CN103040639A - Oil absorption starch compound slurry mask, preparation technology and grinding devices thereof - Google Patents
Oil absorption starch compound slurry mask, preparation technology and grinding devices thereof Download PDFInfo
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- CN103040639A CN103040639A CN2012105864701A CN201210586470A CN103040639A CN 103040639 A CN103040639 A CN 103040639A CN 2012105864701 A CN2012105864701 A CN 2012105864701A CN 201210586470 A CN201210586470 A CN 201210586470A CN 103040639 A CN103040639 A CN 103040639A
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- starch compound
- oil suction
- granulation machine
- mud mask
- ultra micro
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- 229920002472 Starch Polymers 0.000 title claims abstract description 38
- 235000019698 starch Nutrition 0.000 title claims abstract description 38
- 239000008107 starch Substances 0.000 title claims abstract description 38
- 150000001875 compounds Chemical class 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 238000000227 grinding Methods 0.000 title claims abstract description 10
- 238000005516 engineering process Methods 0.000 title abstract description 7
- 238000010521 absorption reaction Methods 0.000 title abstract description 6
- 239000002002 slurry Substances 0.000 title abstract 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 39
- 238000003756 stirring Methods 0.000 claims abstract description 35
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000463 material Substances 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000000203 mixture Substances 0.000 claims abstract description 15
- 239000004927 clay Substances 0.000 claims abstract description 14
- 238000002156 mixing Methods 0.000 claims abstract description 14
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims abstract description 13
- 229960000458 allantoin Drugs 0.000 claims abstract description 13
- 239000000440 bentonite Substances 0.000 claims abstract description 13
- 229910000278 bentonite Inorganic materials 0.000 claims abstract description 13
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000008367 deionised water Substances 0.000 claims abstract description 13
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 13
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 229920001285 xanthan gum Polymers 0.000 claims abstract description 13
- 239000000230 xanthan gum Substances 0.000 claims abstract description 13
- 229940082509 xanthan gum Drugs 0.000 claims abstract description 13
- 235000010493 xanthan gum Nutrition 0.000 claims abstract description 13
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 9
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 9
- WSDISUOETYTPRL-UHFFFAOYSA-N dmdm hydantoin Chemical compound CC1(C)N(CO)C(=O)N(CO)C1=O WSDISUOETYTPRL-UHFFFAOYSA-N 0.000 claims abstract description 9
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000003921 oil Substances 0.000 claims description 36
- 238000005469 granulation Methods 0.000 claims description 31
- 230000003179 granulation Effects 0.000 claims description 31
- 239000004575 stone Substances 0.000 claims description 20
- 238000004519 manufacturing process Methods 0.000 claims description 13
- 239000011265 semifinished product Substances 0.000 claims description 12
- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 claims description 12
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 8
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 8
- 229910052740 iodine Inorganic materials 0.000 claims description 8
- 239000011630 iodine Substances 0.000 claims description 8
- KRPAJLYSLFNDOA-UHFFFAOYSA-N mephenesin carbamate Chemical compound CC1=CC=CC=C1OCC(O)COC(N)=O KRPAJLYSLFNDOA-UHFFFAOYSA-N 0.000 claims description 8
- 229950006838 mephenesin carbamate Drugs 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 8
- 239000000047 product Substances 0.000 claims description 8
- 229910052710 silicon Inorganic materials 0.000 claims description 8
- 239000010703 silicon Substances 0.000 claims description 8
- 238000013019 agitation Methods 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 5
- 238000007599 discharging Methods 0.000 claims description 5
- 239000012467 final product Substances 0.000 claims description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 4
- 229920001577 copolymer Polymers 0.000 claims description 4
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 claims description 4
- 239000001095 magnesium carbonate Substances 0.000 claims description 4
