, oil mixture is prepared: low whipping speed is under the condition of 100r/min, 3.2g stearic acid step one taken, 4g octadecanol, 3g monoglyceride, 4g isopropyl palmitate, 0.2g methyl hydroxybenzoate, 3g lanoline, 4.5g alkyl phosphate, 1.5g triethanolamine and 5g sludge oil-soluble extracting solution mixing and stirring are also heated to 80 DEG C from room temperature, obtain oil mixture; Three, aqueous mixture is prepared: low whipping speed is under the condition of 150r/min, 6g water-soluble silicon oil step one taken, 5g propylene glycol, 9g glycerol, 0.2g propylparaben and 51.38g sludge water-soluble extracting liquid mixing and stirring are also heated to 85 DEG C from room temperature, then continue to stir 30min, obtain aqueous mixture; Four, emulsifying: oil mixture step 2 obtained joins in the aqueous mixture that step 3 obtains, at the emulsified homogenizing 10min of condition that speed is 2500r/min, be cooled to 40 DEG C, obtain water oil mixture, then 0.02g essence step one taken joins in water oil mixture, continue to stir 20min, be cooled to room temperature, namely obtain mineral mud nutrition emulsion.
Sludge water-soluble extracting liquid described in this test procedure one is prepared according to the following steps: one, prepare sludge powder: low whipping speed is under the condition of 40r/min, by moisture content, to be the Wudalianchi Volcanic sludge of 30% and the mass ratio of mineral water be that mineral water joins moisture content by 1:3 is stir in the Wudalianchi Volcanic sludge of 30%, obtain slime water, at room temperature, the slime water obtained is crossed 700 mesh sieves, be removed the slime water of volcanic pisolite and root system of plant, then at room temperature dry 20 days, finally pulverized 600 mesh sieves, obtain the sludge powder that moisture content is 0.3%, two, Centrifugical extraction: low whipping speed is under the condition of 50r/min, 300g mineral water being joined 30g moisture content is stir 24h in the sludge powder of 0.3%, obtain the mud mixture stirred, then be centrifugal 10min under the condition of 4000r/min at rotating speed by the mud mixture stirred, obtain clear liquor and deposit, then be extractant Centrifugical extraction 3 times again with mineral water by the deposit obtained, merge the clear liquor of gained, namely obtain sludge water-soluble extracting liquid, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that mineral water joins in deposit by 3:1 by mineral water and sedimental mass ratio, is centrifugal 10min under the condition of 4000r/min, namely completes sedimental Centrifugical extraction at rotating speed, wherein said mineral water is through pipeline disinfection by ultraviolet light, the Wudalianchi metasilicic acid mineral water filtered by filtering with microporous membrane device.
Sludge oil-soluble extracting solution described in this test procedure one is prepared according to the following steps: one, prepare sludge powder: low whipping speed is under the condition of 40r/min, by moisture content, to be the Wudalianchi Volcanic sludge of 30% and the mass ratio of mineral water be that mineral water joins moisture content by 1:3 is stir in the Wudalianchi Volcanic sludge of 30%, obtain slime water, at room temperature, the slime water obtained is crossed 700 mesh sieves, be removed the slime water of volcanic pisolite and root system of plant, then at room temperature dry 20 days, finally pulverized 600 mesh sieves, obtain the sludge powder that moisture content is 0.3%, two, Centrifugical extraction: low whipping speed is under the condition of 20r/min, 150g squalane being joined 30g moisture content is stir 24h in the sludge powder of 0.3%, obtain the mixture of mud and the squalane stirred, then be centrifugal 10min under the condition of 4000r/min at rotating speed by the mixture of the mud stirred and squalane, obtain clear liquor and deposit, then be extractant Centrifugical extraction 3 times again with squalane by the deposit obtained, merge the clear liquor of gained, namely obtain sludge oil-soluble extracting solution, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that squalane joins in deposit by 3:1 by squalane and sedimental mass ratio, is centrifugal 10min under the condition of 4000r/min, namely completes sedimental Centrifugical extraction at rotating speed, wherein said mineral water is through pipeline disinfection by ultraviolet light, the Wudalianchi metasilicic acid mineral water filtered by filtering with microporous membrane device.
