CN103060090B - Tobacco spice with faint scent style, preparing and using methods thereof, and cigarettes - Google Patents
Tobacco spice with faint scent style, preparing and using methods thereof, and cigarettes Download PDFInfo
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- CN103060090B CN103060090B CN201210534599.8A CN201210534599A CN103060090B CN 103060090 B CN103060090 B CN 103060090B CN 201210534599 A CN201210534599 A CN 201210534599A CN 103060090 B CN103060090 B CN 103060090B
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Abstract
The invention discloses a tobacco spice with a faint scent style. The tobacco spice with the faint scent style comprises compositions of, by weight percentage, 30%-60% of cabbage mustard extract, 1%-8% of Yunnan tobacco extract, 4%-10% of glycyrrhiza fluidextract, 1%-5% of jujube absolute oil, 0.3%-0.7% of ketone tobacco monomer spice, 25%-35% of propylene glycol and 8%-12% of ethanol with the mass fraction greater than or equal to 80%, wherein the sum of the weight percentages of all the compositions is 100%. The tobacco spice is characterized by having a mature tobacco scent with slightly pungent sweet taste and a fresh, natural and harmonious aroma on the nose, and being abundant and prominent in tobacco scent, harmonious and natural in scent type, good in taste, comfortable in remaining taste and prominent in effect of increasing a flue-cured type faint scent style, and further having the unique faint scent style of flue-cured tobacco on the sensory evaluation. The invention further discloses a preparing method. The preparing method is simple and easy in technological process, simple in equipment, easy to industrially produce, and easy to popularize and use.
Description
[technical field]
The invention belongs to technical field of tobacco, particularly a kind of tobacco aromatics using and preparation, using method and cigarette with delicate fragrance style.
[background technology]
Cigarette product is according to adopted tobacco leaf and the difference of processing technology, the difference of product style aspect, and the corresponding consumer group's quantity is divided, wherein Chinese style flue-cured tobacco type cigarette becomes the main cigarette product type of current China, and Chinese style flue-cured tobacco type cigarette is divided into delicate fragrance type, Luzhou-flavor and middle odor type.Delicate fragrance type cigarette taking Yunnan, Fujian delicate fragrance type tobacco leaf is primary raw material, pleasant impression is clean micro-pleasantly sweet, particularly has fresh and sweet tobacco aroma feature.Representative brand is " Red River ".Luzhou-flavor cigarette taking Hunan, Henan Luzhou-flavor tobacco leaf, import flue-cured tobacco and part Shandong high-quality tobacco be body material, has the cigarette of strong tobacco aroma.Representative brand has " white sand " and " China ".Middle odor type cigarette taking Guizhou, the cigarette with middle odor type that forms as primary raw material of Shandong flue-cured tobacco.Not outstanding representative brand at present.
At present, the delicate fragrance type Chinese-style cigarette on market is because tabacco fragrance is new and graceful refreshing light, and alcohol profit that mouthfeel is fresh and sweet, has sizable consumer group in China.The tobacco leaf of the type is mainly derived from the high-quality tobacco of Yunnan Province, gold dollar tobacco leaf as large in safflower, this tobacco leaf is fresh and sweet, and note is obvious, fragrance gracefulness, quality better, perfume quantity foot, is the indispensable raw material of manufacturing high-grade delicate fragrance type cigarette, aspect lifting cigarette product inherent quality, has important function.But the large gold dollar tobacco leaf of safflower is not resistance to fertilizer, easy bacteria infection in the course of cultivation, output is lower, adds the increase in demand of cigarette enterprise to Yunnan tobaccos such as the large gold dollars of safflower in recent years, causes the large gold dollar tobacco leaf of safflower under-supply.
Therefore, developing a kind of tobacco aromatics using of energy efficient hardening flue-cured tobacco delicate fragrance style, and be applied to production of cigarettes, is letter technical problem to be solved in prior art.
[summary of the invention]
Technical problem to be solved by this invention is: a kind of tobacco aromatics using with delicate fragrance style is provided, and its preparation and application, and the cigarette of containing it, this tobacco aromatics using can effectively promote cigarette flavouring essence quality, the delicate fragrance style and features with flue-cured tobacco uniqueness, improves mouthfeel, and pleasant impression is comfortable.
Technical problem of the present invention solves by the following technical programs:
There is a tobacco aromatics using for delicate fragrance style, comprise the component with following weight percentage:
Cabbage mustard extract 30%～60%
Yunyan extract 1%～8%
Liquid extract of liquorice 4%～10%
Date absolute oil 1%～5%
Monomer perfume 0.3% ~ 0.7% for ketone cigarette
Propane diols 25%～35%
The ethanol 8%～12% of mass fraction >=80%;
The percentage composition sum of each component is 100%.
