CN103086794A - Selenium enrichment soil nutrient and preparation method thereof, and cultivation method of Huangshan tribute chrysanthemum - Google Patents
Selenium enrichment soil nutrient and preparation method thereof, and cultivation method of Huangshan tribute chrysanthemum Download PDFInfo
- Publication number
- CN103086794A CN103086794A CN2013100261613A CN201310026161A CN103086794A CN 103086794 A CN103086794 A CN 103086794A CN 2013100261613 A CN2013100261613 A CN 2013100261613A CN 201310026161 A CN201310026161 A CN 201310026161A CN 103086794 A CN103086794 A CN 103086794A
- Authority
- CN
- China
- Prior art keywords
- selenium
- sodium selenite
- zinc sulfate
- chrysanthemum
- nutrition agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Fertilizers (AREA)
Abstract
The invention discloses a selenium enrichment soil nutrient and a preparation method of the nutrient, and a cultivation method of Huangshan tribute chrysanthemum. The nutrient comprises the following components in parts by weight: 100 parts of attapulgite clay, 0.04-0.06 part of sodium selenite and 10-20 parts of zinc sulfate; the preparation method comprises the following steps of: dissolving, spraying and dewatering. The selenium enrichment soil nutrient disclosed by the invention is uniformly distributed in soil, not easy to run off and long in fertilizer efficiency period, and can be sufficiently absorbed by crops.
Description
Technical field
The invention belongs to field of agricultural production technologies, be specifically related to the cultivating method of a kind of selenium-rich soil nutrition agent and compound method thereof, Huangshan Gongju.
Background technology
The selenium element is the mineral nutrient of needed by human, can't synthesize in human body, and the selenium total content of human body itself is 6-20mg.Selenium spreads all over each histoorgan and body fluid, and in kidney, concentration is the highest, and is extremely important to improving immunizing power and preventing cancer.
China is a scarce selenium big country, and approximately 700,000,000 people live in low selenium area.Scientist measures the selenium content of the pedotheque of 1094 counties and cities of China (account for the whole nation half), and measurement result shows: the county that reaches normal threshold value 0.1 mg/kg of international publication only has 1/3, and namely China 2/3 area belongs to and lacks the selenium area.Wherein content≤0.02 mg/kg account for 29%, be the serious selenium area of lacking.Most area Selenium In Foods content is below 0.02mg/kg, and southeastern coast is China's district rich in selenium, also only has 0.10mg/kg, is the minimum of United Nations's health organization regulation.At present, still do not reach the above standard of everyone 40 micrograms every day in population of China food and mend the selenium level, especially lack selenium area crowd, the more difficult purpose of mending selenium that reaches from food.
In present Mt. Huang in Anhui tribute chrysanthemum cultivation process, the heavy dressing inorganic fertilizer causes the problem of plant sulphur intake deficiency, and the Huangshan Gongju selenium content is very low.
Summary of the invention
For the deficiencies in the prior art, the purpose of this invention is to provide the cultivating method of a kind of selenium-rich soil nutrition agent and compound method thereof, Huangshan Gongju.Selenium-rich soil nutrition agent of the present invention is evenly distributed in soil, be difficult for to run off, and fertilizer efficiency period is long, can fully be absorbed by crop, uses more than the content of the tribute chrysanthemum trace element-selenium of cultivating method production of the present invention reaches 500 microgram/kilograms (dry weight).
The technical solution used in the present invention is:
A kind of selenium-rich soil nutrition agent, its composition of raw materials is take parts by weight component and content as 100 parts of attapulgite clays, Sodium Selenite 0.04-0.06 part, zinc sulfate 10-20 part.
A kind of compound method of selenium-rich soil nutrition agent, step comprises:
A, take Sodium Selenite, zinc sulfate, attapulgite clay by formula ratio, use respectively hot water dissolving's Sodium Selenite, zinc sulfate; Also Sodium Selenite, zinc sulfate first can be mixed dissolving again;
B, the solution that respectively steps A is made evenly are sprayed on attapulgite clay, shake fast attapulgite clay to solution while spraying and fully, evenly adsorb on it, and concussion forms small-particle, concussion frequency 2-5 time/second;
C, increase airiness make it moisture is down to below 40% under the normal temperature state.
