CN102998218A - Method and device for testing dynamic viscosity of glass lubricant - Google Patents

Method and device for testing dynamic viscosity of glass lubricant Download PDF

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Publication number
CN102998218A
CN102998218A CN2012104761163A CN201210476116A CN102998218A CN 102998218 A CN102998218 A CN 102998218A CN 2012104761163 A CN2012104761163 A CN 2012104761163A CN 201210476116 A CN201210476116 A CN 201210476116A CN 102998218 A CN102998218 A CN 102998218A
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China
Prior art keywords
glass lubricant
heating furnace
plate pattern
cope match
kinetic viscosity
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Pending
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CN2012104761163A
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Chinese (zh)
Inventor
王忠堂
梁海成
齐广霞
张士宏
程明
李德富
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Shenyang Ligong University
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Shenyang Ligong University
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Priority to CN2012104761163A priority Critical patent/CN102998218A/en
Publication of CN102998218A publication Critical patent/CN102998218A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a method and a device for testing the dynamic viscosity of a glass lubricant. The device comprises an operating platform, and is characterized in that a heating furnace is arranged on the operating platform, an upper template and a lower template are arranged in the heating furnace in parallel, the glass lubricant is filled between the upper template and the lower template, a thermocouple is inserted in the glass lubricant, a pressure bar inwards penetrates through the middle of a top arm of the heating furnace, a steel ball is arranged on the front end of the pressure bar, the steel ball supports against the upper template, a displacement sensor is arranged on the outer wall of the heating furnace, a slide wheel is arranged on one side of the operating platform, a draw cord is arranged on the slide wheel, one end of the draw cord is connected with one side of the upper template, and the other end of the draw cord is connected with a balance weight through a dynamometer. The device for testing the dynamic viscosity of the glass lubricant can be used for measuring the dynamic viscosity in high temperature (above 1000 DEG C), also measuring the dynamic viscosity of the glass lubricant in the condition of pressure, and has the advantages of simple structure and accuracy in measurement and the like.

Description

A kind of glass lubricant kinetic viscosity method of testing and device
Technical field
Patent of the present invention belongs to the research field of glass lubricant greasy property when high temperature, goes for the test of other lubricant kinetic viscosity.
Background technology
The Applicable temperature scope of glass lubricant is 900 ~ 1200 ℃, is mainly used in the plastic forming process of high temperature alloy or titanium alloy component.In the hot forming process, the variation of the viscosity with temperature of glass lubricant and changing, can make glass lubricant be in best lubricating effect very important for the shaping of high temperature alloy or titanium alloy component, and the best lubricating effect of glass lubricant depends on its kinetic viscosity, therefore, relation when high temperature between the kinetic viscosity of glass lubricant and temperature, the pressure etc. is one of the major technique that realizes the forming technology of high temperature alloy or titanium alloy component.
Viscosity is an important indicator of glass lubricant, and it plays an important role in the hot extrusion process of steel, usually represents with kinetic viscosity.Kinetic viscosity has characterized the size of fluid viscosity internal friction.Owing to moulds of industrial equipment temperature, the factors such as variation of running time, extrusion temperature has certain variation during hot extrusion, therefore requires the high temperature viscosity of glass to change little in the extrusion temperature scope.Rule of thumb, when hot extrusion, the viscosity of glass lubricant is when 30 ~ 100 Pa.s scope, and lubricant effect is better.Viscosity too hour, the lubricating film anti-pressure ability is poor, and irregular flowing occurs during hot extrusion easily, from the die orifice ejection and consume rapidly.When viscosity was too large, friction factor was too large, does not have lubricant effect.When different steel grades is carried out hot extrusion, because therefore technological parameter (extrusion temperature, extrusion speed) difference must choose suitable glass lubricant, its viscosity and extrusion process are complementary.
Summary of the invention
Purpose of the present invention is exactly curve and the deficiency that exists for overcoming above-mentioned prior art, and a kind of glass lubricant kinetic viscosity adhesion test method and device are proposed, the kinetic viscosity of (more than 1000 ℃) when adopting method and apparatus of the present invention not only can measure high temperature also can be measured the kinetic viscosity of the glass lubricant under the different pressures condition.So that the relation between research kinetic viscosity and temperature, the pressure.
Adopt technical scheme be:
A kind of glass lubricant kinetic viscosity proving installation, comprise worktable, one side of worktable is fixed with semi-girder, be provided with a heating furnace on the worktable, be arranged with cope match-plate pattern and lower bolster in the heating furnace in parallel, between cope match-plate pattern and the lower bolster glass lubricant is arranged, be inserted with a thermopair in the glass lubricant, the middle part of heating furnace top arm has inwardly penetrated a press rods, the front end of press rods is equiped with steel ball, steel ball is supported on cope match-plate pattern, be equiped with displacement transducer on the lateral wall of heating furnace, a side of worktable is equiped with a pulley, and stay cord is arranged on the pulley, one end of stay cord is connected with a side of described cope match-plate pattern, and the other end of stay cord is connected with a mass through a draw-bar donamometer.
A kind of glass lubricant kinetic viscosity method of testing is characterized in that may further comprise the steps:
(1) glass lubricant is put between cope match-plate pattern and the lower bolster;
(2) start heating furnace, glass lubricant is heated to 900 ~ 1200 ℃;
(3) increase gradually the weight of weight, until the cope match-plate pattern setting in motion, the reading of record draw-bar donamometer, i.e. tensile force f value, and recorded bit displacement sensor reading calculates translational speed;
(4) according to experimental data, calculated velocity gradient (
Figure 2012104761163100002DEST_PATH_IMAGE001
) value;
(5) the glass lubricant kinetic viscosity value of accounting temperature under 900 ~ 1200 ℃ of conditions;
(6) the normal pressure P value on the change press rods repeats above (1) to (5) step, just can obtain the glass lubricant kinetic viscosity value under certain pressure.
The kinetic viscosity of (more than 1000 ℃) when the present invention not only can measure high temperature also can be measured the kinetic viscosity of glass lubricant under stress, has the advantages such as measurement simple in structure is accurate.
Description of drawings
Fig. 1 is structural representation of the present invention.
Embodiment
A kind of glass lubricant kinetic viscosity proving installation, comprise worktable 10, be provided with a heating furnace 3 on the worktable 10, be arranged with cope match-plate pattern 6 and lower bolster 9 in the heating furnace 3 in parallel, between cope match-plate pattern 6 and the lower bolster 9 glass lubricant 7 is arranged, be inserted with a thermopair 8 in the glass lubricant 7, the middle part of heating furnace 3 top arms has inwardly penetrated a press rods 4, the front end of press rods 4 is equiped with steel ball 5, steel ball 5 is supported on cope match-plate pattern 6, be equiped with displacement transducer 11 on the lateral wall of heating furnace 3, one side of worktable 10 is equiped with a pulley 1, stay cord 13 is arranged on the pulley 1, and an end of stay cord 13 is connected with a side of cope match-plate pattern 6, and the other end of stay cord 13 is connected with a mass 12 through a draw-bar donamometer 2.
A kind of glass lubricant kinetic viscosity method of testing may further comprise the steps:
(1) glass lubricant 7 is put between cope match-plate pattern 6 shown in Figure 1 and the lower bolster 9;
(2) start heating furnace 3, glass lubricant is heated to 1000 ℃;
(3) increase gradually the weight of weight 12, until cope match-plate pattern 6 setting in motions, the reading of record draw-bar donamometer 2, and recorded bit displacement sensor reading calculate translational speed;
(4) according to experimental data, the calculated velocity gradient value;
(5) the glass lubricant kinetic viscosity value of accounting temperature under 1000 ℃ of conditions;
(6) the normal pressure P value on the change press rods 4 repeats above (1) to (5) step, just can obtain the glass lubricant kinetic viscosity value under certain pressure.
Patent of the present invention, the kinetic viscosity of (more than 1000 ℃) in the time of not only can measuring high temperature also can be measured the kinetic viscosity of glass lubricant under stress.So that the relation between research kinetic viscosity and temperature, the pressure.

