CN103012467B - 一种在co2超临界状态下制备高度乙酰化大豆磷脂的方法 - Google Patents
一种在co2超临界状态下制备高度乙酰化大豆磷脂的方法 Download PDFInfo
- Publication number
- CN103012467B CN103012467B CN201110278485.7A CN201110278485A CN103012467B CN 103012467 B CN103012467 B CN 103012467B CN 201110278485 A CN201110278485 A CN 201110278485A CN 103012467 B CN103012467 B CN 103012467B
- Authority
- CN
- China
- Prior art keywords
- soybean phospholipid
- highly acetylated
- supercritical state
- reaction
- phosphatide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000000034 method Methods 0.000 title claims abstract description 42
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 title claims abstract description 22
- 239000008347 soybean phospholipid Substances 0.000 title claims abstract description 22
- 238000006243 chemical reaction Methods 0.000 claims abstract description 13
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims abstract description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 4
- 229940067606 lecithin Drugs 0.000 claims description 3
- 239000000787 lecithin Substances 0.000 claims description 3
- 235000010445 lecithin Nutrition 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 2
- 238000000605 extraction Methods 0.000 claims description 2
- 238000006386 neutralization reaction Methods 0.000 claims description 2
- 238000012512 characterization method Methods 0.000 claims 1
- 239000007788 liquid Substances 0.000 abstract description 7
- WTJKGGKOPKCXLL-RRHRGVEJSA-N phosphatidylcholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCCC=CCCCCCCCC WTJKGGKOPKCXLL-RRHRGVEJSA-N 0.000 abstract description 5
- 230000035484 reaction time Effects 0.000 abstract description 5
- 239000012530 fluid Substances 0.000 abstract description 4
- 239000007789 gas Substances 0.000 abstract description 4
- 238000004090 dissolution Methods 0.000 abstract description 2
- 238000004134 energy conservation Methods 0.000 abstract description 2
- 230000004048 modification Effects 0.000 abstract description 2
- 238000012986 modification Methods 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 description 9
- 238000007385 chemical modification Methods 0.000 description 3
- JZNWSCPGTDBMEW-UHFFFAOYSA-N Glycerophosphorylethanolamin Natural products NCCOP(O)(=O)OCC(O)CO JZNWSCPGTDBMEW-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003995 emulsifying agent Substances 0.000 description 2
- 150000008104 phosphatidylethanolamines Chemical class 0.000 description 2
- 229940067626 phosphatidylinositols Drugs 0.000 description 2
- 150000003905 phosphatidylinositols Chemical class 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000009736 wetting Methods 0.000 description 2
- 238000004965 Hartree-Fock calculation Methods 0.000 description 1
- 238000005917 acylation reaction Methods 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- -1 lecithin phospholipid Chemical class 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 230000005501 phase interface Effects 0.000 description 1
- 150000008103 phosphatidic acids Chemical class 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110278485.7A CN103012467B (zh) | 2011-09-20 | 2011-09-20 | 一种在co2超临界状态下制备高度乙酰化大豆磷脂的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110278485.7A CN103012467B (zh) | 2011-09-20 | 2011-09-20 | 一种在co2超临界状态下制备高度乙酰化大豆磷脂的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103012467A CN103012467A (zh) | 2013-04-03 |
CN103012467B true CN103012467B (zh) | 2015-12-16 |
Family
ID=47961617
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201110278485.7A Active CN103012467B (zh) | 2011-09-20 | 2011-09-20 | 一种在co2超临界状态下制备高度乙酰化大豆磷脂的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103012467B (zh) |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1035436C (zh) * | 1994-03-07 | 1997-07-16 | 中国科学院山西煤炭化学研究所 | 超临界co2抽提高纯度卵黄磷脂的方法 |