In described steps A, the hot water temperature is not less than 80 ℃, and Sodium Selenite, zinc sulfate are dissolved into saturated solution.
A kind of cultivating method of Huangshan Gongju, step comprises:
A, the selenium-rich soil nutrition agent is mixed in basic fertilise, evenly spreads fertilizer over the fields, plough plantation chrysanthemum seedling after soil; To produce 1 mu of basic fertilise of tribute chrysanthemum, in the base fertilising, selenium-rich soil nutrition agent content is: 10 kilograms of attapulgite clays, 1 ~ 2 kilogram, zinc sulfate, Sodium Selenite 4 ~ 6 grams;
B, before the chrysanthemum flower bud forms, to tribute chrysanthemum foliage-spray leaf nutritive agent; To produce 1 mu of tribute chrysanthemum leaf nutritive agent, foliar nutrition agent prescription and consumption are: 10 ~ 20 milliliters of the sodium selenite solutions of 10wt%, 20 ~ 50 milliliters of tween 20s.
Selenium-rich soil nutrition agent of the present invention is evenly distributed in soil, be difficult for to run off, and fertilizer efficiency period is long, can fully be absorbed by crop, uses more than the content of the tribute chrysanthemum trace element-selenium of cultivating method production of the present invention reaches 500 microgram/kilograms (dry weight).
Cultivating method of the present invention, on the basis of conventional Huangshan Gongju planting type, selemium nutrition for rich selenium tribute chrysanthemum transforms demand, add respectively the nutrition agent that contains selenium in basic fertilise before cuttage and the fertilizer for spraying on leaf surface of flower bud before the phase, inorganic states selenium in the selemium nutrition agent is through plant absorbing, change into the organoselenium composition useful to HUMAN HEALTH, thereby produce the Huangshan Gongju of rich selenium.By before the chrysanthemum flower bud forms, the mode of taking foliage-spray to contain selenium fertilizer is carried out primary treatment to plant, reaches the purpose of the rich selenium Huangshan Gongju of production enhancement.
Embodiment
Embodiment 1
A kind of selenium-rich soil nutrition agent, its composition of raw materials be (high 111 types, Anhui Province bright U.S. mineral chemical industry company limited) 100 parts take parts by weight component and content as: attapulgite clay, 0.05 part of Sodium Selenite, 15 parts, zinc sulfate.
A kind of compound method of selenium-rich soil nutrition agent, step comprises:
A, take Sodium Selenite, zinc sulfate, attapulgite clay by formula ratio, use respectively 85 ℃ of hot water dissolving's Sodium Selenites, zinc sulfate, be mixed with saturated solution;
B, the solution that respectively steps A is made evenly are sprayed on attapulgite clay, shake fast attapulgite clay to solution while spraying and fully, evenly adsorb on it, and concussion forms small-particle; Concussion frequency 4 times/second;
C, increase airiness make it moisture is down to 35% under the normal temperature state.
A kind of cultivating method of Huangshan Gongju, step comprises:
A, above-mentioned selenium-rich soil nutrition agent is mixed in basic fertilise, evenly spreads fertilizer over the fields, plough plantation chrysanthemum seedling after soil; To produce 1 mu of basic fertilise of tribute chrysanthemum, in the base fertilising, selenium-rich soil nutrition agent content is: 10 kilograms of attapulgite clays, 1.5 kilograms, zinc sulfate, Sodium Selenite 5 grams;
B, before the chrysanthemum flower bud forms, to tribute chrysanthemum foliage-spray leaf nutritive agent; To produce 1 mu of tribute chrysanthemum leaf nutritive agent, foliar nutrition agent prescription and consumption are: 15 milliliters of the sodium selenite solutions of 10wt%, 35 milliliters of tween 20s; When spraying, leaf nutritive agent is sneaked into mixing in 50 kg of water, spraying.
