CN103103595B - Ultrasonic wave bright clean-out system and preparation method before the anodic oxidation of high ferro vehicle special die casting aluminium workpiece - Google Patents

Ultrasonic wave bright clean-out system and preparation method before the anodic oxidation of high ferro vehicle special die casting aluminium workpiece Download PDF

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Publication number
CN103103595B
CN103103595B CN201210452731.0A CN201210452731A CN103103595B CN 103103595 B CN103103595 B CN 103103595B CN 201210452731 A CN201210452731 A CN 201210452731A CN 103103595 B CN103103595 B CN 103103595B
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raw material
out system
die casting
preparation
anodic oxidation
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CN103103595A (en
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潘德顺
黄文飞
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Dalian Sandaaoke Chemistry Co Ltd
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Dalian Sandaaoke Chemistry Co Ltd
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Abstract

The present invention discloses Ultrasonic wave bright clean-out system before the anodic oxidation of a kind of high ferro vehicle special die casting aluminium workpiece, be made up of the component of following mass percent: potassium pyrophosphate 1 ~ 3%, borax 1 ~ 3%, tripoly phosphate sodium STPP 0.5 ~ 2.5%, metasilicate pentahydrate sodium 0.5 ~ 2.5%, trolamine 1 ~ 5%, promoting agent (QYL-20) 0.1 ~ 1.0%, AEO-9? 1 ~ 2%, alizarin assistant 1 ~ 2%, pull open powder 0.1 ~ 1.0%, JFC? 0.1 ~ 1.0%, defoamer 0.1 ~ 0.6% and deionized water surplus.Deionized water first joins in stainless steel cauldron by preparation method, starts agitator, and rotating speed is 60 revs/min, is slowly joined in reactor by solid part raw material, often adds a kind of raw material and all stirs at least 15 minutes; Slowly joined successively in reactor by liquid part raw material, often add a kind of raw material and all stir at least 10 minutes, being continuously stirring to solution is light brown clear liquid.

