CN103060097A - 一种固体催化剂催化生产生物柴油连续化生产线 - Google Patents
一种固体催化剂催化生产生物柴油连续化生产线 Download PDFInfo
- Publication number
- CN103060097A CN103060097A CN2012105880507A CN201210588050A CN103060097A CN 103060097 A CN103060097 A CN 103060097A CN 2012105880507 A CN2012105880507 A CN 2012105880507A CN 201210588050 A CN201210588050 A CN 201210588050A CN 103060097 A CN103060097 A CN 103060097A
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- Prior art keywords
- production line
- transesterification reaction
- solid catalyst
- continuous production
- producing biodiesel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003225 biodiesel Substances 0.000 title claims abstract description 19
- 238000010924 continuous production Methods 0.000 title claims abstract description 15
- 239000011949 solid catalyst Substances 0.000 title claims abstract description 14
- 238000006555 catalytic reaction Methods 0.000 title abstract 2
- 230000032050 esterification Effects 0.000 claims abstract description 28
- 238000005886 esterification reaction Methods 0.000 claims abstract description 28
- 238000004519 manufacturing process Methods 0.000 claims abstract description 27
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 30
- 238000005809 transesterification reaction Methods 0.000 claims description 28
- 235000011187 glycerol Nutrition 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 239000002551 biofuel Substances 0.000 claims description 9
- 239000000047 product Substances 0.000 claims description 7
- 238000000926 separation method Methods 0.000 claims description 7
- 235000019387 fatty acid methyl ester Nutrition 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 230000018044 dehydration Effects 0.000 claims description 4
- 238000006297 dehydration reaction Methods 0.000 claims description 4
- 238000000746 purification Methods 0.000 claims description 4
- 238000007670 refining Methods 0.000 claims description 4
- 239000006228 supernatant Substances 0.000 claims description 4
- 238000007710 freezing Methods 0.000 claims description 3
- 230000008014 freezing Effects 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- 150000004702 methyl esters Chemical class 0.000 claims description 3
- 238000004062 sedimentation Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 239000004367 Lipase Substances 0.000 claims description 2
- 102000004882 Lipase Human genes 0.000 claims description 2
- 108090001060 Lipase Proteins 0.000 claims description 2
- 235000019421 lipase Nutrition 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 abstract description 6
- 125000004185 ester group Chemical group 0.000 abstract 1
- CMDGQTVYVAKDNA-UHFFFAOYSA-N propane-1,2,3-triol;hydrate Chemical compound O.OCC(O)CO CMDGQTVYVAKDNA-UHFFFAOYSA-N 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 21
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
- 238000000034 method Methods 0.000 description 7
- 239000000463 material Substances 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 4
- 102000004190 Enzymes Human genes 0.000 description 3
- 108090000790 Enzymes Proteins 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000000446 fuel Substances 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000002283 diesel fuel Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 150000002148 esters Chemical group 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 239000010773 plant oil Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011973 solid acid Substances 0.000 description 1