The content of the tribute chrysanthemum trace element-selenium of the present embodiment cultivating method production is 572 microgram/kilograms (dry weight).
Embodiment 2
A kind of selenium-rich soil nutrition agent, its composition of raw materials is take parts by weight component and content as 100 parts of attapulgite clays, 0.04 part of Sodium Selenite, 10 parts, zinc sulfate.
A kind of compound method of selenium-rich soil nutrition agent, step comprises:
A, take Sodium Selenite, zinc sulfate, attapulgite clay by formula ratio, use respectively 80 ℃ of hot water dissolving's Sodium Selenites, zinc sulfate, be mixed with saturated solution;
B, the solution that respectively steps A is made evenly are sprayed on attapulgite clay, shake fast attapulgite clay to solution while spraying and fully, evenly adsorb on it, and concussion forms small-particle; Concussion frequency 5 times/second;
C, increase airiness make it moisture is down to 40% under the normal temperature state.
A kind of cultivating method of Huangshan Gongju, step comprises:
A, above-mentioned selenium-rich soil nutrition agent is mixed in basic fertilise, evenly spreads fertilizer over the fields, plough plantation chrysanthemum seedling after soil; To produce 1 mu of basic fertilise of tribute chrysanthemum, in the base fertilising, selenium-rich soil nutrition agent content is: 10 kilograms of attapulgite clays, 1 kilogram, zinc sulfate, Sodium Selenite 4 grams;
B, before the chrysanthemum flower bud forms, to tribute chrysanthemum foliage-spray leaf nutritive agent; To produce 1 mu of tribute chrysanthemum leaf nutritive agent, foliar nutrition agent prescription and consumption are: 10 milliliters of the sodium selenite solutions of 10wt%, 20 milliliters of tween 20s; When spraying, leaf nutritive agent is sneaked into mixing in 50 kg of water, spraying.
The content of the tribute chrysanthemum trace element-selenium of the present embodiment cultivating method production is 527 microgram/kilograms (dry weight).
Embodiment 3
A kind of selenium-rich soil nutrition agent, its composition of raw materials is take parts by weight component and content as 100 parts of attapulgite clays, 0.06 part of Sodium Selenite, 20 parts, zinc sulfate.
A kind of compound method of selenium-rich soil nutrition agent, step comprises:
A, take Sodium Selenite, zinc sulfate, attapulgite clay by formula ratio, use respectively 90 ℃ of hot water dissolving's Sodium Selenites, zinc sulfate, be mixed with saturated solution;
B, the solution that respectively steps A is made evenly are sprayed on attapulgite clay, shake fast attapulgite clay to solution while spraying and fully, evenly adsorb on it, and concussion forms small-particle; Concussion frequency 2 times/second;
C, increase airiness make it moisture is down to 30% under the normal temperature state.
A kind of cultivating method of Huangshan Gongju, step comprises:
A, above-mentioned selenium-rich soil nutrition agent is mixed in basic fertilise, evenly spreads fertilizer over the fields, plough plantation chrysanthemum seedling after soil; To produce 1 mu of basic fertilise of tribute chrysanthemum, in the base fertilising, selenium-rich soil nutrition agent content is: 10 kilograms of attapulgite clays, 2 kilograms, zinc sulfate, Sodium Selenite 6 grams;
B, before the chrysanthemum flower bud forms, to tribute chrysanthemum foliage-spray leaf nutritive agent; To produce 1 mu of tribute chrysanthemum leaf nutritive agent, foliar nutrition agent prescription and consumption are: 20 milliliters of the sodium selenite solutions of 10wt%, 50 milliliters of tween 20s; When spraying, leaf nutritive agent is sneaked into mixing in 50 kg of water, spraying.
The content of the tribute chrysanthemum trace element-selenium of the present embodiment cultivating method production is 608 microgram/kilograms (dry weight).
Embodiment 4
A kind of selenium-rich soil nutrition agent, its composition of raw materials is take parts by weight component and content as 100 parts of attapulgite clays, 0.05 part of Sodium Selenite, 14 parts, zinc sulfate.
