CN103060093B - Fragrance-invigorating and moisture-retention particles in cigarette and their preparation method and use - Google Patents
Fragrance-invigorating and moisture-retention particles in cigarette and their preparation method and use Download PDFInfo
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- CN103060093B CN103060093B CN201210585262.XA CN201210585262A CN103060093B CN 103060093 B CN103060093 B CN 103060093B CN 201210585262 A CN201210585262 A CN 201210585262A CN 103060093 B CN103060093 B CN 103060093B
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Abstract
The invention relates to fragrance-invigorating and moisture-retention particles in the cigarette and their preparation method and use. The preparation method utilizes a release base material and an organic polymer skeleton as main raw materials and comprises the processes of mixing, cladding, granulation, drying and screening. Through the preparation method, the fragrance-invigorating and moisture-retention particles in the cigarette can be obtained and can be released proactively. The release base material is prepared from an organic acid and a release matrix material. An adopted fragrance-invigorating curing agent comprises an anhydrous solvent, the organic polymer skeleton and spice. The preparation method comprises rotation coating, drying and screening. After contacting mainstream flue gas, the fragrance-invigorating and moisture-retention particles proactively and slowly release the spice and produce water. The fragrance-invigorating and moisture-retention particles can react stably and persistently, can reinforce a cigarette style and smoking quality and has a moisture retention effect.
Description
[technical field]
The invention belongs to cigarette material technical field, the preparation method and its usage of the fragrant humectation particle of benefit particularly adding in cigarette filter.
[background technology]
Lowering harm and decreasing coking problem is one of countries tobacco sixty-four dollar question.The first half of the year in 2011 whole nation cigarette list props up weighted average tar content and drops to below 11 milligrams, and part cigarette product tar content has dropped to below 10 milligrams.Also not rare on the cigarette market of 5 milligrams, 1 milligram even the cigarette of 0.1 milligram also come out.
For reaching the object of reducing tar and reducing harm, the technology industry such as filter tip, the fine composite filter of paper/vinegar, natural permeable degree tipping paper, online laser boring are introduced.When their effectively reduce the harmful components in cigarette smoke, also can make the aspect such as original suction taste, mouthfeel, physiological strength of cigarette follow corresponding reduction.Especially the loss of fragrance matter and perfume quantity in cigarette, easily make taste lose original style, this just need to make up by adding other spices to carry out part, and one of effect of perfuming is in reducing cigarette harm, make up the loss of fragrance, provide satisfied product to consumer.
Chinese invention patent 200710098075 discloses a kind of manufacturing technology of cigarette filter tip rod capable, it is characterized in that this cigarette filter tip rod capable (being called for short CAPF filter stick) adopts acetate fibre paper (being called for short CAP paper) as filling filtering material.CAPF filter stick, refers to the various filter stick for cigarettes that adopt CAP paper to make, and comprises the filter stick for cigarettes of CAPF filter stick and other kinds composite filter after compound.CAPF filter stick, except having the repertoire and external appearance characteristic of paper filter stick, applies triacetyl glycerine or other cellulose acetate plasticizer in the forming process of filter stick, and its filter bar can be " solidifying ", can be also " uncured ".
Chinese invention patent 201210017865 discloses a kind of sodium alginate particulate and cigarette with filter tip for cigarette filter.This sodium alginate particulate prepares by the following method: the sodium alginate that viscosity is less than to 200mpa.s is mixed with sodium alginate soln, then add essence and flavoring agent, prepare sodium alginate particle by dropping preparation method again, final drying obtains sodium alginate particulate.Essence and flavoring agent can be added in filter tip by this sodium alginate particulate, avoid the Pintsch process of essence and flavoring agent to produce harmful substance, can increase the fragrance in cigarette sucking process simultaneously.