- 229910000021 magnesium carbonate Inorganic materials 0.000 claims description 4
- 230000001954 sterilising effect Effects 0.000 claims description 4
- 238000004659 sterilization and disinfection Methods 0.000 claims description 4
- 238000004891 communication Methods 0.000 claims description 3
- AICOOMRHRUFYCM-ZRRPKQBOSA-N oxazine, 1 Chemical compound C([C@@H]1[C@H](C(C[C@]2(C)[C@@H]([C@H](C)N(C)C)[C@H](O)C[C@]21C)=O)CC1=CC2)C[C@H]1[C@@]1(C)[C@H]2N=C(C(C)C)OC1 AICOOMRHRUFYCM-ZRRPKQBOSA-N 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 10
- 239000011148 porous material Substances 0.000 abstract description 10
- 229940099451 3-iodo-2-propynylbutylcarbamate Drugs 0.000 abstract 2
- WYVVKGNFXHOCQV-UHFFFAOYSA-N 3-iodoprop-2-yn-1-yl butylcarbamate Chemical compound CCCCNC(=O)OCC#CI WYVVKGNFXHOCQV-UHFFFAOYSA-N 0.000 abstract 2
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- 229960001484 edetic acid Drugs 0.000 abstract 2
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 abstract 1
- 229910052570 clay Inorganic materials 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- 210000003491 skin Anatomy 0.000 description 18
- 239000006185 dispersion Substances 0.000 description 7
- 241000863032 Trieres Species 0.000 description 6
- 239000000839 emulsion Substances 0.000 description 5
- 230000028327 secretion Effects 0.000 description 4
- 206010000496 acne Diseases 0.000 description 3
- 230000001804 emulsifying effect Effects 0.000 description 3
- 239000003925 fat Substances 0.000 description 3
- 238000000265 homogenisation Methods 0.000 description 3
- 235000014593 oils and fats Nutrition 0.000 description 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 2
- 208000002874 Acne Vulgaris Diseases 0.000 description 2
- 206010040943 Skin Ulcer Diseases 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 210000001732 sebaceous gland Anatomy 0.000 description 2
- 210000002374 sebum Anatomy 0.000 description 2
- 231100000019 skin ulcer Toxicity 0.000 description 2
- 239000002569 water oil cream Substances 0.000 description 2
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 108010066551 Cholestenone 5 alpha-Reductase Proteins 0.000 description 1
- 206010010356 Congenital anomaly Diseases 0.000 description 1
- 206010020880 Hypertrophy Diseases 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 230000024245 cell differentiation Effects 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 230000003862 health status Effects 0.000 description 1
- 239000008309 hydrophilic cream Substances 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 239000008308 lipophilic cream Substances 0.000 description 1
- 239000013521 mastic Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
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- Cosmetics (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention relates to a special oil absorption starch compound slurry mask, preparation technology and preparation devices. The mask aims to absorb excessive fat secreted by skin and achieve the effect of compact pores in skin. The preparation technology can produce materials with scattered and uniform compositions. The devices can produce evenly scattered slurry materials. The technical scheme is that the oil absorption starch compound slurry mask comprises a special oil absorption starch compound, glycerol, kaolin, green clay, bentonite, silica, xanthan gum, allantoin, ethylene diamine tetraacetic acid (EDTA) disodium, DMDM hydantoin, iodopropynyl butylcarbamate (IPBC), essence and deionized water. The preparation method comprises four steps as follows: 1) mixing a part of raw materials, heating, dissolving and grinding the mixture; 2) treating the green clay; 3) mixing and grinding all raw materials to meet the standard; and 4) mixing and stirring the treated mixture in vacuum. The preparation devices are a continuous high-speed ultramicron granulating machine and a vacuum agitating pan communicated through a pipeline.
Description
Technical field
The present invention relates to a kind of special oil suction starch compound and preparation technology thereof, mud mask and the preparation technology thereof of a kind of special oil suction starch compound that is specifically related to arrange in pairs or groups.
The invention still further relates to a kind of Novel grinding apparatus, be used for the ground and mixed equipment that special oil suction starch compound mud mask is produced, belong to the Cosmetic Manufacture equipment technical field.