A kind of compound method of selenium-rich soil nutrition agent, step comprises:
A, take Sodium Selenite, zinc sulfate, attapulgite clay by formula ratio, use respectively 85 ℃ of hot water dissolving's Sodium Selenites, zinc sulfate, be mixed with saturated solution;
B, the solution that respectively steps A is made evenly are sprayed on attapulgite clay, shake fast attapulgite clay to solution while spraying and fully, evenly adsorb on it, and concussion forms small-particle; Concussion frequency 3 times/second;
C, increase airiness make it moisture is down to below 40% under the normal temperature state.
A kind of cultivating method of Huangshan Gongju, step comprises:
A, above-mentioned selenium-rich soil nutrition agent is mixed in basic fertilise, evenly spreads fertilizer over the fields, plough plantation chrysanthemum seedling after soil; To produce 1 mu of basic fertilise of tribute chrysanthemum, in the base fertilising, selenium-rich soil nutrition agent content is: 10 kilograms of attapulgite clays, 1.5 kilograms, zinc sulfate, Sodium Selenite 5 grams;
B, before the chrysanthemum flower bud forms, to tribute chrysanthemum foliage-spray leaf nutritive agent; To produce 1 mu of tribute chrysanthemum leaf nutritive agent, foliar nutrition agent prescription and consumption are: 15 milliliters of the sodium selenite solutions of 10wt%, 40 milliliters of tween 20s; When spraying, leaf nutritive agent is sneaked into mixing in 50 kg of water, spraying.
The content of the tribute chrysanthemum trace element-selenium of the present embodiment cultivating method production is 582 microgram/kilograms (dry weight).
Claims (7)
1. selenium-rich soil nutrition agent, its composition of raw materials is take parts by weight component and content as 100 parts of attapulgite clays, Sodium Selenite 0.04-0.06 part, zinc sulfate 10-20 part.
2. the compound method of a selenium-rich soil nutrition agent, step comprises:
A, take Sodium Selenite, zinc sulfate, attapulgite clay by formula ratio, use respectively hot water dissolving's Sodium Selenite, zinc sulfate;
B, the solution that respectively steps A is made evenly are sprayed on attapulgite clay, shake fast attapulgite clay to solution while spraying and fully, evenly adsorb on it, and concussion forms small-particle;
C, increase airiness make it moisture is down to below 40% under the normal temperature state.
3. compound method as claimed in claim 2, it is characterized in that: in described steps A, the hot water temperature is not less than 80 ℃, and Sodium Selenite, zinc sulfate are dissolved into saturated solution.
4. compound method as claimed in claim 2 is characterized in that: in described step B, the concussion frequency is 2-5 time/second.
5. the cultivating method of a Huangshan Gongju, step comprises:
A, the selenium-rich soil nutrition agent is mixed in basic fertilise, evenly spreads fertilizer over the fields, plough plantation chrysanthemum seedling after soil;
B, before the chrysanthemum flower bud forms, to tribute chrysanthemum foliage-spray leaf nutritive agent.
6. cultivating method as claimed in claim 5 is characterized in that: in described step a, to produce 1 mu of basic fertilise of tribute chrysanthemum, in the base fertilising, selenium-rich soil nutrition agent content is: 10 kilograms of attapulgite clays, 1 ~ 2 kilogram, zinc sulfate, Sodium Selenite 4 ~ 6 grams.