Chinese invention patent 201010239046.0 discloses a kind of novel flavoring filter tip, choose diameter and cause fragrant particle in 20-40 object, by mouth rod forming machine, add equably 3 milligrams in the mouth rod tow of every millimeter described in, cause fragrant particle, make function mouth rod, described function mouth rod and base rod are rolled into flavoring filter tip by the Length Ratio of 10: 15 by composite molding machine; Describedly cause fragrant particle and formed in comminutor taking aluminosilicate as carrier by weight by following component: 4 parts of cloud and mist absolute oil; 1.5 parts of oak moss absolutes; 0.5 part of tree orchid essential oil; 4 parts of maltols; 15 parts of caramel colorants; 65 parts of propane diols; 10 parts, water.Flavoring filter tip of the present invention can make cigarette flavouring material increase on year-on-year basis 17.7%, and fragrance integrate score increases by 10% on year-on-year basis, and flavoring filter tip length ratio qualification rate reaches 100%.
[summary of the invention]
The inventor, through research, utilizes organic acid acid and carbonate mixture to meet water and reacts Heat of Formation or CO
2with the mechanism of water, set up flue gas Active Compensation system; Heat and CO
2while overflowing, can take the essence being added in soda acid particle out of reach flavor compensating effect, the generation of water has increased the moisture in flue gas and has reached the effect of humectation; Due to the fragrance overflowing and the aerosol of moisture formation and the similitude of flue gas, make compensation effect more obvious.
For this reason, the invention provides the preparation method who mends fragrant humectation particle in a kind of cigarette, step is as follows:
A, preparation discharge base-material: get the organic acid of 1:2 ~ 3:2 and discharge bed material with weight ratio score another name, and for subsequent use;
B, prepare spice solution: take anhydrous solvent and the spices of 4:1 ~ 9:1 in weight ratio, mix through emulsification or dissolving, obtain spice solution; Described spices is Zimbabwe's extract;
C, prepare solid spice: take described spice solution and the organic acid of 1:5 ~ 1:20 and discharge bed material in weight ratio, spice solution being sprayed on described organic acid to the air-dry solid spice that obtains;
D, prepare spray solidification agent: take absolute ethyl alcohol and the lac of 4:1 ~ 19:1 in weight ratio, dissolving mixes, and obtains spray solidification agent;
E, organic acid powder preparation: the spray solidification agent of the solid spice of step c and steps d is coated, obtains organic acid powder; The quality that coated ratio meets the lac in described spray solidification agent be in solid spice organic acid quality 4%;
F, release bed material particle: the spray solidification agent of the release bed material of step a and d step is coated, obtains discharging bed material particle; The quality that coated ratio meets the lac in described spray solidification agent is to discharge 4% of bed material quality;
H, batch mixing: by the release bed material particle of the organic acid powder of step e and step f with ... ratio mixes, then compressing tablet, pulverizing are granulated again to add excipient microcrystalline cellulose, then dry in baking oven, the product of particle diameter in 18～100 orders chosen in screening again, obtains the fragrant humectation particle of described benefit.
In the present invention, described organic acid is selected from one or more organic acids in citric acid, citric acid, tartaric acid and/or malic acid.
In the present invention, described release bed material is selected from one or more release bed materials of sodium acid carbonate, saleratus, sodium carbonate, lithium carbonate and/or potash.
Preferably, described release base-material and organic acid powder are sieved, choose particles more than particle diameter 40 orders.
In the present invention, described in step e, organic polymer skeleton is selected from cellulose acetate and/or PLA.
In the present invention, described anhydrous solvent is absolute ethyl alcohol and/or anhydrous propylene glycol.
In the present invention, the quality of described excipient microcrystalline cellulose is described organic acid powder and discharges 10% of bed material particle gross mass.
Preferably, the emulsification of step b is ultrasonic emulsification.
Cigarette filter application in cigarette filter with lac coated particle that the present invention also provides said method to obtain, preferably with cigarette filter length gauge, the addition of described perfuming particle is 0.5-35mg/mm, the particularly preferably compound 0.5-3.4mg/mm of tow, the compound 15-35mg/mm of cavity.
In the present invention, Zimbabwe's tobacco extract is the product that can buy acquisition on market, Zimbabwe's tobacco extract that for example Huabao Edible Essence & Condiment (Shanghai) sells.
In the present invention, be coated and undertaken by flat die rolling granulator, the flat die rolling granulator of for example selecting Shandong Zibo Xing Ying Mechanology Inc. to manufacture.