Background technology
Fat secretion vigorous (summer is especially obvious) is that a lot of reasons causes in the human body skin; The relation of having plenty of congenital heredity has plenty of that acquired environment causes; Especially adolescence is more obvious, the generation of the vigorous easy initiation comedo of fat secretion, and T word position is especially obvious.In addition, sebaceous gland is subjected to the impact of high temperature and pungent fry, also can allow sebaceous gland constantly secrete oils and fats, causes pore to block, and then causes the activity of 5α-reductase, makes the hypertrophy of sebaceous cell differentiation and seat skin ulcer bacillus, and then causes the generation of acne and seat skin ulcer; Door ?the patient is often arranged because of the glossy normal mad suction of oil suction face Paper of taking of the fuel-displaced Tam of Face Xin Full Face, its Real can only adsorb with oil suction face Paper or wash away grease Da to the short Temporary effect of deoiling, fundamentally do not solve the problem of skin fat secretion, life-time service also can make the skin drier oil that becomes more greasy responsive, is unfavorable for skin health.
In Cosmetics Production, form complete, the finely dispersed emulsified body of composition of oil-water emulsion for making the material body, often carry out high-speed stirred, high speed homogenization by mechanical force, reach the purpose of dispersion and emulsion.
The general mixing plant that adopts forms the high speed dispersion dish by gate stirrer and high speed homogenization dispersion emulsifying machine usually.
Gate stirrer is usually used in the mixing of general emulsifiable paste shape material, and its mixing speed is generally relatively slow, for the larger material-mud body of proportion, stirs the torsion underpower to stir the material body, can't form the material body of homogeneous.
The high speed homogenization dispersion emulsifying machine is comprised of rotor and stator, is generally used for the less and mobile good material body of the general proportion of emulsion dispersion.Yet the material-mud body is larger because itself expecting body thickness and proportion, can't obtain desirable emulsion dispersion effect; Too high such as rotor speed, also easily cause the overheated and axle center distortion of mechanical shaft seal, can't make the good material-mud body of homogeneity.
Summary of the invention
The objective of the invention is for the deficiencies in the prior art, the special oil suction starch compound of a kind of collocation mud mask is provided, this mud mask is take special oil suction starch compound as primary raw material, the too much oils and fats that can adsorb sebum secretion, reach the effect that the skin pore compacts, recovers the sebum normal function, it is dynamic that skin is got well.
Another object of the present invention provides a kind of preparation method of above-mentioned mud mask, and the method should be able to be produced the material body that composition disperses homogeneous, and has characteristics easy to make.
A further object of the present invention provides a kind of lapping device of above-mentioned mud mask, and this device should be able to be produced finely dispersed material-mud body, and simple in structure, easy to manufacture.
The technical solution used in the present invention is:
A kind of oil suction starch compound mud mask, the composition and the part by weight that comprise are:
Special oil suction starch compound 0.7～1.6%, glycerol 10.0～20.0%, Kaolin 10.0～20.0%, green clay 5.0～10.0%, bentonite 2.0～5.0%, Silicon stone 1.0～3.0%, xanthan gum 0.1～0.2%, allantoin 0.05～0.2%, EDETATE SODIUM 0.05～0.15%, DMDM Hydantoin 0.05～0.10%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05～0.1%, essence 0.02～0.1%, surplus is deionized water.
A kind of oil suction starch compound mud mask, the composition and the part by weight that comprise are:
Special oil suction starch compound 0.9～1.3%, glycerol 12.0～18.0%, Kaolin 12.0～18.0%, green clay 6.0～8.0%, bentonite 3.0～4.5%, Silicon stone 1.5～2.5%, xanthan gum 0.1～0.15%, allantoin 0.05～0.2%, EDETATE SODIUM 0.05～0.15%, DMDM Hydantoin 0.05～0.10%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05～0.1%, essence 0.02～0.1%, surplus is deionized water.
A kind of oil suction starch compound mud mask, the composition and the part by weight that comprise are: special oil suction starch compound 1.0%, glycerol 12%, Kaolin 15%, green clay 8%, bentonite 3.5%, Silicon stone 2%, xanthan gum 0.1%, allantoin 0.2%, EDETATE SODIUM 0.05%, DMDM Hydantoin 0.05%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05%, essence 0.1%, surplus is deionized water.
Described special oil suction starch compound comprises starch ocentyl succinic aluminum, acrylic acid-propylene analog copolymer, the magnesium carbonate that mixes with any ratio.