7. cultivating method as claimed in claim 5, it is characterized in that: in described step b, to produce 1 mu of tribute chrysanthemum leaf nutritive agent, foliar nutrition agent prescription and consumption are: 10 ~ 20 milliliters of the sodium selenite solutions of 10wt%, 20 ~ 50 milliliters of tween 20s.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310026161.3A CN103086794B (en) | 2013-01-23 | 2013-01-23 | Selenium enrichment soil nutrient and preparation method thereof, and cultivation method of Huangshan tribute chrysanthemum |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310026161.3A CN103086794B (en) | 2013-01-23 | 2013-01-23 | Selenium enrichment soil nutrient and preparation method thereof, and cultivation method of Huangshan tribute chrysanthemum |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103086794A true CN103086794A (en) | 2013-05-08 |
| CN103086794B CN103086794B (en) | 2015-01-21 |
Family
ID=48199987
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310026161.3A Expired - Fee Related CN103086794B (en) | 2013-01-23 | 2013-01-23 | Selenium enrichment soil nutrient and preparation method thereof, and cultivation method of Huangshan tribute chrysanthemum |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103086794B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103553746A (en) * | 2013-10-30 | 2014-02-05 | 成都新朝阳作物科学有限公司 | Selenium-rich nutrient and application thereof |
| CN105660150A (en) * | 2016-03-02 | 2016-06-15 | 黄山市芽典生态农业有限公司 | Nutrition bowl cultivation method of Huangshan tribute chrysanthemums |
| CN109453736A (en) * | 2018-10-29 | 2019-03-12 | 佛山市铁人环保科技有限公司 | A kind of soil conditioner and preparation method thereof of silicon sulphur selenium zinc multiple elements design attapulgite |
| CN112457120A (en) * | 2021-01-04 | 2021-03-09 | 方连明 | Selenium-rich trace element fertilizer, selenium-rich controlled release fertilizer, preparation method and application thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101496476A (en) * | 2008-02-03 | 2009-08-05 | 凌如文 | Selenium-rich chrysanthemum |
| CN101575223A (en) * | 2008-05-09 | 2009-11-11 | 上海鑫辰实业发展有限公司 | Silicic acid fertilizer |
| CN101768032A (en) * | 2010-01-26 | 2010-07-07 | 安徽省农业科学院土壤肥料研究所 | Fertilizer for medicinal chrysanthemums and production method thereof |
| CN101928190A (en) * | 2010-09-16 | 2010-12-29 | 安徽科技学院 | Fertilizer special for medicinal Chuzhou chrysanthemum and preparation method thereof |
| CN102599305A (en) * | 2012-03-08 | 2012-07-25 | 刘茜 | Selenium-rich chrysanthemum tea or tea |
| CN102617251A (en) * | 2012-04-13 | 2012-08-01 | 常熟市平冶机械有限公司 | Selenium-rich composite organic fertilizer and preparing method thereof |
| CN102617247A (en) * | 2012-04-13 | 2012-08-01 | 常熟市平冶机械有限公司 | Selenium-rich nutrient solution |
-
2013
- 2013-01-23 CN CN201310026161.3A patent/CN103086794B/en not_active Expired - Fee Related
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101496476A (en) * | 2008-02-03 | 2009-08-05 | 凌如文 | Selenium-rich chrysanthemum |
| CN101575223A (en) * | 2008-05-09 | 2009-11-11 | 上海鑫辰实业发展有限公司 | Silicic acid fertilizer |
| CN101768032A (en) * | 2010-01-26 | 2010-07-07 | 安徽省农业科学院土壤肥料研究所 | Fertilizer for medicinal chrysanthemums and production method thereof |
| CN101928190A (en) * | 2010-09-16 | 2010-12-29 | 安徽科技学院 | Fertilizer special for medicinal Chuzhou chrysanthemum and preparation method thereof |
| CN102599305A (en) * | 2012-03-08 | 2012-07-25 | 刘茜 | Selenium-rich chrysanthemum tea or tea |
| CN102617251A (en) * | 2012-04-13 | 2012-08-01 | 常熟市平冶机械有限公司 | Selenium-rich composite organic fertilizer and preparing method thereof |
| CN102617247A (en) * | 2012-04-13 | 2012-08-01 | 常熟市平冶机械有限公司 | Selenium-rich nutrient solution |
Non-Patent Citations (4)
| Title |
|---|
| HTTP://BAIKE.BAIDU.COM/HISTORY/ID=24027233凹凸棒土: "http://baike.***.com/history/id=24027233凹凸棒土", 《百度百科》, 8 October 2011 (2011-10-08) * |