Images
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Liquid Carbonaceous Fuels (AREA)
- Fats And Perfumes (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
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CN201210588050.7A CN103060097B (zh) | 2012-12-30 | 2012-12-30 | 一种固体催化剂催化生产生物柴油连续化生产线 |
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CN201210588050.7A CN103060097B (zh) | 2012-12-30 | 2012-12-30 | 一种固体催化剂催化生产生物柴油连续化生产线 |
Publications (2)
Publication Number | Publication Date |
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CN103060097A true CN103060097A (zh) | 2013-04-24 |
CN103060097B CN103060097B (zh) | 2014-11-26 |
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CN201210588050.7A Expired - Fee Related CN103060097B (zh) | 2012-12-30 | 2012-12-30 | 一种固体催化剂催化生产生物柴油连续化生产线 |
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CN (1) | CN103060097B (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104419526A (zh) * | 2013-09-02 | 2015-03-18 | 河南隆正生物能源有限公司 | 一种利用废弃餐饮油生产生物柴油的装置 |
CN111733020A (zh) * | 2020-07-08 | 2020-10-02 | 北京启迪德清生物能源科技有限公司 | 移动撬装生物燃料一体化反应装置 |
CN113862085A (zh) * | 2021-09-09 | 2021-12-31 | 江苏英汇能源科技有限公司 | 一种利用废弃油脂生产甲酯的工艺 |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101033411A (zh) * | 2007-04-19 | 2007-09-12 | 龙岩卓越新能源发展有限公司 | 生物柴油连续精馏装置 |
CN200951999Y (zh) * | 2006-03-10 | 2007-09-26 | 昆明理工大学 | 一种制备生物柴油的装置 |
CN101067091A (zh) * | 2007-06-08 | 2007-11-07 | 清华大学 | 一种由高酸值原料固相催化连续制备生物柴油的工艺 |
CN101096603A (zh) * | 2006-06-30 | 2008-01-02 | 董清华 | 一种利用分子蒸馏技术生产生物柴油的生产方法以及制造设备 |
CN101173176A (zh) * | 2007-08-07 | 2008-05-07 | 崔明林 | 利用动植物废油连续生产生物柴油的工艺方法 |
CN101177617A (zh) * | 2006-11-10 | 2008-05-14 | 北京化工大学 | 一种制备生物柴油的工艺方法 |
CN101294093A (zh) * | 2007-04-29 | 2008-10-29 | 华中农业大学 | 生物柴油的一体化生产工艺及专用装置 |
CN201695009U (zh) * | 2010-05-31 | 2011-01-05 | 贵州江南航天生物能源科技有限公司 | 一种生物柴油生产线 |
CN202297552U (zh) * | 2011-11-08 | 2012-07-04 | 焦作市新生生物化工有限公司 | 一种生物柴油原料的预处理装置 |
-
2012
- 2012-12-30 CN CN201210588050.7A patent/CN103060097B/zh not_active Expired - Fee Related
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN200951999Y (zh) * | 2006-03-10 | 2007-09-26 | 昆明理工大学 | 一种制备生物柴油的装置 |
CN101096603A (zh) * | 2006-06-30 | 2008-01-02 | 董清华 | 一种利用分子蒸馏技术生产生物柴油的生产方法以及制造设备 |
CN101177617A (zh) * | 2006-11-10 | 2008-05-14 | 北京化工大学 | 一种制备生物柴油的工艺方法 |
CN101033411A (zh) * | 2007-04-19 | 2007-09-12 | 龙岩卓越新能源发展有限公司 | 生物柴油连续精馏装置 |
CN101294093A (zh) * | 2007-04-29 | 2008-10-29 | 华中农业大学 | 生物柴油的一体化生产工艺及专用装置 |
CN101067091A (zh) * | 2007-06-08 | 2007-11-07 | 清华大学 | 一种由高酸值原料固相催化连续制备生物柴油的工艺 |
CN101173176A (zh) * | 2007-08-07 | 2008-05-07 | 崔明林 | 利用动植物废油连续生产生物柴油的工艺方法 |
CN201695009U (zh) * | 2010-05-31 | 2011-01-05 | 贵州江南航天生物能源科技有限公司 | 一种生物柴油生产线 |
CN202297552U (zh) * | 2011-11-08 | 2012-07-04 | 焦作市新生生物化工有限公司 | 一种生物柴油原料的预处理装置 |
Non-Patent Citations (1)
Title |
---|
艾汉丹米尔巴斯: "《生物燃料》", 30 May 2011, article "生物柴油生产中使用的基本设备", pages: 143 * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104419526A (zh) * | 2013-09-02 | 2015-03-18 | 河南隆正生物能源有限公司 | 一种利用废弃餐饮油生产生物柴油的装置 |
CN111733020A (zh) * | 2020-07-08 | 2020-10-02 | 北京启迪德清生物能源科技有限公司 | 移动撬装生物燃料一体化反应装置 |
CN113862085A (zh) * | 2021-09-09 | 2021-12-31 | 江苏英汇能源科技有限公司 | 一种利用废弃油脂生产甲酯的工艺 |
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CN103060097B (zh) | 2014-11-26 |
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