Test two: mineral mud nutrition emulsion test prepared by test one, method of testing is carried out according to the following steps:
Emulsion is the articles for use being applied directly to skin, so easy to use and have comfortable use sense to be determine that value of the product and consumer are to the key factor of this product ratings.Sensory evaluation is the subjective assessment in using emulsion and after using, and carries out overall merit in conjunction with skin physiology characteristic, permeability principle.
Test result: in evaluation, adopts scoring method of inspection to carry out sense organ evaluation and test, sets up 8 organoleptic indicators, and each organoleptic indicator carries out ten point system marking and evaluates, and sense organ group comprises 10 group members.Test result is as shown in table 1:
Table 1
From test result of use, mineral mud nutrition emulsion viscosity is low, non-greasy, easy to apply, ductility good and fine and smooth, be conducive to skin absorbing from dividing mineral mud nutrition emulsion abundant nutrition composition, moist degree and the salubrious degree of product are higher, and, use rear skin glossy, be conducive to skin and recover nature, resilient health status.
Claims (5)
1. a mineral mud nutrition emulsion, it is characterized in that mineral mud nutrition emulsion by mass percentage by 3% ~ 3.5% stearic acid, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 2% ~ 4% lanoline, 5% ~ 7% water-soluble silicon oil, 5% ~ 7% sludge oil-soluble extracting solution, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben, 0.1% ~ 0.3% methyl hydroxybenzoate, 0.01% ~ 0.05% essence and surplus are that sludge water-soluble extracting liquid forms through emulsifying,
Described sludge water-soluble extracting liquid is prepared according to the following steps: one, prepare sludge powder: low whipping speed is under the condition of 20r/min ~ 50r/min, be the Wudalianchi Volcanic sludge of 25% ~ 30% and the mass ratio of mineral water by moisture content being 1:(2 ~ 3.5) mineral water to be joined moisture content be stir in the Wudalianchi Volcanic sludge of 25% ~ 30%, obtain slime water, at room temperature, the slime water obtained is crossed 700 mesh sieves, be removed the slime water of volcanic pisolite and root system of plant, then at room temperature dry 15 days ~ 20 days, finally pulverized 600 mesh sieves, obtain the sludge powder of moisture content < 1%, two, Centrifugical extraction: low whipping speed is under the condition of 20r/min ~ 50r/min, be that mineral water to join in the sludge powder of moisture content < 1% and stirs 24h ~ 30h by 10:1 by the mass ratio of the sludge powder of mineral water and moisture content < 1%, obtain the mud mixture stirred, then be centrifugal 10min ~ 15min under the condition of 3000r/min ~ 4000r/min at rotating speed by the mud mixture stirred, obtain clear liquor and deposit, then be extractant Centrifugical extraction 2 times ~ 3 times again with mineral water by the deposit obtained, merge the clear liquor of gained, namely sludge water-soluble extracting liquid is obtained, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that mineral water joins in deposit by 3:1 by mineral water and sedimental mass ratio, be centrifugal 8min ~ 10min under the condition of 3000r/min ~ 4000r/min at rotating speed, namely complete sedimental Centrifugical extraction,
Described sludge oil-soluble extracting solution is prepared according to the following steps: one, prepare sludge powder: low whipping speed is under the condition of 20r/min ~ 50r/min, be the Wudalianchi Volcanic sludge of 25% ~ 30% and the mass ratio of mineral water by moisture content being 1:(2 ~ 3.5) mineral water to be joined moisture content be stir in the Wudalianchi Volcanic sludge of 25% ~ 30%, obtain slime water, at room temperature, the slime water obtained is crossed 700 mesh sieves, be removed the slime water of volcanic pisolite and root system of plant, then at room temperature dry 15 days ~ 20 days, finally pulverized 600 mesh sieves, obtain the sludge powder of moisture content < 1%, two, Centrifugical extraction: low whipping speed is under the condition of 10r/min ~ 30r/min, be that squalane to join in the sludge powder of moisture content < 1% and stirs 24h ~ 30h by 5:1 by the mass ratio of the sludge powder of squalane and moisture content < 1%, obtain the mixture of mud and the squalane stirred, then be centrifugal 10min ~ 15min under the condition of 3000r/min ~ 4000r/min at rotating speed by the mixture of the mud stirred and squalane, obtain clear liquor and deposit, then be extractant Centrifugical extraction 2 times ~ 3 times again with squalane by the deposit obtained, merge the clear liquor of gained, namely sludge oil-soluble extracting solution is obtained, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that squalane joins in deposit by 3:1 by squalane and sedimental mass ratio, be centrifugal 8min ~ 10min under the condition of 3000r/min ~ 4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.