Similarly, the particle that the present invention prepares can also be applied to that binary is compound, in tri compound, cavity composite filter.
Method of the present invention is simple, cost of manufacture is lower, and gained perfuming particle has consolidation homogeneous, the mellow and full advantage such as smooth.Utilize the cigarette filter material that the inventive method prepares to have nontoxic.Slowly disintegration after particle and main flume effect, produces CO
2can carry out active perfuming, can ensure that fragrance uniformity, acid-base reaction stable and suction taste produce water and reach humectation effect as perfuming carrier with water.
[brief description of the drawings]
Fig. 1 is preparation method's flow chart of the present invention.
[detailed description of the invention]
Can understand better the present invention by following embodiment.
Embodiment 1
Take tartaric acid 180g, sodium acid carbonate 120g, for subsequent use.
Take Zimbabwe extract 3g absolute ethyl alcohol 12g and dissolved, obtain spice solution.
Tartaric acid is air-dry with after spice solution mixing homogeneous, obtain air-dry compound.
Take 12g lac and be dissolved in 228g absolute ethyl alcohol, obtain shellac solution 240g.
By dry to air-dry compound and shellac solution 144g spraying, obtain solid spice.
By dry to sodium acid carbonate 120g and shellac solution 96g spraying, obtain discharging bed material particle.
By solid spice and release bed material particle mixing homogeneous; gross weight 300g; add after microcrystalline cellulose 30g and mix homogeneous, compressing tablet, pulverize granulation again, dry complete particle is sieved and chooses 20 to 40 orders and be active release type with interior material and mend fragrant humectation particle.
Gained active release type is mended fragrant humectation particle and is applied to composite particles filter stick formation by addition 2mg/mm, makes binary compound filter candle.Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, then the complete active release type particle filter stick of tipping preparation is placed in cigarette 22 DEG C, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 DEG C of room temperatures, humidity 60% that ventilates, under environment, evaluate again.Evaluation result is shown in description subordinate list 1.
Embodiment 2
Take citric acid 30g, tartaric acid 20g, citric acid 50g, sodium acid carbonate 120g, sodium carbonate 80g, for subsequent use.
Take Zimbabwe extract 6g absolute ethyl alcohol 54g and dissolved for subsequent usely, obtain 60g spice solution.
Organic acid is air-dry with after spice solution mixing homogeneous, obtain air-dry compound.
Take 12g lac and be dissolved in 48g absolute ethyl alcohol, obtain 60g shellac solution.
By air-dry compound and shellac solution 20g spray drying granulation, obtain solid spice.
By sodium acid carbonate 120g and sodium carbonate 80g mixing homogeneous, with shellac solution 40g spray-drying process, obtain discharging bed material particle.
By solid spice and release bed material particle mixing homogeneous, after interpolation microcrystalline cellulose 30g, mix homogeneous, compressing tablet, pulverize granulation again.Dry complete particle is sieved and chooses 20 to 40 orders and be initiatively release type with interior material and mend fragrant particle.
Gained particle is applied to composite particles filter stick formation by addition 2mg/mm, makes binary compound filter candle.Select the finished cigarettes of quality between 0.880-0.900g, as Yunnan Yuxi Cigarette Factory produces red plum board, remove original filter stick, the active release type particle filter stick that tipping preparation is complete.Then cigarette is placed in to 22 DEG C, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 DEG C of room temperatures, humidity 60% that ventilates, under environment, evaluate again.Evaluation result is shown in description subordinate list 1.
Embodiment 3
Take citric acid 70g, citric acid 80g, sodium carbonate 50g, lithium carbonate 100g, for subsequent use.
Take Zimbabwe extract 5g absolute ethyl alcohol 25g and dissolved, obtain spice solution.
Organic acid is air-dry with after spice solution mixing homogeneous, obtain air-dry compound.
Get 12g lac and be dissolved in 108g absolute ethyl alcohol, obtain shellac solution.
By the compound after air-dry and shellac solution 60g spray drying granulation, obtain solid spice.
By sodium carbonate 50g, lithium carbonate 100g mixing homogeneous, with shellac solution 60g spray-drying process, obtains discharging bed material particle.