In technique scheme, cabbage mustard extract has to cigarette the sweet effect of increasing, yunyan extract has the fresh and sweet style effect of increasing, date absolute oil has harmonious flue gas, soft taste, covers peppery assorted taste effect, and liquid extract of liquorice can strengthen back sweet sense, reducing flue gas stimulates, ketone cigarette has the effect that strengthens fresh and sweet note, makes the plentiful alcohol of flue gas and exquisiteness with monomer perfume, propane diols plays humectation to tobacco aromatics using and is beneficial to its long-term preservation, and ethanol plays solubilising and sterilization; The tobacco aromatics using that each component forms after coordinating above has delicate fragrance style, has proved that it has that cigarette is fragrant to be coordinated smokeing panel test in experiment, promotes flavouring essence quality, and strengthening flue-cured tobacco delicate fragrance style, promotes flue gas richness, covers assorted gas, improves the advantages such as mouthfeel.
Preferably, described ketone cigarette is geranyl acetone or solanone or both mixtures with monomer perfume; In the time that described ketone cigarette is the mixture of geranyl acetone and solanone with monomer perfume, in described tobacco aromatics using, the weight percentage of described geranyl acetone and solanone is respectively 0.2%～0.4% and 0.1%～0.3%.
Wherein, geranyl acetone can strengthen fresh and sweet note; Solanone can increase tobacco perfume (or spice), makes the plentiful alcohol of flue gas and exquisiteness.
A preparation method for above-mentioned tobacco aromatics using, comprises the following steps to prepare cabbage mustard extract:
1) extraction: add water or ethanol or both mixtures after surface moisture is cleaned, drained to fresh cabbage mustard, carry out ultrasonic extraction;
2) centrifugation: the mixed liquor after ultrasonic extraction is carried out to solid-liquid separation;
3) film purifying: the supernatant obtaining after centrifugal, by milipore filter, is seen through to liquid and is concentrated to solid quality content 15～20% through reverse osmosis membrane again, be described cabbage mustard extract.
Preferably, in described extraction, the addition of water or ethanol or both mixtures is 1～4 times of weight that drains the cabbage mustard after surface moisture; Ultrasonic extraction condition is: time 10～25min, and 10～30 DEG C of temperature, power 600～1000W, ultrasonic frequency is 20～60KHz.
Preferably, in described centrifugation: temperature is 15 ~ 30 DEG C, centrifugal rotational speed is 2500～5000 revs/min, and the time is 15～30min.
Preferably, in described film purifying, milipore filter energy molecular cut off is greater than 1000 daltonian materials, and the concentrated concentrated pressure of reverse osmosis membrane is 1.0～1.6MPa, and temperature is 35 ± 1 DEG C.
Preferably, after the each component in described tobacco aromatics using is mixed by proportioning, at 50～60 DEG C, stir after 1 hour, be placed at 4 DEG C and leave standstill after 1～3 day, cross leaching supernatant, obtain described tobacco aromatics using.
A using method for above-mentioned tobacco aromatics using, sprays the tobacco leaf surface in flue-cured tobacco by described tobacco aromatics using, and the amount of spraying of described tobacco aromatics using accounts for 0.08%～0.8%. of its flue-cured tobacco weight spraying
Preferably, the amount of spraying of described tobacco aromatics using accounts for 0.1%～0.5% of its flue-cured tobacco weight spraying.
A kind of cigarette of having added above-mentioned tobacco aromatics using.
The invention has the beneficial effects as follows:
Tobacco aromatics using of the present invention possesses following characteristics: smell perfume (or spice): have ripe tobacco flavor, slightly pungent sweet sense, the fresh and clean harmony of fragrance; Sensory evaluating smoking: cigarette is fragrant abundant outstanding, and odor type harmony is natural, has the delicate fragrance style and features of flue-cured tobacco uniqueness, and mouthfeel is good, and pleasant impression is comfortable, remarkably productive aspect increase fire-cured tobacco type delicate fragrance style.
Preparation method of the present invention is owing to having adopted ultrasonic extraction and film concentration technique, both synergies, the aroma substance being easily damaged in the cabbage mustard extract of preparation is retained, combine by itself and other constituent optimization again, obtain a kind of tobacco aromatics using with delicate fragrance style, preparation method's technical process is simple, and equipment is simple, be easy to suitability for industrialized production, easy to utilize.