A kind of preparation method of oil suction starch compound mud mask, its making step is as follows:
1) xanthan gum, allantoin, EDETATE SODIUM, bentonite, glycerol, deionized water are heated to 55-65 ℃, fully after the dissolving, adopt continuous high-speed ultra micro granulation machine be ground to＜below the 10 μ m, for subsequent use as A phase mixed material;
2) with green clay by behind the irradiation 30mins, sterilization is finished, as B phase raw material;
3) A phase mixed material is added again again in the continuous high-speed ultra micro granulation machine at last, open machine, sequentially with B item raw material and other surplus stock, all add in this machine and mix, and adjust the grinding gap and repeatedly grind, make the following rear barrelling of material body particle diameter＜5 μ m for subsequent use;
4) will be transported in the vacuum stirring pot through the compound after upper the step, open the high-viscosity stirring blade of this pot, mixing speed 900-11,00rpm, vacuum is to Ya Li – 0.8Mpa, after stirring 25-30Mins, carry again discharging, get final product to get the special oil suction starch compound of a kind of interpolation mud mask finished product.
Grinding in the described step 1) needs progressively to adjust to grind the gap, grinds at least 3 times.
For understanding result of use of the present invention, form with questionnaire survey has been carried out widely investigation on probation to this product, men and women trier 250 people in all parts of the country are included in this investigation altogether in, male 110 people wherein, women 140 people, the oldest 48 years old, minimum 18 years old, about 25 years old mean age, regain altogether 195 parts of effective questionnaires.
195 triers use the present invention after 28 days, and are as follows to the result who restrains relevant indices degree self evaluation:
Increase the pore convergence: have respectively 29.2% and 68% trier to have moderate to improve and obviously improve;
Increase the careful sense of skin: have respectively 38.4% and 58.1% trier to have moderate to improve and obviously improve;
Reduce the skin oil soapy feeling: have respectively 74.3% and 52.4% trier to have moderate to improve and obviously improve;
Hide skin microgroove amount: have respectively 48.41% and 35.56% trier to have moderate to improve and obviously improve;
Can find out from the result of trier's self assessment, this product to increase pore penetrating, increase skin careful, reduce skin greasing, hide the skin microgroove in various degree improvement is arranged.
Show according to survey result: this adds special oil suction starch compound mud mask and has preferably pore convergence effect.
The present invention has added special oil suction starch compound in mud mask, the porous physical arrangement in this starch compound can in skin epidermis, play the effect of absorb oil and pore convergence; And by the amplification of the oil absorption of what own, can effectively reduce the oil pump capacity of skin pore, and then promote the skin contraction sense, make skin salubriouser; In addition, the micron-sized particle diameter that this facial film possesses can reach the effect of the covering microgroove of physical property; Life-time service will make skin be in health status, and allow skin exquisiteness Paint Gloss.
This mud mask has the clean pore of deep layer, the oils and fats (weight ratio of absorbing grease can reach the weight ratio 1/2 of raw material own) of absorption hypersteatosis, and then the ratio of minimizing acne generation, superior convergence pore effect, to the generation of skin without any zest and toxic and side effects, easy to use, be fit to any age level and use, especially for the people of oiliness skin, result of use is better.
A kind of for the production of mud mask continous way wet type high speed ultra micro granulation machine agitation mixer, comprise continuous high-speed ultra micro granulation machine and the vacuum stirring pot that passes through pipeline communication; The cavity volume that described granulation facility have a conical shell to form, the cavity volume top end opening is as feeding mouth; It is characterized in that: be equipped with in the granulation machine to regulate and grind the clearance adjuster that the gap is used, the semi-finished product discharge gate on granulation machine limit is provided with the high-viscosity stirring device by the pipeline communication vacuum stirring pot with impeller pump in this agitated kettle.
Described continuous high-speed ultra micro granulation machine, high-viscosity stirring device, impeller pump are by motor-driven.
Described clearance adjuster is the circular stone clearance adjuster that supports.
Also be provided with the intermediate water device for cooling in the described granulation machine.
Described high-viscosity stirring device is disposing the high-viscosity stirring blade.
