CN103014856B - 掺铁钛蓝宝石晶片及其制备方法 - Google Patents
掺铁钛蓝宝石晶片及其制备方法 Download PDFInfo
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- CN103014856B CN103014856B CN201310008435.6A CN201310008435A CN103014856B CN 103014856 B CN103014856 B CN 103014856B CN 201310008435 A CN201310008435 A CN 201310008435A CN 103014856 B CN103014856 B CN 103014856B
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- wafer
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- sapphire
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- 229910052594 sapphire Inorganic materials 0.000 title claims abstract description 50
- 239000010980 sapphire Substances 0.000 title claims abstract description 50
- 229910001200 Ferrotitanium Inorganic materials 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 68
- 239000013078 crystal Substances 0.000 claims abstract description 63
- 239000010936 titanium Substances 0.000 claims abstract description 52
- 229910052742 iron Inorganic materials 0.000 claims abstract description 29
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 29
- 238000000034 method Methods 0.000 claims abstract description 28
- 239000000463 material Substances 0.000 claims abstract description 12
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000002994 raw material Substances 0.000 claims description 29
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 14
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 13
- 229910052750 molybdenum Inorganic materials 0.000 claims description 13
- 239000011733 molybdenum Substances 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 11
- 239000007858 starting material Substances 0.000 claims description 8
- 238000000137 annealing Methods 0.000 claims description 7
- 239000000155 melt Substances 0.000 claims description 6
- 230000007246 mechanism Effects 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 238000003892 spreading Methods 0.000 claims description 3
- 230000007480 spreading Effects 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 2
- 230000003287 optical effect Effects 0.000 abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 8
- 230000003595 spectral effect Effects 0.000 abstract description 7
- 238000005336 cracking Methods 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 6
- 238000013001 point bending Methods 0.000 abstract description 6
- 238000005452 bending Methods 0.000 abstract description 5
- 230000007547 defect Effects 0.000 abstract description 4
- 238000002834 transmittance Methods 0.000 abstract description 3
- 238000005520 cutting process Methods 0.000 abstract description 2
- 238000005498 polishing Methods 0.000 abstract description 2
- 238000005231 Edge Defined Film Fed Growth Methods 0.000 description 14
- 150000002500 ions Chemical class 0.000 description 9
- 230000000694 effects Effects 0.000 description 6
- 238000005728 strengthening Methods 0.000 description 6
- 230000005540 biological transmission Effects 0.000 description 5
- 230000008569 process Effects 0.000 description 5
- 239000002019 doping agent Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 239000011159 matrix material Substances 0.000 description 3
- 238000005204 segregation Methods 0.000 description 3
- 238000001228 spectrum Methods 0.000 description 3
- 230000009471 action Effects 0.000 description 2
- 238000003776 cleavage reaction Methods 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 230000006698 induction Effects 0.000 description 2
- 230000007017 scission Effects 0.000 description 2
- 239000006104 solid solution Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- GANNOFFDYMSBSZ-UHFFFAOYSA-N [AlH3].[Mg] Chemical compound [AlH3].[Mg] GANNOFFDYMSBSZ-UHFFFAOYSA-N 0.000 description 1