[detailed description of the invention]
For ease of understanding better the present invention, be illustrated by following instance.These examples belong to protection scope of the present invention, but do not limit the scope of the invention.
In an embodiment, the tobacco aromatics using with delicate fragrance style comprises the component with following weight percentage:
Cabbage mustard extract 30%～60%
Yunyan extract 1%～8%
Liquid extract of liquorice 4%～10%
Date absolute oil 1%～5%
Monomer perfume 0.3% ~ 0.7% for ketone cigarette
Propane diols 25%～35%
The ethanol 8%～12% of mass fraction >=80%;
The percentage composition sum of each component is 100%.
Preferably, ketone cigarette is geranyl acetone or solanone or both mixtures with monomer perfume; In the time being the mixture of geranyl acetone and solanone, in tobacco aromatics using, the weight percentage of geranyl acetone and solanone is respectively 0.2%～0.4% and 0.1%～0.3%.
In another embodiment, the preparation method of tobacco aromatics using, comprises the following steps to prepare cabbage mustard extract:
1) extraction: add water or ethanol or both mixtures after surface moisture is cleaned, drained to fresh cabbage mustard, carry out ultrasonic extraction;
2) centrifugation: the mixed liquor after ultrasonic extraction is carried out to solid-liquid separation;
3) film purifying: the supernatant obtaining after centrifugal, by milipore filter, is seen through to liquid and is concentrated to solid quality content 15～20% through reverse osmosis membrane again, be described cabbage mustard extract.
Preferably, in extraction, the addition of water or ethanol or both mixtures is 1～4 times of weight that drains the cabbage mustard after surface moisture; Ultrasonic extraction condition is: time 10～25min, and 10～30 DEG C of temperature, power 600～1000W, ultrasonic frequency is 20～60KHz.
Preferably, in centrifugation: temperature is 15 ~ 30 DEG C, centrifugal rotational speed is 2500～5000 revs/min, and the time is 15～30min.
Preferably, in film purifying, milipore filter energy molecular cut off is greater than 1000 daltonian materials, and reverse osmosis membrane energy molecular cut off is greater than 100 daltonian materials, and the concentrated concentrated pressure of reverse osmosis membrane is 1.0～1.6MPa, and temperature is 35 ± 1 DEG C.
Preferably, after the each component in tobacco aromatics using is mixed by proportioning, at 50～60 DEG C, stir after 1 hour, be placed at 4 DEG C and leave standstill after 1～3 day, cross leaching supernatant, obtain described tobacco aromatics using.
Below by embodiment more specifically, the present invention will be described in detail.
embodiment 1
Each component and the mass content thereof of tobacco aromatics using with delicate fragrance style is as follows:
Cabbage mustard extract 45%
Yunyan extract 4.5%
Liquid extract of liquorice 7%
Date absolute oil 3%
Geranyl acetone 0.3%
Solanone 0.2%
Propane diols 30%
The ethanol 10% of mass fraction 95%.
embodiment 2
Fresh cabbage mustard being cleaned, drained the water that adds 2 times of its weight after surface moisture, is 15 DEG C extracting temperature, and ultrasonic power is 800W, and supersonic frequency is ultrasonic extraction 20min under 49KHz; Mixed liquor after ultrasonic extraction is complete is at 15 DEG C, centrifugation 10min under the condition of 3500 revs/min, the supernatant obtaining is by being greater than after the milipore filter of 1000 daltonian materials by molecular cut off, see through liquid 35 ± 1 DEG C of temperature, pressure is under 1.2MPa, carry out film with the reverse osmosis membrane that can molecular cut off be greater than 100 daltonian materials concentrated, be about 15～20% when being concentrated into solid content, be cabbage mustard extract.Cabbage mustard extract and other components are pressed after the proportioning mixing of above-described embodiment, at 50～60 DEG C, stirred after 1 hour, be placed at 4 DEG C and leave standstill after 1～3 day, cross leaching supernatant, obtain tobacco aromatics using.
embodiment 3
Fresh cabbage mustard is cleaned, is drained the 30%(mass fraction that adds 2 times of its weight after surface moisture) ethanolic solution, be 10 DEG C extracting temperature, ultrasonic power is 600W, supersonic frequency is ultrasonic extraction 15min under 60KHz; Mixed liquor after ultrasonic extraction is complete is at 20 DEG C, centrifugation 10min under the condition of 5000 revs/min, the supernatant obtaining is by being greater than after the milipore filter of 1000 daltonian materials by molecular cut off, see through liquid 35 ± 1 DEG C of temperature, pressure is under 1.6MPa, carry out film with the reverse osmosis membrane that can molecular cut off be greater than 100 daltonian materials concentrated, be about 15～20% when being concentrated into solid content, be cabbage mustard extract.Cabbage mustard extract and other components are pressed after the proportioning mixing of above-described embodiment, at 50～60 DEG C, stirred after 1 hour, be placed at 4 DEG C and leave standstill after 1～3 day, cross leaching supernatant, obtain tobacco aromatics using.