By solid spice and release bed material particle mixing homogeneous, after interpolation microcrystalline cellulose 30g, mix homogeneous, compressing tablet, pulverize granulation again.Dry complete particle is sieved and chooses 20 to 40 orders and be initiatively release type with interior material and mend fragrant particle.
Gained particle is applied to composite particles filter stick formation by addition 20mg/mm, makes ternary cavity composite filter.Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, the active release type particle filter stick that tipping preparation is complete.Then cigarette is placed in to 22 DEG C, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 DEG C of room temperatures, humidity 60% that ventilates, under environment, evaluate again.Evaluation result is shown in description subordinate list 1.
Embodiment 4
Take citric acid 50g, tartaric acid 100g, saleratus 150g, for subsequent use.
Take Zimbabwe's extract (alcohol extracting part) 3g propane diols 10g, alcohol 8g and dissolved for subsequent usely, obtain spice solution.
Organic acid is air-dry with after spice solution mixing homogeneous, obtain compound.
Take 12g lac and be dissolved in 168g absolute ethyl alcohol, obtain shellac solution.
By the compound after air-dry and shellac solution 90g spray drying granulation, obtain solid spice.
By saleratus 150g, with shellac solution 90g spray-drying process, obtain discharging bed material particle.
By solid spice and release bed material particle mixing homogeneous, after interpolation microcrystalline cellulose 30g, mix homogeneous, compressing tablet, pulverize granulation again.Dry complete particle is sieved and chooses 40 to 60 orders and be initiatively release type with interior material and mend fragrant particle.
Gained particle is applied to composite particles filter stick formation by addition 25mg/mm, makes ternary cavity composite filter.Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, the active release type particle filter stick that tipping preparation is complete.Then cigarette is placed in to 22 DEG C, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 DEG C of room temperatures, humidity 60% that ventilates, under environment, evaluate again.Evaluation result is shown in description subordinate list 1.
Embodiment 5
Take tartaric acid 140g, sodium acid carbonate 160g, for subsequent use.
Take Zimbabwe's extract (alcohol extracting part) 5g alcohol 25g and dissolved for subsequent usely, obtain spice solution.
Organic acid is air-dry with after spice solution mixing homogeneous, obtain compound.
Take 12g lac and be dissolved in 108g absolute ethyl alcohol, obtain shellac solution.
By the compound after air-dry and shellac solution 56g spray drying granulation, obtain solid spice.
By sodium acid carbonate 160g, with shellac solution 64g spray-drying process, obtain discharging bed material particle.
By solid spice and release bed material particle mixing homogeneous, after interpolation microcrystalline cellulose 30g, mix homogeneous, compressing tablet, pulverize granulation again.Dry complete particle is sieved and chooses 20 to 40 orders and be initiatively release type with interior material and mend fragrant particle.
Gained particle is applied to composite particles filter stick formation by addition 20mg/mm, makes ternary cavity composite filter.
Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, then the complete active release type particle filter stick of tipping preparation is placed in cigarette 22 DEG C, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 DEG C of room temperatures, humidity 60% that ventilates, under environment, evaluate again.Evaluation result is shown in description subordinate list 1.
Subordinate list 1
。
Claims (8)
1. in cigarette, mend a preparation method for fragrant humectation particle, it is characterized in that step is as follows:
A, preparation discharge base-material: get the organic acid of 1:2～3:2 and discharge bed material with weight ratio score another name, and for subsequent use; Described organic acid is that one or more are selected from the organic acid in citric acid, citric acid and/or malic acid; Described release bed material is one or more release bed materials that are selected from saleratus, sodium carbonate, lithium carbonate and/or potash;
B, prepare spice solution: take anhydrous solvent and the spices of 4:1～9:1 in weight ratio, mix through emulsification or dissolving, obtain spice solution; Described spices is Zimbabwe's extract;
C, prepare solid spice: take described spice solution and the organic acid of 1:5～1:20 and discharge bed material in weight ratio, spice solution being sprayed on described organic acid to the air-dry solid spice that obtains;
D, prepare spray solidification agent: take absolute ethyl alcohol and the lac of 4:1～19:1 in weight ratio, dissolving mixes, and obtains spray solidification agent;
E, organic acid powder preparation: the spray solidification agent of the solid spice of step c and steps d is coated, obtains organic acid powder; The quality that coated ratio meets the lac in described spray solidification agent be in solid spice organic acid quality 4%;
F, release bed material particle: the spray solidification agent of the release bed material of step a and steps d is coated, obtains discharging bed material particle; The quality that coated ratio meets the lac in described spray solidification agent is to discharge 4% of bed material quality;
H, batch mixing: the organic acid powder of step e is mixed with the release bed material particle of step f; then compressing tablet, pulverizing are granulated again to add excipient microcrystalline cellulose; then dry in baking oven, then sieve and choose the product of particle diameter in 18～100 orders, the fragrant humectation particle of described benefit obtained.
