CN103073951A - Anti-forgery printing ink and manufacturing method thereof - Google Patents
Anti-forgery printing ink and manufacturing method thereof Download PDFInfo
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- CN103073951A CN103073951A CN201310037088XA CN201310037088A CN103073951A CN 103073951 A CN103073951 A CN 103073951A CN 201310037088X A CN201310037088X A CN 201310037088XA CN 201310037088 A CN201310037088 A CN 201310037088A CN 103073951 A CN103073951 A CN 103073951A
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Abstract
The invention relates to anti-forgery printing ink and a manufacturing method thereof. The anti-forgery printing ink comprises rosin modified isooctyl phenolic resin, lauric acid modified alkyd resin, polyethene wax, polytetrafluoroethylene wax, tung oil, soybean oil, colloidal calcium carbonate, cobalt iso-octoate, manganese iso-octoate, zirconium iso-octoate, an antidesiccant, mineral oil, an infrared absorbate and infrared excitation powder. Compared with the existing infrared absorption printing ink or infrared laser printing ink, the anti-forgery printing ink has functions of the infrared absorption printing ink and the infrared laser printing ink, and the anti-forgery printing ink is only required to be printed on a medium at one time to form an anti-forgery mark, so that labor is saved, and equipment investment is reduced.
Description
Technical field
The present invention relates to a kind of anti-forgery ink and manufacture method thereof, particularly related to a kind of anti-forgery ink and manufacture method thereof that contains infrared absorption thing and infrared excitation powder.
Background technology
Chinese patent ZL201210179557 patent disclosure the manufacture method of anti-fake mark, it is infrared absorption printing ink and infrared laser printing ink to be printed on respectively consist of anti-fake mark on the medium, it has increased anti-counterfeiting power and Extraordinary information is provided.But this manufacture method, print twice, not only take a lot of work, effort, also increased simultaneously the input of equipment, therefore, the inventor is placing always two kinds of printing ink is being united two into one, produce a kind of antifalse printing ink and manufacture method thereof that can one-step print just has two kinds of printing ink functions, but whether simply two kinds of printing ink are mixed, just can obtain having the printing ink of above-mentioned two kinds of functions, because the proportion of infrared absorption printing ink and infrared laser printing ink is all not identical with viscosity, even after two kinds of printing ink are mixed simply, also can't mix, so that mixed printing ink still only has the function of one of infrared absorption printing ink or infrared laser printing ink.
Summary of the invention
The application's goal of the invention provide a kind of have not only have infrared absorption printing ink but also have anti-forgery ink and the manufacture method thereof of infrared laser printing ink dual-use function, this printing ink can carry out the function that one-step print just has above-mentioned two kinds of printing ink at anti-counterfeiting medium.
In order to finish the application's goal of the invention, the present invention by the following technical solutions:
A kind of anti-forgery ink of the present invention, wherein: according to the parts by weight meter, it comprises following component:
Anti-forgery ink of the present invention, wherein: described antidesiccant is butyraldehyde oxime or Diacetylmonoxime;
Anti-forgery ink of the present invention, wherein: described infrared absorption material is one or more the mixture in phthalocyanine naphthalene phthalocyanine, aromatic amine or the methine dyes;
Anti-forgery ink of the present invention, wherein: described infrared absorption material is in the carborundum powder of parts by weight: 65-80%, the silica powder of 15-30% and the zirconium white of 1-8%; The carborundum powder that described infrared absorption material is 65-80%, the silica powder of 15-30% and the titanium oxide of 1-8%;
Anti-forgery ink of the present invention, wherein: described infrared excitation powder is the infrared excitation powder that Pola security protection pseudo-Science and Technology Ltd. in Guangzhou makes.