| 张静芬: "黄山贡菊的栽培", 《云南农业》, 31 December 2009 (2009-12-31) * |
| 王文军等: "黄山贡菊产区土壤养分状况调查分析", 《安徽农业科学》, vol. 34, no. 21, 31 December 2006 (2006-12-31) * |
| 程立光: "黄山贡菊栽培管理技术", 《现代农业科技》, no. 21, 31 December 2009 (2009-12-31), pages 106 - 107 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103553746A (en) * | 2013-10-30 | 2014-02-05 | 成都新朝阳作物科学有限公司 | Selenium-rich nutrient and application thereof |
| CN103553746B (en) * | 2013-10-30 | 2015-09-09 | 成都新朝阳作物科学有限公司 | Selenium-rich nutrient and application thereof |
| CN105660150A (en) * | 2016-03-02 | 2016-06-15 | 黄山市芽典生态农业有限公司 | Nutrition bowl cultivation method of Huangshan tribute chrysanthemums |
| CN105660150B (en) * | 2016-03-02 | 2018-05-25 | 黄山市芽典生态农业有限公司 | A kind of nutritive cube cultural method of Huangshan Gongju |
| CN109453736A (en) * | 2018-10-29 | 2019-03-12 | 佛山市铁人环保科技有限公司 | A kind of soil conditioner and preparation method thereof of silicon sulphur selenium zinc multiple elements design attapulgite |
| CN112457120A (en) * | 2021-01-04 | 2021-03-09 | 方连明 | Selenium-rich trace element fertilizer, selenium-rich controlled release fertilizer, preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103086794B (en) | 2015-01-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103708920B (en) | Foliar nutrient | |
| CN103875517B (en) | A kind of paddy rice non-soil culture nutrient matrix | |
| CN104557293B (en) | Special high-content water soluble fertilizer for citrus and preparation method for water soluble fertilizer | |
| CN103012004A (en) | Leaf vegetable nutrient solution formula | |
| CN102942937B (en) | Hydrosulphate soil amendment and preparation method thereof | |
| CN102498950A (en) | Selenium sustained-release edible fungus additive for selenium-rich culturing of edible fungus and preparation method thereof | |
| CN103787776A (en) | Biological water flushing fertilizer and preparation method thereof | |
| CN106718454A (en) | A kind of implantation methods of selenium-rich rice | |
| CN103787764A (en) | Biological all-element fertilizer and preparation method thereof | |
| CN102792840A (en) | Organic selenium-rich dendrobium candidum and cultivation method thereof | |
| CN105272508A (en) | Hypericum perforatum L. selenium-rich foliar fertilizer | |
| CN103641657A (en) | A fertilizer used for killing pests and weeding and a preparation method thereof | |
| CN103755497A (en) | Compound fertilizer with soil activator and preparation method thereof | |
| CN103086794B (en) | Selenium enrichment soil nutrient and preparation method thereof, and cultivation method of Huangshan tribute chrysanthemum | |
| CN105130586A (en) | Sugar alcohol chelated nano organic selenium fertilizer and preparation method thereof | |
| CN102503711A (en) | Slow release fertilizer with selenium and preparation method and application thereof | |
| CN104893734A (en) | A regulator for lowering the pH value of slightly-alkaline tea plantation soil, a preparing method thereof and applications of the regulator | |
| CN103641604A (en) | Nutrient solution for water-cultured seedling of strawberry | |
| CN104557294A (en) | Special water-soluble fertilizer for roses and preparation method | |
| CN102771295A (en) | Method for improving selenium fertilizer absorption efficiency of tea trees | |
| CN103086807B (en) | Bulk blend fertilizer for controlling soil-borne disease and preparation method of bulk blend fertilizer | |
| CN106588334A (en) | Water culture nutrient solution formula promoting rooting of dracaena sanderiana | |
| CN104045450B (en) | A kind of poly micro element special fertilizer for orchid | |
| CN102992850A (en) | Fertilizer special for producing organic selenium-rich watermelons and preparation method thereof | |
| CN105104041A (en) | Production method of selenium-enriched rice |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150121 Termination date: 20190123 |