Description

Ultrasonic wave bright clean-out system and preparation method before the anodic oxidation of high ferro vehicle special die casting aluminium workpiece
Technical field
The present invention relates to a kind of aluminium matter workpiece ultrasonic cleaning agent, especially a kind of dirt can thoroughly removed on workpiece, ensure cleanliness factor and the luminance brightness of workpiece surface, Ultrasonic wave bright clean-out system and preparation method before the anodic oxidation of long-lived high ferro vehicle special die casting aluminium workpiece.
Background technology
Metal cleans, adopt corresponding processing unit and processing condition exactly, with specific solution, the dirt removal on metal products workpiece surface is fallen, product is made to reach the technical requirements of design, as ultrasonic cleaning, steam purge, high pressure cleaning, ozone-ultraviolet cleaning, ion beam cleaning and plasma clean etc., just need to carry out ultrasonic cleaning to it before die casting aluminium workpiece as special in high ferro vehicle anodic oxidation.There are two technical problems in existing high ferro vehicle special die casting aluminium workpiece anodic oxidation fore shell ultrasonic cleaning agent: one is that after cleaning, workpiece surface luminance brightness is not up to standard always; Two is that the cleaning liquid life-span is short, and every day is changed once, and cleaning cost is high.
Summary of the invention
The present invention is the above-mentioned technical problem in order to solve existing for prior art, a kind of dirt can thoroughly removed on workpiece is provided, ensures the cleanliness factor of workpiece surface and luminance brightness and Ultrasonic wave bright clean-out system and preparation method before the anodic oxidation of long-lived high ferro vehicle special die casting aluminium workpiece.
Technical solution of the present invention is: Ultrasonic wave bright clean-out system before the anodic oxidation of a kind of high ferro vehicle special die casting aluminium workpiece, is made up of the component of following mass percent: potassium pyrophosphate 1 ~ 3%, borax 1 ~ 3%, tripoly phosphate sodium STPP 0.5 ~ 2.5%, metasilicate pentahydrate sodium 0.5 ~ 2.5%, trolamine 1 ~ 5%, promoting agent (QYL-20) 0.1 ~ 1.0%, AEO-91 ~ 2%, alizarin assistant 1 ~ 2%, pull open powder 0.1 ~ 1.0%, JFC0.1 ~ 1.0%, defoamer 0.1 ~ 0.6% and deionized water surplus.
The preparation method of Ultrasonic wave bright clean-out system before a kind of above-mentioned high ferro vehicle special die casting aluminium workpiece anodic oxidation, it is characterized in that carrying out as follows: first join in stainless steel cauldron by calculating the deionized water weighed, start agitator, rotating speed is 60 revs/min, by calculate weigh solid part raw material potassium pyrophosphate, borax, tripoly phosphate sodium STPP, trisodium phosphate, metasilicate pentahydrate sodium, pull open powder and slowly join successively in reactor, often add a kind of raw material and all stir at least 15 minutes; Liquid part raw material trolamine calculating weighed again, promoting agent (QYL-20), AEO-9, alizarin assistant, JFC, defoamer join in reactor successively slowly, often add a kind of raw material and all stir at least 10 minutes, being continuously stirring to solution is light brown clear liquid.
The present invention is the acidic cleaner being applicable to ultrasonic cleaning, effectively can remove the dirt of the special die casting aluminium workpiece surface of high ferro vehicle, ensure that cleanliness factor and the luminance brightness of workpiece surface, reaches the specification of quality before anodic oxidation.And the usage period long (three days), reduce the production cost of the special die casting aluminium workpiece of high ferro vehicle, and No oxidation discoloration phenomenon in six months after cleaning.
Embodiment
Embodiment 1:
Each component and mass percent as follows: be made up of the component of following mass percent: potassium pyrophosphate 1%, borax 3%, tripoly phosphate sodium STPP 0.5%, metasilicate pentahydrate sodium 2.5%, trolamine 1%, promoting agent (QYL-20) 1.0%, AEO-91%, alizarin assistant 2%, pull open powder 0.1%, JFC1.0%, defoamer (MS-575) 0.1% and deionized water surplus.
Preparation method carries out as follows: first join in stainless steel cauldron by calculating the deionized water weighed, start agitator, rotating speed is 60 revs/min, by calculate weigh solid part raw material potassium pyrophosphate, borax, tripoly phosphate sodium STPP, trisodium phosphate, metasilicate pentahydrate sodium, pull open powder and slowly join successively in reactor, often add a kind of raw material and all stir at least 15 minutes; Liquid part raw material trolamine calculating weighed again, promoting agent (QYL-20), AEO-9, alizarin assistant, JFC, defoamer join in reactor successively slowly, often add a kind of raw material and all stir at least 10 minutes, being continuously stirring to solution is light brown clear liquid.
Raw materials usedly adopt commercially available prod, wherein promoting agent (QYL-20) is the product of Qi Yanglong Science and Technology Ltd. of Shenzhen public offering, and product type is QYL-20.
Embodiment 2:
Each component and mass percent as follows: potassium pyrophosphate 3%, borax 1%, tripoly phosphate sodium STPP 2.5%, metasilicate pentahydrate sodium 0.5%, trolamine 5%, promoting agent (QYL-20) 0.1%, AEO-92%, alizarin assistant 1%, pull open powder 1.0%, JFC0.1%, defoamer (MS-575) 0.6% and deionized water surplus.
Raw material sources and preparation method are with embodiment 1.
Embodiment 3:
Potassium pyrophosphate 2%, borax 2%, tripoly phosphate sodium STPP 1.0%, metasilicate pentahydrate sodium 1.0%, trolamine 3%, promoting agent (QYL-20) 0.5%, AEO-91.5%, alizarin assistant 1.5%, pull open powder 0.5%, JFC0.5%, defoamer (MS-575) 0.3% and deionized water surplus.
Raw material sources and preparation method are with embodiment 1.
During use, adopt deionized water by the embodiment of the present invention 1,2 or 3 by mass concentration be 8 ~ 10% preparation ultrasonic cleaning agents, ultrasonic cleaning schrittmacher Precision Aluminum matter workpiece, 50 ~ 60 DEG C, 4 ~ 8min, reaches bright cleaning degree, meets anodised requirement, No oxidation discoloration within six months, changes once for three days.