The manufacture method of anti-forgery ink of the present invention, wherein: it may further comprise the steps:
(1) the infrared absorption thing with 7-10 part adds in the mineral oil of 1-4 part under 60-80 ℃ temperature, fully stirs to make it to mix;
(2) the infrared excitation powder with 7-10 part adds in the mineral oil of 2-3 part under 30-50 ℃ temperature, fully stirs to mix to make it to close evenly;
(3) with the Abietyl modified isooctyl phenol resol of 22-28 part, the soybean oil of the tung oil of 6-7 part and 22-23 part is put into reactor, then be filled with the nitrogen of 0.1-0.15Mpa pressure in the reactor, reactor is persistently overheating to 240-260 ℃ with 2 ℃/minute speed, simultaneously under the effect of reactor agitator, above-mentioned Abietyl modified isooctyl phenol resol, tung oil and soybean oil are ceaselessly stirred, insulation is 2-3 hour under 240-260 ℃ temperature, then the lauric acid modified alkyd resin that adds 8-10 part, when adding above-mentioned lauric acid modified alkyd resin, the reactor agitator ceaselessly stirs again, after being incubated again 1-1.5 hour, when being cooled to 175-185 ℃ of temperature, said mixture is transferred to storage tank, naturally cools to normal temperature;
(4) with the infrared absorption thing and the infrared excitation powder that have evenly mixed with mineral oil in step (1) and the step (2), 0.1-0.3 the cobalt iso-octoate of part, 0.3-0.5 the manganese iso-octoate of part, 0.1-0.5 part zirconium iso-octoate, the calcene of 3-5 part, mixture in the tetrafluoroethylene wax of the polyethylene wax of 2-3 part and 0.8-1.2 part and step (3) storage tank adds in the planetary-type mixer, planetary-type mixer ceaselessly stirred 20-40 minute, the antidesiccant that adds again 0.1-0.5 part, planetary-type mixer ceaselessly stirred 20-40 minute, then said mixture is sent in the three-roller and be rolled, be transferred at last turbine mixer, detect the viscosity of said mixture, when the viscosity of said mixture during greater than 30,000 centipoise, when stirring, be that the sylvic oil of 100-300 centipoise is adjusted into 10,000 to 30,000 centipoises with the viscosity of above-mentioned mixing with viscosity, when the viscosity of said mixture during less than 10,000 centipoise, when stirring, be that the sylvic oil of 7-9 ten thousand centipoise viscosity is adjusted into 10,000 to 30,000 centipoises with the viscosity of said mixture with viscosity, namely obtained anti-forgery ink of the present invention.
The manufacture method of anti-forgery ink of the present invention, wherein: the rotating speed of described reactor agitator must not be lower than 100 rev/mins; The rotating speed of planetary-type mixer must not be lower than 60 rev/mins; Turbine mixer must not be lower than 50 rev/mins.
Anti-forgery ink of the present invention is compared with existing infrared absorption printing ink or infrared laser printing ink, this printing ink has possessed the function of infrared absorption printing ink and infrared laser printing ink simultaneously, anti-forgery ink of the present invention only needs one-step print just can consist of anti-fake mark on medium, saving of labor not only, laborsaving, also reduced simultaneously the input of equipment, and anti-forgery ink of the present invention never is that above-mentioned two kinds of printing ink are simply mixed, but by batching and manufacturing process infrared absorption thing and infrared excitation powder are organically mixed, so that anti-forgery ink of the present invention has possessed the function of infrared absorption printing ink and infrared laser printing ink simultaneously.
Embodiment
A kind of anti-forgery ink of the present invention, according to the parts by weight meter, it comprises following component:
Wherein: antidesiccant is butyraldehyde oxime or Diacetylmonoxime; The infrared absorption material is one or more the mixture in phthalocyanine naphthalene phthalocyanine, aromatic amine or the methine dyes; Perhaps the infrared absorption material is by weight percentage: the zirconium white of the carborundum powder of 65-80%, the silica powder of 15-30% and 1-8%; Perhaps the infrared absorption material is the carborundum powder of 65-80%, the silica powder of 15-30% and the titanium oxide of 1-8%, and the infrared excitation powder is the infrared excitation powder that Pola security protection pseudo-Science and Technology Ltd. in Guangzhou makes.
The manufacture method of anti-forgery ink of the present invention, it may further comprise the steps:
(1) with infrared absorption thing and the mineral oil of 1-4 part under 60-80 ℃ temperature of 7-10 part, stirs;
(2) with infrared excitation powder and the mineral oil of 2-3 part under 30-50 ℃ temperature of 7-10 part, stir;
(3) with the Abietyl modified isooctyl phenol resol of 22-28 part, the soybean oil of the tung oil of 6-7 part and 22-23 part is put into reactor, then be filled with the nitrogen of 0.1-0.15Mpa pressure in the reactor, reactor is persistently overheating to 240-260 ℃ with 2 ℃/minute speed, simultaneously under the effect of reactor agitator, above-mentioned Abietyl modified isooctyl phenol resol, tung oil and soybean oil are ceaselessly stirred, insulation is 2-3 hour under 240-260 ℃ temperature, then the lauric acid modified alkyd resin that adds 8-10 part, when adding above-mentioned lauric acid modified alkyd resin, the reactor agitator ceaselessly stirs again, after being incubated again 1-1.5 hour, when being cooled to 175-185 ℃ of temperature, said mixture is transferred to storage tank, naturally cools to normal temperature;
(4) with the infrared absorption thing and the infrared excitation powder that have evenly mixed with mineral oil in step (1) and the step (2), 0.1-0.3 the cobalt iso-octoate of part, 0.3-0.5 the manganese iso-octoate of part, 0.1-0.5 part zirconium iso-octoate, the calcene of 3-5 part, mixture in the tetrafluoroethylene wax of the polyethylene wax of 2-3 part and 0.8-1.2 part and step (3) storage tank adds in the planetary-type mixer, planetary-type mixer ceaselessly stirred 20-40 minute, the antidesiccant that adds again 0.1-0.5 part, planetary-type mixer ceaselessly stirred 20-40 minute, then said mixture is sent in the three-roller and be rolled, be transferred at last turbine mixer, detect the viscosity of said mixture, when the viscosity of said mixture during greater than 30,000 centipoise, when stirring, be that the sylvic oil of 100-300 centipoise is adjusted into 10,000 to 30,000 centipoises with the viscosity of above-mentioned mixing with viscosity, when the viscosity of said mixture during less than 10,000 centipoise, when stirring, be that the sylvic oil of 7-9 ten thousand centipoise viscosity is adjusted into 10,000 to 30,000 centipoises with the viscosity of said mixture with viscosity, namely obtained anti-forgery ink of the present invention.