2. method according to claim 1, is characterized in that described release base-material and organic acid powder to sieve, and chooses particles more than particle diameter 40 orders.
3. method according to claim 1, is characterized in that described in step e that organic polymer skeleton is selected from cellulose acetate and/or PLA.
4. method according to claim 1, is characterized in that described anhydrous solvent is absolute ethyl alcohol and/or anhydrous propylene glycol.
5. method according to claim 1, the quality that it is characterized in that described excipient microcrystalline cellulose is described organic acid powder and discharges 10% of bed material particle gross mass.
6. method according to claim 1, the emulsification that it is characterized in that step b is ultrasonic emulsification.
7. the cigarette filter that described in claim 1-6, method obtains is the application in cigarette filter with lac coated particle.
8. the cigarette filter that described in claim 7, method obtains is the application in cigarette filter with lac coated particle, it is characterized in that with cigarette filter length gauge, and the addition of described perfuming particle is 0.5-35mg/mm.
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| CN1045911A (en) * | 1989-03-28 | 1990-10-10 | 箭牌糖类有限公司 | Improve the stability of Ai Litan (Alitame) in the chewing gum by encapsulation process |
| US20060254606A1 (en) * | 2005-05-16 | 2006-11-16 | Fazlani Arif Abdul K | Novel smoking composition |
| CN100593980C (en) * | 2006-08-31 | 2010-03-17 | 云南瑞升烟草技术（集团）有限公司 | Composite additive for raising cigarette smoke moisture and its use |
| CN101766332B (en) * | 2009-12-31 | 2011-07-27 | 云南烟草科学研究院 | Pills capable of adding fragrance to cigarettes |
| CN101889734A (en) * | 2010-03-10 | 2010-11-24 | 邓培友 | Water storage device for cigarette filter tip |
| CN101889733B (en) * | 2010-07-23 | 2011-09-14 | 安徽中烟工业公司 | Novel flavoring filter tip |
| CN102068039A (en) * | 2010-12-10 | 2011-05-25 | 湖北中烟工业有限责任公司 | Preparation method of novel aromatic filter tip and application of novel aromatic filter tip in cigarettes |
| CN102578711A (en) * | 2012-01-19 | 2012-07-18 | 湖北中烟工业有限责任公司 | Sodium alginate microparticles for cigarette filter and filtered cigarette |
| CN102533445B (en) * | 2012-02-05 | 2013-09-18 | 云南正邦生物技术有限公司 | Method for preparing active release type cigarette flavor complementing particles |
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Address after: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building, Patentee after: HUABAO FLAVOURS & FRAGRANCES CO.,LTD. Address before: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building, Patentee before: Huabao flavor Ltd. |
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Address after: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building, Patentee after: Huabao flavor Ltd. Address before: 201821 Yecheng Road, Shanghai, No. 1299, No. Patentee before: Huabao Flavours & Fragrances Co.,Ltd |
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Effective date of registration: 20170123 Address after: 650503 Yunnan province Kunming city Kunming high tech Zone Jinpu rural Metro high-tech industrial base A6-2 Patentee after: YUNNAN XINYUN TECHNOLOGY DEVELOPMENT Co.,Ltd. Address before: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building, Patentee before: HUABAO FLAVOURS & FRAGRANCES CO.,LTD. |