Equipment provided by the invention can be produced completely equal refining body of oil-water emulsion effectively, is fit to very much the production of mud mask.Wherein, continuous high-speed ultra micro granulation machine (wet type) can the production high viscosity, than pulp product great, poor fluidity, and the mixing dispersion and the powder body that carry out material grind; Cream frost latex product that also can the production mixed flow; The vacuum stirring pot also can be used as Water-In-Oil cream frost emulsion, the emulsifying homogenizer of oil-in-water cream frost emulsion.It is larger that this device is processed the mud mask amount, can adjust with the variation of conical shell volume; Can contrast great, viscosity is high, the mastic of poor fluidity disperses effectively with evenly, grind out the material-mud body of homogeneous particle diameter.
Description of drawings
Fig. 1 is the structural representation of equipment of the present invention.
Have among the figure: 1, feeding mouth; 2, clearance adjuster; 3, intermediate water device for cooling; 4, the first motor; 5, semi-finished product discharge gate; 6, impeller pump; 7, the second motor; 8, high-viscosity stirring blade; 9, vacuum stirring pot; 10, pipeline.
As shown in Figure 1, the continous way wet type high speed ultra micro granulation machine agitation mixer for the production of mud mask comprises continuous high-speed ultra micro granulation machine and vacuum stirring pot; The conical shell of described continuous high-speed ultra micro granulation machine forms an open cavity volume, be provided with feeding mouth 1 on the housing, connect the circular inside of supporting stone clearance adjuster 2 intermediate water device for cooling 3 is arranged, semi-finished product discharge gate 5 belows are connected with the first motor 4, and the semi-finished product discharge gate is communicated with vacuum stirring pot 9 by the pipeline 10 with impeller pump 6; In the vacuum stirring pot, the output shaft of the second motor 7 is vertically down arranged, is fixed wtih high-viscosity stirring blade 8 on the output shaft.
Above-mentioned continous way wet type high speed ultra micro granulation machine, the equal outsourcing of vacuum stirring pot obtain.
During concrete the application, A, B phase raw material are added in the conical shell 1, open the first motor semi-finals power mix and blend, adjust the circular stone clearance adjuster 2(of supporting and open interlayer water cooling plant 3) the grinding gap, make material body particle diameter reach the regulation requirement; Open again impeller pump 6, semi-finished product are carried move in the fixation type vacuum agitated kettle 9, then open the second motor 7 high-viscosity stirring blade 8 is stirred; Mixing speed 900-11,00rpm, vacuum behind the stirring 25-35Mins, carries dischargings to get final product by the pipeline 5 with impeller pump 6 to – 0.8Mpa again.
Need progressively turn down during grinding and grind the gap; Usually turn down circular support the gap of stone clearance adjuster after, will the semi-finished product material body add in the conical shell and grind 5-10Mins, then be disposed to by the semi-finished product discharge gate and leave standstill that (pipeline with impeller pump is removed from the semi-finished product discharge gate in advance in the bucket 11; Leaving standstill bucket 11 is conventional vessels, represents with double dot dash line among the figure); Then again turn the circular gap of supporting the stone clearance adjuster down, again the semi-finished product material body is added in the conical shell and grind 5-10Mins, again be disposed to by the semi-finished product discharge gate and leave standstill in the bucket; So circulation is at least three times, the particle diameter of semi-finished product material body could be ground to＜below the 10 μ m.
The specific embodiment
The invention will be further described below by non-limiting examples.
Embodiment one
Get glycerol 10.0Kg, Kaolin 10.0Kg, green clay 5.0Kg, bentonite 2.0Kg, Silicon stone 1.0Kg, starch ocentyl succinic aluminum 0.5Kg, acrylic acid (ester) analog copolymer 0.15Kg, magnesium carbonate 0.1Kg, xanthan gum 0.1Kg, allantoin 0.05Kg, EDETATE SODIUM 0.05Kg, DMDM Hydantoin 0.05Kg, iodine propilolic alcohol butyl mephenesin Carbamate 0.05Kg, essence 0.02Kg, deionized water 70.98Kg.