Above embodiment is described preferred implementation of the present invention; be not that scope of the present invention is limited; design under the prerequisite of spirit not breaking away from the present invention; various distortion and improvement that those of ordinary skills make technical scheme of the present invention all should fall in the definite protection domain of claims of the present invention.
Claims (10)
1. anti-forgery ink, it is characterized in that: according to the parts by weight meter, it comprises following component:
2. anti-forgery ink as claimed in claim 1, it is characterized in that: described antidesiccant is butyraldehyde oxime or Diacetylmonoxime.
3. anti-forgery ink as claimed in claim 2 is characterized in that: described infrared absorption material is one or more the mixture in phthalocyanine naphthalene phthalocyanine, aromatic amine or the methine dyes.
4. anti-forgery ink as claimed in claim 2 is characterized in that: described infrared absorption material is for by weight percentage: the zirconium white of the carborundum powder of 65-80%, the silica powder of 15-30% and 1-8%; The carborundum powder that described infrared absorption material is 65-80%, the silica powder of 15-30% and the titanium oxide of 1-8%.
5. such as claim 3 or 4 described anti-forgery inks, it is characterized in that: described infrared excitation powder is the infrared excitation powder that Pola security protection pseudo-Science and Technology Ltd. in Guangzhou makes.
6. the manufacture method of anti-forgery ink as claimed in claim 1, it is characterized in that: it may further comprise the steps:
(1) the infrared absorption thing with 7-10 part adds the mineral oil of 1-4 part under 60-80 ℃ temperature, mixes;
(2) the infrared excitation powder with 7-10 part adds the mineral oil of 2-3 part under 30-50 ℃ temperature, mixes;
(3) with the Abietyl modified isooctyl phenol resol of 22-28 part, the soybean oil of the tung oil of 6-7 part and 22-23 part is put into reactor, then be filled with the nitrogen of 0.1-0.15Mpa pressure in the reactor, reactor is persistently overheating to 240-260 ℃ with 2 ℃/minute speed, simultaneously under the effect of reactor agitator, above-mentioned Abietyl modified isooctyl phenol resol, tung oil and soybean oil are ceaselessly stirred, insulation is 2-3 hour under 240-260 ℃ temperature, then the lauric acid modified alkyd resin that adds 8-10 part, when adding above-mentioned lauric acid modified alkyd resin, the reactor agitator ceaselessly stirs, after being incubated again 1-1.5 hour, when being cooled to 175-185 ℃ of temperature, said mixture is transferred to storage tank, naturally cools to normal temperature;
(4) with the infrared absorption thing and the infrared excitation powder that have evenly mixed with mineral oil in step (1) and the step (2), 0.1-0.3 the cobalt iso-octoate of part, 0.3-0.5 the manganese iso-octoate of part, 0.1-0.5 part zirconium iso-octoate, the calcene of 3-5 part, mixture in the tetrafluoroethylene wax of the polyethylene wax of 2-3 part and 0.8-1.2 part and step (3) storage tank adds in the planetary-type mixer, planetary-type mixer ceaselessly stirred 20-40 minute, the antidesiccant that adds again 0.1-0.5 part, planetary-type mixer ceaselessly stirred 20-40 minute again, then said mixture is sent in the three-roller and be rolled, be transferred at last turbine mixer, detect the viscosity of said mixture, when the viscosity of said mixture during greater than 30,000 centipoise, when stirring, be that the sylvic oil of 100-300 centipoise is adjusted into 10,000 to 30,000 centipoises with the viscosity of above-mentioned mixing with viscosity, when the viscosity of said mixture during less than 10,000 centipoise, when stirring, be that the sylvic oil of 7-9 ten thousand centipoise viscosity is adjusted into 10,000 to 30,000 centipoises with the viscosity of said mixture with viscosity, namely obtained anti-forgery ink of the present invention.