embodiment 4
Fresh cabbage mustard is cleaned, is drained the 50%(mass fraction that adds 3 times of its weight after surface moisture) ethanolic solution, be 20 DEG C extracting temperature, ultrasonic power is 100W, supersonic frequency is ultrasonic extraction 25min under 49KHz; Mixed liquor after ultrasonic extraction is complete is at 30 DEG C, centrifugation 20min under the condition of 3000 revs/min, the supernatant obtaining is by being greater than after the milipore filter of 1000 daltonian materials by molecular cut off, see through liquid 35 ± 1 DEG C of temperature, pressure is under 1.0MPa, carry out film with the reverse osmosis membrane that can molecular cut off be greater than 100 daltonian materials concentrated, be about 15～20% when being concentrated into solid content, be cabbage mustard extract.Cabbage mustard extract and other components are pressed after the proportioning mixing of above-described embodiment, at 50～60 DEG C, stirred after 1 hour, be placed at 4 DEG C and leave standstill after 1～3 day, cross leaching supernatant, obtain tobacco aromatics using.
embodiment 5
A using method for above-mentioned tobacco aromatics using, sprays the tobacco leaf surface in flue-cured tobacco by described tobacco aromatics using, and the amount of spraying of described tobacco aromatics using accounts for 0.08%～0.8% of its flue-cured tobacco weight spraying.Preferably, the amount of spraying of described tobacco aromatics using accounts for 0.1%～0.5% of its flue-cured tobacco weight spraying.
Concrete experimental test: be sprayed at the middle-grade blank of same (not flavoring and casing) flue-cured tobacco pipe tobacco surface using the tobacco aromatics using in embodiment 1 as additive, addition is respectively 0.08%, 0.1%, 0.3%, 0.5%, 0.8% of pipe tobacco weight.Subsequent treatment cigarette process routinely carries out, spraying after tobacco aromatics using, by flue-cured tobacco tobacco storage 4 hours, then through chopping, dry silk, perfuming, storage silk, cigarette and packaging process and make cigarette finished product.The group of smokeing panel test being made up of 8 people is respectively to the contrast of smokeing panel test of above-mentioned sample, and the overall sensory test result obtaining is as shown in the table.Wherein, the interior quality of blank sample is all set as to 0, improves to some extent (as flue gas richness promotes, cover assorted gas, strengthen fresh and sweet sense, improve pleasant impression) with respect to blank sample interior quality, mutually deservedly just divide, score value is higher, and it is better to improve; Decrease (as flue gas richness declines, assorted gas increases, and fresh and sweet sense is lowered, and pleasant impression is uncomfortable) with respect to blank sample interior quality, mutually deserved negative point, negative point lower, and it is poorer to improve.
Smokeing panel test to test through cigarette charging shows, the spices of the cigarette delicate fragrance style of preparation has perfuming effect well, coordinates with cigarette is fragrant, promotes flavouring essence quality, strengthening flue-cured tobacco delicate fragrance style, and lifting flue gas richness, covers assorted gas, improves mouthfeel.
Above content is in conjunction with concrete preferred embodiment further description made for the present invention, can not assert that specific embodiment of the invention is confined to these explanations.For general technical staff of the technical field of the invention, make without departing from the inventive concept of the premise some substituting or obvious modification, and performance or purposes identical, all should be considered as belonging to protection scope of the present invention.
Claims (10)
1. a tobacco aromatics using with delicate fragrance style, is characterized in that, the raw material of preparing described tobacco aromatics using is made up of the component with following weight percentage:
The percentage composition sum of each component is 100%.
2. tobacco aromatics using according to claim 1, is characterized in that: described ketone cigarette monomer perfume is geranyl acetone or solanone or both mixtures; In the time that described ketone cigarette is the mixture of geranyl acetone and solanone with monomer perfume, in described tobacco aromatics using, the weight percentage of described geranyl acetone and solanone is respectively 0.2%～0.4% and 0.1%～0.3%.