By formula ratio xanthan gum, allantoin, EDETATE SODIUM, bentonite, glycerol, deionized water are heated to 55 ℃, fully after the dissolving, by continous way wet type high speed ultra micro granulation machine, motor rotary speed is fixed 3,000rpm, adjusts and supports crack between the stone clearance adjuster, the each adjustment dwindled to stone gap 2mm, grind above more than 3 times, reach to＜10 μ m, mutually for subsequent use as A;
By behind the irradiation 30mins, sterilization is finished with green clay, as the B phase;
Mixed material with A adds in the granulation machine more again at last, opens machine, sequentially with B item and the raw material that do not add, add A mutually in, add until whole raw materials and to grind after finishing mixing; The each adjustment dwindled to stone gap 2mm, repeatedly grinds 5 times, and particle diameter＜below the 5 μ m, barrelling is for subsequent use to make it reach the material body;
The compound of upper step is transported in the fixed evacuation agitated kettle by impeller pump, open the high-viscosity stirring blade, mixing speed 1,000rpm, open evacuation Zhi – 0.8Mpa, after stirring 30Mins, carry discharging by impeller pump again, get final product to get the special oil suction starch compound of a kind of interpolation mud mask finished product.
Embodiment two
Get glycerol 12.0Kg, Kaolin 15.0Kg, green clay 8.0Kg, bentonite 3.5Kg, Silicon stone 2.0Kg, starch ocentyl succinic aluminum 0.6Kg, acrylic acid (ester) analog copolymer 0.2Kg, magnesium carbonate 0.2Kg, xanthan gum 0.1Kg, allantoin 0.2Kg, EDETATE SODIUM 0.05Kg, DMDM Hydantoin 0.05Kg, iodine propilolic alcohol butyl mephenesin Carbamate 0.05Kg, essence 0.1Kg, deionized water 57.95Kg;
Just xanthan gum, allantoin, EDETATE SODIUM, bentonite, glycerol, deionized water are heated to 65 ℃ by formula ratio, fully after the dissolving, by continous way wet type high speed ultra micro granulation machine, motor rotary speed is fixed 3,000rpm, adjusts and supports crack between the stone, the each adjustment dwindled to stone gap 2mm, grind above more than 3 times, reach to＜10 μ m, mutually for subsequent use as A;
By behind the irradiation 30mins, sterilization is finished with green clay, as the B phase;
Mixed material with A adds putting in the charging basket of granulation machine more again at last, open machine, sequentially the B item is reached the raw material that does not add, add A mutually in, grind after mixing is finished in whole raw materials addings, the each adjustment dwindled to stone gap 2mm, repeatedly grinds 4 times, particle diameter＜below the 5 μ m, barrelling is for subsequent use to make it reach the material body;
The compound of upper step is transported in the fixed evacuation agitated kettle by impeller pump, open fixed high-viscosity stirring blade, mixing speed 1,000rpm, open evacuation Zhi – 0.8Mpa, after stirring 30Mins, carry discharging by impeller pump again, get final product to get the special oil suction starch compound of a kind of interpolation mud mask finished product.
Claims (10)
1. oil suction starch compound mud mask, the composition and the part by weight that comprise are:
Special oil suction starch compound 0.7～1.6%, glycerol 10.0～20.0%, Kaolin 10.0～20.0%, green clay 5.0～10.0%, bentonite 2.0～5.0%, Silicon stone 1.0～3.0%, xanthan gum 0.1～0.2%, allantoin 0.05～0.2%, EDETATE SODIUM 0.05～0.15%, DMDM Hydantoin 0.05～0.10%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05～0.1%, essence 0.02～0.1%, surplus is deionized water;
Described special oil suction starch compound comprises starch ocentyl succinic aluminum, acrylic acid-propylene analog copolymer, the magnesium carbonate that mixes with any ratio.
2. a kind of oil suction starch compound mud mask according to claim 1 is characterized in that composition and part by weight that this mud mask comprises are:
Special oil suction starch compound 0.9～1.3%, glycerol 12.0～18.0%, Kaolin 12.0～18.0%, green clay 6.0～8.0%, bentonite 3.0～4.5%, Silicon stone 1.5～2.5%, xanthan gum 0.1～0.15%, allantoin 0.05～0.2%, EDETATE SODIUM 0.05～0.15%, DMDM Hydantoin 0.05～0.10%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05～0.1%, essence 0.02～0.1%, surplus is deionized water.