7. the manufacture method of anti-forgery ink as claimed in claim 6, it is characterized in that: described antidesiccant is butyraldehyde oxime or Diacetylmonoxime.
8. the manufacture method of anti-forgery ink as claimed in claim 7 is characterized in that: described infrared absorption material is one or more the mixture in phthalocyanine naphthalene phthalocyanine, aromatic amine or the methine dyes; Described infrared absorption material is in the carborundum powder of parts by weight: 65-80%, the silica powder of 15-30% and the zirconium white of 1-8%; The carborundum powder that described infrared absorption material is 65-80%, the silica powder of 15-30% and the titanium oxide of 1-8%.
9. the manufacture method of anti-forgery ink as claimed in claim 7 is characterized in that: described infrared excitation powder is the infrared excitation powder that Pola security protection pseudo-Science and Technology Ltd. in Guangzhou makes.
10. the manufacture method of anti-forgery ink as claimed in claim 8 or 9, it is characterized in that: the rotating speed of described reactor agitator must not be lower than 100 rev/mins; The rotating speed of planetary-type mixer must not be lower than 60 rev/mins; Turbine mixer must not be lower than 50 rev/mins.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104312275A (en) * | 2014-11-10 | 2015-01-28 | 合肥宏图彩印有限公司 | Low-cost special thin and light printing ink containing banana fiber and preparation method thereof |
| CN106243830A (en) * | 2016-07-31 | 2016-12-21 | 梁枭 | The gel ink pen ink that writing can be eliminated |
| CN107418302A (en) * | 2016-05-24 | 2017-12-01 | 中钞油墨有限公司 | Spirit soluble dyestuff type Antiforge infrared ink and its manufacture method |
| CN107991727A (en) * | 2018-01-15 | 2018-05-04 | 浙江美迪凯现代光电有限公司 | A kind of crystal cloth of coating-type near-infrared low-pass filter and manufacture method |
| CN112341864A (en) * | 2020-11-30 | 2021-02-09 | 广东金冠科技股份有限公司 | Anti-counterfeiting ink formula |
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| US20030236331A1 (en) * | 2002-06-21 | 2003-12-25 | Harima Chemicals, Inc. | Method of producing resin varnish for printing ink |
| CN101250351A (en) * | 2008-03-26 | 2008-08-27 | 中国印钞造币总公司 | Soybean oil based silk-screen ink |
| CN101250350A (en) * | 2008-03-26 | 2008-08-27 | 中国印钞造币总公司 | Soybean oil based protruding printing ink |
| CN102658740A (en) * | 2012-06-04 | 2012-09-12 | 广东恒立信息科技有限公司 | Manufacturing method of anti-fake label |
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2013
- 2013-01-31 CN CN201310037088.XA patent/CN103073951B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030236331A1 (en) * | 2002-06-21 | 2003-12-25 | Harima Chemicals, Inc. | Method of producing resin varnish for printing ink |
| CN101250351A (en) * | 2008-03-26 | 2008-08-27 | 中国印钞造币总公司 | Soybean oil based silk-screen ink |
| CN101250350A (en) * | 2008-03-26 | 2008-08-27 | 中国印钞造币总公司 | Soybean oil based protruding printing ink |
| CN102658740A (en) * | 2012-06-04 | 2012-09-12 | 广东恒立信息科技有限公司 | Manufacturing method of anti-fake label |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104312275A (en) * | 2014-11-10 | 2015-01-28 | 合肥宏图彩印有限公司 | Low-cost special thin and light printing ink containing banana fiber and preparation method thereof |
| CN107418302A (en) * | 2016-05-24 | 2017-12-01 | 中钞油墨有限公司 | Spirit soluble dyestuff type Antiforge infrared ink and its manufacture method |
| CN107418302B (en) * | 2016-05-24 | 2020-12-29 | 中钞油墨有限公司 | Alcohol-soluble dye type infrared anti-counterfeiting ink and manufacturing method thereof |
| CN106243830A (en) * | 2016-07-31 | 2016-12-21 | 梁枭 | The gel ink pen ink that writing can be eliminated |
| CN107991727A (en) * | 2018-01-15 | 2018-05-04 | 浙江美迪凯现代光电有限公司 | A kind of crystal cloth of coating-type near-infrared low-pass filter and manufacture method |
| CN112341864A (en) * | 2020-11-30 | 2021-02-09 | 广东金冠科技股份有限公司 | Anti-counterfeiting ink formula |
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| CN103073951B (en) | 2014-04-16 |
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