- 230000032900 absorption of visible light Effects 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000001458 anti-acid effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000011029 spinel Substances 0.000 description 1
- 229910052596 spinel Inorganic materials 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
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- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
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CN201310008435.6A CN103014856B (zh) | 2013-01-10 | 2013-01-10 | 掺铁钛蓝宝石晶片及其制备方法 |
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CN201310008435.6A CN103014856B (zh) | 2013-01-10 | 2013-01-10 | 掺铁钛蓝宝石晶片及其制备方法 |
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CN103014856A CN103014856A (zh) | 2013-04-03 |
CN103014856B true CN103014856B (zh) | 2015-11-04 |
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Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103882520A (zh) * | 2014-04-04 | 2014-06-25 | 玉溪市明珠晶体材料有限公司 | 饰品级蓝宝石单晶体的生长方法 |
CN106149053A (zh) * | 2015-04-13 | 2016-11-23 | 中国科学院上海硅酸盐研究所 | 一种导模法生长高灵敏度热释光掺碳蓝宝石晶体的方法 |
CN105538813A (zh) * | 2015-12-09 | 2016-05-04 | 安徽海聚信息科技有限责任公司 | 一种蓝宝石屏幕及其生产工艺 |
CN107022792A (zh) * | 2017-02-28 | 2017-08-08 | 梧州市东麟宝石机械有限公司 | 一种人工合成蓝宝石的制备方法 |
CN108663381B (zh) * | 2018-05-09 | 2020-12-01 | 中国科学院长春光学精密机械与物理研究所 | 一种掺铁激光晶体缺陷检测方法和装置 |
Citations (8)
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CN1362384A (zh) * | 2002-01-11 | 2002-08-07 | 烟台北极星华晶宝石有限责任公司 | 一种合成蓝宝石及其生产工艺 |
CN101280458A (zh) * | 2007-12-28 | 2008-10-08 | 中国科学院上海光学精密机械研究所 | 导模法生长掺碳蓝宝石晶体的方法 |
CN101906663A (zh) * | 2010-08-09 | 2010-12-08 | 西峡县正弘单晶刚玉有限责任公司 | 蓝色超单晶刚玉及其制备方法 |
CN101941727A (zh) * | 2010-09-14 | 2011-01-12 | 李振亚 | 作为焰熔法生产蓝宝石晶体之原料的氧化铝粉末生产方法 |
CN102586866A (zh) * | 2012-02-09 | 2012-07-18 | 上海施科特光电材料有限公司 | 在采用导模法生长片状蓝宝石过程中抑制气泡的方法 |
US8236102B1 (en) * | 2008-01-30 | 2012-08-07 | Solid State Scientific Corporation | Hydrothermal methods of fabricating trivalent-metal-ion-doped sapphire crystals |
CN102817072A (zh) * | 2012-07-30 | 2012-12-12 | 鸿福晶体科技(安徽)有限公司 | 一种用于导模法生长宝石单晶生长的掺杂原料的制备方法 |
CN103710743A (zh) * | 2012-09-28 | 2014-04-09 | 苹果公司 | 连续蓝宝石生长 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
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JPS59116188A (ja) * | 1982-12-22 | 1984-07-04 | Seiko Epson Corp | ブル−サフアイヤの合成方法 |
JPS59174599A (ja) * | 1983-03-24 | 1984-10-03 | Seiko Epson Corp | ブル−サフアイヤ人工結晶合成法 |
JP2004123467A (ja) * | 2002-10-03 | 2004-04-22 | Shinkosha:Kk | サファイア単結晶およびサファイア単結晶用原料 |
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Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1362384A (zh) * | 2002-01-11 | 2002-08-07 | 烟台北极星华晶宝石有限责任公司 | 一种合成蓝宝石及其生产工艺 |
CN101280458A (zh) * | 2007-12-28 | 2008-10-08 | 中国科学院上海光学精密机械研究所 | 导模法生长掺碳蓝宝石晶体的方法 |
US8236102B1 (en) * | 2008-01-30 | 2012-08-07 | Solid State Scientific Corporation | Hydrothermal methods of fabricating trivalent-metal-ion-doped sapphire crystals |
CN101906663A (zh) * | 2010-08-09 | 2010-12-08 | 西峡县正弘单晶刚玉有限责任公司 | 蓝色超单晶刚玉及其制备方法 |
CN101941727A (zh) * | 2010-09-14 | 2011-01-12 | 李振亚 | 作为焰熔法生产蓝宝石晶体之原料的氧化铝粉末生产方法 |
CN102586866A (zh) * | 2012-02-09 | 2012-07-18 | 上海施科特光电材料有限公司 | 在采用导模法生长片状蓝宝石过程中抑制气泡的方法 |
CN102817072A (zh) * | 2012-07-30 | 2012-12-12 | 鸿福晶体科技(安徽)有限公司 | 一种用于导模法生长宝石单晶生长的掺杂原料的制备方法 |
CN103710743A (zh) * | 2012-09-28 | 2014-04-09 | 苹果公司 | 连续蓝宝石生长 |
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Denomination of invention: Ferric-titanium-doped sapphire wafer and preparation method thereof Effective date of registration: 20190619 Granted publication date: 20151104 Pledgee: JIANGXI WEIJIA CHUANGZHAN ENTERPRISE MANAGEMENT Co.,Ltd. Pledgor: JIANGXI EAST OCEAN SAPPHIRE OPTOELECTRONICS TECHNOLOGY CO.,LTD. Registration number: 2019360000018 |
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