3. a kind of oil suction starch compound mud mask according to claim 2 is characterized in that composition and part by weight that this mud mask comprises are:
Special oil suction starch compound 1.0%, glycerol 12%, Kaolin 15%, green clay 8%, bentonite 3.5%, Silicon stone 2%, xanthan gum 0.1%, allantoin 0.2%, EDETATE SODIUM 0.05%, DMDM Hydantoin 0.05%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05%, essence 0.1%, surplus is deionized water.
4. the preparation method of the described oil suction starch compound of claim 1 mud mask, its making step is as follows:
1) xanthan gum, allantoin, EDETATE SODIUM, bentonite, glycerol, deionized water are heated to 55-65 ℃, fully after the dissolving, adopt continuous high-speed ultra micro granulation machine be ground to＜below the 10 μ m, for subsequent use as A phase mixed material;
2) with green clay by behind the irradiation 30mins, sterilization is finished, as B phase raw material;
3) A phase mixed material is added again again in the continuous high-speed ultra micro granulation machine at last, open machine, sequentially with B item raw material and other surplus stock, all add in this machine and mix, and adjust the grinding gap and repeatedly grind, make the following rear barrelling of material body particle diameter＜5 μ m for subsequent use;
4) will be transported in the vacuum stirring pot through the compound after upper the step, open the high-viscosity stirring blade of this pot, mixing speed 900-11,00rpm, vacuum is to Ya Li – 0.8Mpa, after stirring 25-30Mins, carry again discharging, get final product to get the special oil suction starch compound of a kind of interpolation mud mask finished product.
5. the preparation method of described oil suction starch compound mud mask according to claim 4 is characterized in that the grinding in the described step 1), needs progressively to adjust to grind the gap, grinds at least 3 times.
6. one kind for the production of mud mask continous way wet type high speed ultra micro granulation machine agitation mixer, comprises continuous high-speed ultra micro granulation machine and the vacuum stirring pot (9) by pipeline communication; The cavity volume that described granulation facility have a conical shell to form, the cavity volume top end opening is as feeding mouth (1); It is characterized in that: be equipped with in the granulation machine to regulate and grind the clearance adjuster (2) that the gap is used, the semi-finished product discharge gate (5) on granulation machine limit is communicated with the vacuum stirring pot by the pipeline (10) with impeller pump (6), is provided with the high-viscosity stirring device in this agitated kettle.
7. described a kind of for the production of mud mask continous way wet type high speed ultra micro granulation machine agitation mixer according to claim 6, it is characterized in that described continuous high-speed ultra micro granulation machine, high-viscosity stirring device, impeller pump are by motor-driven.
8. described a kind of for the production of mud mask continous way wet type high speed ultra micro granulation machine agitation mixer according to claim 7, it is characterized in that described clearance adjuster is the circular stone clearance adjuster that supports.
9. described a kind of for the production of mud mask continous way wet type high speed ultra micro granulation machine agitation mixer according to claim 8, it is characterized in that also being provided with in the described granulation machine intermediate water device for cooling (3).
10. described a kind of for the production of mud mask continous way wet type high speed ultra micro granulation machine agitation mixer according to claim 9, it is characterized in that described high-viscosity stirring device is disposing high-viscosity stirring blade (8).
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| CN111991254A (en) * | 2020-08-12 | 2020-11-27 | 暨南大学 | Halloysite mud mask and preparation method thereof |
| CN112006926A (en) * | 2020-09-15 | 2020-12-01 | 广州艾蓓生物科技有限公司 | Hair oil-removing no-clean composition and preparation method thereof |
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| CN112006926A (en) * | 2020-09-15 | 2020-12-01 | 广州艾蓓生物科技有限公司 | Hair oil-removing no-clean composition and preparation method thereof |
| CN112006926B (en) * | 2020-09-15 | 2022-08-19 | 广州艾蓓生物科技有限公司 | Hair oil-removing no-clean composition and preparation method thereof |
| CN112494392A (en) * | 2020-12-25 | 2021-03-16 | 彭氏(惠州)实业发展有限公司 | Clean oil-in-water cosmetic composition and preparation method thereof |
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