3. a preparation method for tobacco aromatics using claimed in claim 1, is characterized in that, comprises the following steps to prepare cabbage mustard extract:
1) extraction: add water or ethanol or both mixtures after surface moisture is cleaned, drained to fresh cabbage mustard, carry out ultrasonic extraction;
2) centrifugation: the mixed liquor after ultrasonic extraction is carried out to solid-liquid separation;
3) film purifying: the supernatant obtaining after centrifugal, by milipore filter, is seen through to liquid and is concentrated to solid quality content 15～20% through reverse osmosis membrane again, be described cabbage mustard extract.
4. according to the preparation method of tobacco aromatics using claimed in claim 3, it is characterized in that: in described extraction, the addition of water or ethanol or both mixtures is 1～4 times of weight that drains the cabbage mustard after surface moisture; Ultrasonic extraction condition is: time 10～25min, and 10～30 DEG C of temperature, power 600～1000W, ultrasonic frequency is 20～60KHz.
5. according to the preparation method of tobacco aromatics using claimed in claim 3, it is characterized in that: in described centrifugation: temperature is 15～30 DEG C, centrifugal rotational speed is 2500～5000 revs/min, and the time is 15～30min.
6. according to the preparation method of tobacco aromatics using claimed in claim 3, it is characterized in that: in described film purifying, milipore filter energy molecular cut off is greater than 1000 daltonian materials, the concentrated concentrated pressure of reverse osmosis membrane is 1.0～1.6MPa, and temperature is 35 ± 1 DEG C.
7. according to the preparation method of the tobacco aromatics using described in claim 3 to 6 any one, it is characterized in that: after the each component in described tobacco aromatics using is mixed by proportioning, at 50～60 DEG C, stir after 1 hour, be placed at 4 DEG C and leave standstill after 1～3 day, cross leaching supernatant, obtain described tobacco aromatics using.
8. a using method for tobacco aromatics using claimed in claim 1, is characterized in that: described tobacco aromatics using is sprayed to the tobacco leaf surface in flue-cured tobacco, and the amount of spraying of described tobacco aromatics using accounts for 0.08%～0.8% of its flue-cured tobacco weight spraying.
9. the using method of tobacco aromatics using according to claim 8, is characterized in that: the amount of spraying of described tobacco aromatics using accounts for 0.1%～0.5% of its flue-cured tobacco weight spraying.
10. a cigarette of adding tobacco aromatics using claimed in claim 1.
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| CN201210534599.8A CN103060090B (en) | 2012-12-12 | 2012-12-12 | Tobacco spice with faint scent style, preparing and using methods thereof, and cigarettes |
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Families Citing this family (3)
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| CN105372364B (en) * | 2015-10-29 | 2017-09-01 | 宁波威龙香精香料有限公司 | A kind of method of use leaching method analysed for powder essence sample |
| CN108576917A (en) * | 2018-04-13 | 2018-09-28 | 袁承淼 | A kind of preparation method of tobacco aromaticss |
| CN111876256A (en) * | 2020-07-16 | 2020-11-03 | 云南中烟工业有限责任公司 | Fresh and sweet flavor type tobacco essence and preparation method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1102557A (en) * | 1993-11-12 | 1995-05-17 | 李龙召 | Tabacco modifier |
| CN101215805A (en) * | 2008-01-07 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Cigarette perfuming agent and its preparation method and application |
| CN101224041B (en) * | 2008-01-22 | 2010-10-20 | 深圳波顿香料有限公司 | Spice for tobacco |
| CN102304432B (en) * | 2011-03-17 | 2013-06-05 | 广州市澳键丰泽生物科技有限公司 | Tobacco flavoring essence containing purple perilla |
| CN102309061B (en) * | 2011-03-17 | 2013-06-05 | 广州市澳键丰泽生物科技有限公司 | Tobacco feeding essence formula |
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Application publication date: 20130424 Assignee: Shenzhen Haoyu Biological Technology Co. Ltd. Assignor: Bodun Perfume Co., Ltd., Shenzhen Contract record no.: 2017440020056 Denomination of invention: Tobacco spice with faint scent style, preparing and using methods thereof, and cigarettes Granted publication date: 20140618 License type: Common License Record date: 20170726 |
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Assignee: Shenzhen Haoyu Biological Technology Co. Ltd. Assignor: Bodun Perfume Co., Ltd., Shenzhen Contract record no.: 2017440020056 Date of cancellation: 20171218 |
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Application publication date: 20130424 Assignee: Shenzhen Haoyu Biological Technology Co. Ltd. Assignor: Bodun Perfume Co., Ltd., Shenzhen Contract record no.: 2017440020102 Denomination of invention: Tobacco spice with faint scent style, preparing and using methods thereof, and cigarettes Granted publication date: 20140618 License type: Common License Record date: 20171219 |