2. the preparation method of a kind of mineral mud nutrition emulsion as claimed in claim 1, is characterized in that the preparation method of mineral mud nutrition emulsion is carried out according to the following steps:
One, take each component: take 3% ~ 3.5% stearic acid by mass percentage, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 2% ~ 4% lanoline, 5% ~ 7% water-soluble silicon oil, 5% ~ 7% sludge oil-soluble extracting solution, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben, 0.1% ~ 0.3% methyl hydroxybenzoate, 0.01% ~ 0.05% essence and surplus are sludge water-soluble extracting liquid, two, oil mixture is prepared: low whipping speed is under the condition of 80r/min ~ 100r/min, 3% ~ 3.5% stearic acid step one taken, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 0.1% ~ 0.3% methyl hydroxybenzoate, 2% ~ 4% lanoline, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine and 5% ~ 7% sludge oil-soluble extracting solution mixing and stirring are also heated to 70 DEG C ~ 85 DEG C from room temperature, obtain oil mixture, three, aqueous mixture is prepared: low whipping speed is under the condition of 100r/min ~ 150r/min, 5% ~ 7% water-soluble silicon oil step one taken, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben and sludge water-soluble extracting liquid mixing and stirring are also heated to 80 DEG C ~ 90 DEG C from room temperature, then continue to stir 20min ~ 30min, obtain aqueous mixture, four, emulsifying: oil mixture step 2 obtained joins in the aqueous mixture that step 3 obtains, at the emulsified homogenizing 5min ~ 10min of condition that speed is 2500r/min ~ 3000r/min, be cooled to 30 DEG C ~ 50 DEG C, obtain water oil mixture, then 0.01% ~ 0.05% essence step one taken joins in water oil mixture, continue to stir 10min ~ 20min, be cooled to room temperature, namely obtain mineral mud nutrition emulsion, sludge water-soluble extracting liquid described in step one is prepared according to the following steps: one, prepare sludge powder: low whipping speed is under the condition of 20r/min ~ 50r/min, be the Wudalianchi Volcanic sludge of 25% ~ 30% and the mass ratio of mineral water by moisture content being 1:(2 ~ 3.5) mineral water to be joined moisture content be stir in the Wudalianchi Volcanic sludge of 25% ~ 30%, obtain slime water, at room temperature, the slime water obtained is crossed 700 mesh sieves, be removed the slime water of volcanic pisolite and root system of plant, then at room temperature dry 15 days ~ 20 days, finally pulverized 600 mesh sieves, obtain the sludge powder of moisture content < 1%, two, Centrifugical extraction: low whipping speed is under the condition of 20r/min ~ 50r/min, be that mineral water to join in the sludge powder of moisture content < 1% and stirs 24h ~ 30h by 10:1 by the mass ratio of the sludge powder of mineral water and moisture content < 1%, obtain the mud mixture stirred, then be centrifugal 10min ~ 15min under the condition of 3000r/min ~ 4000r/min at rotating speed by the mud mixture stirred, obtain clear liquor and deposit, then be extractant Centrifugical extraction 2 times ~ 3 times again with mineral water by the deposit obtained, merge the clear liquor of gained, namely sludge water-soluble extracting liquid is obtained, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that mineral water joins in deposit by 3:1 by mineral water and sedimental mass ratio, be centrifugal 8min ~ 10min under the condition of 3000r/min ~ 4000r/min at rotating speed, namely complete sedimental Centrifugical extraction,
Sludge oil-soluble extracting solution described in step one is prepared according to the following steps: one, prepare sludge powder: low whipping speed is under the condition of 20r/min ~ 50r/min, be the Wudalianchi Volcanic sludge of 25% ~ 30% and the mass ratio of mineral water by moisture content being 1:(2 ~ 3.5) mineral water to be joined moisture content be stir in the Wudalianchi Volcanic sludge of 25% ~ 30%, obtain slime water, at room temperature, the slime water obtained is crossed 700 mesh sieves, be removed the slime water of volcanic pisolite and root system of plant, then at room temperature dry 15 days ~ 20 days, finally pulverized 600 mesh sieves, obtain the sludge powder of moisture content < 1%, two, Centrifugical extraction: low whipping speed is under the condition of 10r/min ~ 30r/min, be that squalane to join in the sludge powder of moisture content < 1% and stirs 24h ~ 30h by 5:1 by the mass ratio of the sludge powder of squalane and moisture content < 1%, obtain the mixture of mud and the squalane stirred, then be centrifugal 10min ~ 15min under the condition of 3000r/min ~ 4000r/min at rotating speed by the mixture of the mud stirred and squalane, obtain clear liquor and deposit, then be extractant Centrifugical extraction 2 times ~ 3 times again with squalane by the deposit obtained, merge the clear liquor of gained, namely sludge oil-soluble extracting solution is obtained, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that squalane joins in deposit by 3:1 by squalane and sedimental mass ratio, be centrifugal 8min ~ 10min under the condition of 3000r/min ~ 4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.