Claims (1)

1. the preparation method of Ultrasonic wave bright clean-out system before high ferro vehicle special die casting aluminium workpiece anodic oxidation, described clean-out system is made up of the component of following mass percent: potassium pyrophosphate 1 ~ 3%, borax 1 ~ 3%, tripoly phosphate sodium STPP 0.5 ~ 2.5%, metasilicate pentahydrate sodium 0.5 ~ 2.5%, trolamine 1 ~ 5%, QYL-20 promoting agent 0.1 ~ 1.0%, AEO-91 ~ 2%, alizarin assistant 1 ~ 2%, pull open powder 0.1 ~ 1.0%, JFC0.1 ~ 1.0%, defoamer 0.1 ~ 0.6% and deionized water surplus, it is characterized in that carrying out as follows: first join in stainless steel cauldron by calculating the deionized water weighed, start agitator, rotating speed is 60 revs/min, the solid part raw material potassium pyrophosphate weighed will be calculated, borax, tripoly phosphate sodium STPP, metasilicate pentahydrate sodium, pull open powder slowly to join successively in reactor, often add a kind of raw material and all stir at least 15 minutes, liquid part raw material trolamine calculating weighed again, QYL-20 promoting agent, AEO-9, alizarin assistant, JFC, defoamer join in reactor successively slowly, often add a kind of raw material and all stir at least 10 minutes, being continuously stirring to solution is light brown clear liquid.
CN201210452731.0A 2012-11-13 2012-11-13 Ultrasonic wave bright clean-out system and preparation method before the anodic oxidation of high ferro vehicle special die casting aluminium workpiece Active CN103103595B (en)

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CN108754507B (en) * 2018-05-26 2020-11-10 厦门力九化工有限公司 Ultrasonic cleaning agent, preparation method and use method

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CN101956199A (en) * 2010-11-03 2011-01-26 大连三达奥克化学股份有限公司 Non-phosphorus environment-friendly water-based degreasing agent and manufacturing method thereof
CN102418108A (en) * 2011-12-30 2012-04-18 大连三达奥克化学股份有限公司 Spraying normal temperature degreasing agent for galvanized steel sheet and production method thereof
CN102534634A (en) * 2011-12-30 2012-07-04 大连三达奥克化学股份有限公司 Ultrasonic degreasing agent for cast magnesium alloy workpiece and production method thereof
CN102533421A (en) * 2011-12-30 2012-07-04 大连三达奥克化学股份有限公司 Machining cutting fluid for die casting aluminum alloy to cast motor shell and preparation method
CN102719840A (en) * 2012-06-21 2012-10-10 大连三达奥克化学股份有限公司 Cleaning agent for stainless steel-aluminum alloy plate combined electric kettle and preparation method

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1479959A (en) * 1973-09-26 1977-07-13 Hoeganaes Ab Magnetite article and method of its production
CN101660152A (en) * 2009-09-27 2010-03-03 大连三达奥克化学股份有限公司 Normal-temperature cleaning anti-rust agent of cylinder body of host machine of iron-casting diesel engine and preparation method thereof
CN101956200A (en) * 2010-11-03 2011-01-26 大连三达奥克化学股份有限公司 Non-phosphorus environment-friendly powdery degreasing agent and manufacturing method thereof
CN101956199A (en) * 2010-11-03 2011-01-26 大连三达奥克化学股份有限公司 Non-phosphorus environment-friendly water-based degreasing agent and manufacturing method thereof
CN102418108A (en) * 2011-12-30 2012-04-18 大连三达奥克化学股份有限公司 Spraying normal temperature degreasing agent for galvanized steel sheet and production method thereof
CN102534634A (en) * 2011-12-30 2012-07-04 大连三达奥克化学股份有限公司 Ultrasonic degreasing agent for cast magnesium alloy workpiece and production method thereof
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