EP1004245A2 (de) * | 1998-11-27 | 2000-05-31 | Krupp Uhde GmbH | Verfahren zur Gewinnung insbesondere von Lecithin aus Trockenei |
CN1634939A (zh) * | 2003-12-29 | 2005-07-06 | 黑龙江省大豆技术开发研究中心 | 一种超临界co2提取大豆卵磷脂的方法 |
CN1687084A (zh) * | 2005-04-30 | 2005-10-26 | 海城后英生物工程有限公司 | 大豆卵磷脂的加工工艺 |
CN101423530A (zh) * | 2007-10-30 | 2009-05-06 | 东北农业大学 | 一种用超临界co2为溶解剂氢化大豆磷脂的方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003000192A2 (en) * | 2001-06-22 | 2003-01-03 | Raveendran Poovathinthodiyil | Renewable, carbohydrate based co2-philes |
-
2011
- 2011-09-20 CN CN201110278485.7A patent/CN103012467B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1035436C (zh) * | 1994-03-07 | 1997-07-16 | 中国科学院山西煤炭化学研究所 | 超临界co2抽提高纯度卵黄磷脂的方法 |
EP1004245A2 (de) * | 1998-11-27 | 2000-05-31 | Krupp Uhde GmbH | Verfahren zur Gewinnung insbesondere von Lecithin aus Trockenei |
CN1634939A (zh) * | 2003-12-29 | 2005-07-06 | 黑龙江省大豆技术开发研究中心 | 一种超临界co2提取大豆卵磷脂的方法 |
CN1687084A (zh) * | 2005-04-30 | 2005-10-26 | 海城后英生物工程有限公司 | 大豆卵磷脂的加工工艺 |
CN101423530A (zh) * | 2007-10-30 | 2009-05-06 | 东北农业大学 | 一种用超临界co2为溶解剂氢化大豆磷脂的方法 |
Non-Patent Citations (2)
Title |
---|
大豆磷脂改性及其改性技术分析;徐振山等;《粮食与油脂》;20081110(第11期);第1.2.1节第3段 * |
大豆磷脂的改性方法及其应用;王利等;《黑龙江八一农垦大学学报》;20020930;第14卷(第3期);第1.2节第2段 * |
Also Published As
Publication number | Publication date |
---|---|
CN103012467A (zh) | 2013-04-03 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN108450954A (zh) | 一种亚麻籽油微胶囊及其制备方法 | |
Shao et al. | Chemical stability and in vitro release properties of β-carotene in emulsions stabilized by Ulva fasciata polysaccharide | |
CN106509893A (zh) | 一种精油微胶囊及其制备方法 | |
CN102362864A (zh) | 提高维生素a或维生素d3微胶囊流散性和堆密度的方法 | |
CN106311157A (zh) | 一种具有吸附作用复合膜的制备方法 | |
CN107242347B (zh) | 一种以豆粕为原料利用酶复合处理提高大豆蛋白起泡性的方法 | |
CN103012467B (zh) | 一种在co2超临界状态下制备高度乙酰化大豆磷脂的方法 | |
CN108504708A (zh) | 一种提高面筋蛋白溶解性的方法 | |
CN106467725A (zh) | 一种生物质钻井液基础液、其制备方法及其应用 | |
CN107311882A (zh) | 一种脱氢枞酸基二肽表面活性剂及其性能 | |
CN105295162B (zh) | 一种聚乙烯蜡微乳液及其制备方法 | |
CN110105542A (zh) | 一种双亲油基改性双酚a型环氧树脂表面活性剂及其制备方法与应用 | |
CN109911907A (zh) | 一种超细高吸油值食品级二氧化硅的制备方法及产品 | |
CN101390588B (zh) | 一种利用高压均质改性大米淀粉制备的油脂微胶囊及其方法 | |
CN103306134B (zh) | 一种类能改性蛋白质纤维的表面处理剂及其制备方法和用途 | |
CN103005458B (zh) | 一种盐生杜氏藻β-胡萝卜素微胶囊及其制备方法 | |
CN105456225B (zh) | 一种维生素e软胶囊及其制备方法 | |
CN104448009A (zh) | 食品级耐酸型羧甲基纤维素钠的制备方法 | |
CN108440682A (zh) | 一种膦酸化海带多糖的制备方法 | |
CN102731796B (zh) | 蛋白质基表面活性剂丝蛋白酸钙的制备方法 | |
CN110028597A (zh) | 一种柚皮果胶的提取方法 | |
CN106386809A (zh) | 一种高含量的稻瘟酰胺悬浮剂及制备方法 | |
CN109938291A (zh) | 一种营养强化水解蛋黄粉及其加工方法 | |
Chen et al. | Effect of compressed CO 2 on the chloroperoxidase catalyzed halogenation of 1, 3-dihydroxybenzene in reverse micelles | |
CN106260104B (zh) | 一种复合植物油微乳液及其制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20170830 Address after: Xiangfang District of Heilongjiang city of Harbin province haping road 150001 No. 1 Patentee after: The 93 group Harbin Wellcome Food Co. Ltd. Address before: 150030, room 6, building 104, 3 Bei'an street, Daoli District, Heilongjiang, Harbin Patentee before: Yu Dianyu |
|
TR01 | Transfer of patent right | ||
CP01 | Change in the name or title of a patent holder |
Address after: 150001 No.1, haping East Road, Xiangfang District, Harbin City, Heilongjiang Province Patentee after: Jiusan Food Co.,Ltd. Address before: 150001 No.1, haping East Road, Xiangfang District, Harbin City, Heilongjiang Province Patentee before: THE NINE THREE GROUP HARBIN WELLCOME FOOD Co.,Ltd. |
|
CP01 | Change in the name or title of a patent holder |