3. the preparation method of a kind of mineral mud nutrition emulsion according to claim 2, it is characterized in that in step 2, low whipping speed is under the condition of 90r/min ~ 100r/min, 3% ~ 3.5% stearic acid that step one is taken, 4% ~ 5% octadecanol, 2% ~ 3% monoglyceride, 3% ~ 5% isopropyl palmitate, 0.1% ~ 0.3% methyl hydroxybenzoate, 2% ~ 4% lanoline, 4% ~ 5% alkyl phosphate, 1.5% ~ 2.5% triethanolamine and 5% ~ 7% sludge oil-soluble extracting solution mixing and stirring are also heated to 75 DEG C ~ 80 DEG C from room temperature, obtain oil mixture.
4. the preparation method of a kind of mineral mud nutrition emulsion according to claim 2, it is characterized in that in step 3, low whipping speed is under the condition of 100r/min ~ 150r/min, 5% ~ 7% water-soluble silicon oil step one taken, 1% ~ 3% propylene glycol, 8% ~ 9% glycerol, 0.1% ~ 0.3% propylparaben and sludge water-soluble extracting liquid mixing and stirring are also heated to 80 DEG C ~ 85 DEG C from room temperature, then continue to stir 25min ~ 30min, obtain aqueous mixture.
5. the preparation method of a kind of mineral mud nutrition emulsion according to claim 2, it is characterized in that in step 4, the oil mixture that step 2 obtains being joined in the aqueous mixture that step 3 obtains, at the emulsified homogenizing 10min of condition that speed is 3000r/min, be cooled to 30 DEG C, obtain water oil mixture, 0.01% ~ 0.05% essence then step one taken joins in water oil mixture, continues to stir 20min, be cooled to room temperature, namely obtain mineral mud nutrition emulsion.
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| CN105078770A (en) * | 2014-05-20 | 2015-11-25 | 李复兴 | Preparation method of mineral cleaning and maintaining ingot |
| CN104666128B (en) * | 2015-03-16 | 2017-07-18 | 黑龙江省科学院火山与矿泉研究所 | Volcanic mud essence spray mask |
| CN105232369B (en) * | 2015-09-28 | 2018-09-28 | 黑龙江省科学院火山与矿泉研究所 | Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof |
| CN106074855A (en) * | 2016-07-25 | 2016-11-09 | 王波林 | A kind of absorption sludge |
| CN106074231B (en) * | 2016-08-03 | 2019-04-02 | 黑龙江省科学院火山与矿泉研究所 | Slime skin-cleaning gel and preparation method thereof |
| CN107080724A (en) * | 2017-04-19 | 2017-08-22 | 北海蓝晖环保科技有限公司 | Nti-freckle anti-wrinkle cream |
| CN107137302A (en) * | 2017-04-19 | 2017-09-08 | 北海蓝晖环保科技有限公司 | Compound face cream |
| CN110101613B (en) * | 2019-06-24 | 2022-03-22 | 黑龙江省科学院火山与矿泉研究所 | Natural skin-care volcanic mud particle emulsified oil-in-water emulsion and preparation method thereof |
| CN110179699B (en) * | 2019-06-24 | 2022-03-22 | 黑龙江省科学院火山与矿泉研究所 | Natural skin-care volcanic mud particle emulsified water-in-oil emulsion and preparation method thereof |
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| CN102068389A (en) * | 2010-09-06 | 2011-05-25 | 厦门澳丽尔日化有限公司 | Micro-emulsified environmentally-friendly facial treatment milk and preparation method thereof |
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| CN1252266A (en) * | 1998-10-28 | 2000-05-10 | 黑龙江省科学院火山矿泉资源研究所 | Beautifying skincare slime paste and its compounding process |
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