Claims (2)

1. glass lubricant kinetic viscosity proving installation, comprise worktable, it is characterized in that being provided with on the described worktable heating furnace, be arranged with cope match-plate pattern and lower bolster in the heating furnace in parallel, between cope match-plate pattern and the lower bolster glass lubricant is arranged, be inserted with a thermopair in the glass lubricant, the middle part of heating furnace top arm has inwardly penetrated a press rods, the front end of press rods is equiped with steel ball, and steel ball is supported on cope match-plate pattern, is equiped with displacement transducer on the lateral wall of heating furnace, one side of worktable is equiped with a pulley, stay cord is arranged on the pulley, and an end of stay cord is connected with a side of described cope match-plate pattern, and the other end of stay cord is connected with a mass through a draw-bar donamometer.
2. the method for testing of a glass lubricant kinetic viscosity is characterized in that may further comprise the steps:
(1) glass lubricant is put between cope match-plate pattern and the lower bolster;
(2) start heating furnace, glass lubricant is heated to 900 ~ 1200 ℃;
(3) increase gradually the weight of weight, until the cope match-plate pattern setting in motion, the reading of record draw-bar donamometer, i.e. tensile force f value, and recorded bit displacement sensor reading calculates translational speed;
(4) according to experimental data, calculated velocity gradient (
Figure 40234DEST_PATH_IMAGE001
) value;
(5) the glass lubricant kinetic viscosity value of accounting temperature under 900 ~ 1200 ℃ of conditions;
(6) the normal pressure P value on the change press rods repeats above (1) to (5) step, just can obtain the glass lubricant kinetic viscosity value under certain pressure.
CN2012104761163A 2012-11-22 2012-11-22 Method and device for testing dynamic viscosity of glass lubricant Pending CN102998218A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012104761163A CN102998218A (en) 2012-11-22 2012-11-22 Method and device for testing dynamic viscosity of glass lubricant

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Application Number Priority Date Filing Date Title
CN2012104761163A CN102998218A (en) 2012-11-22 2012-11-22 Method and device for testing dynamic viscosity of glass lubricant

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103480974A (en) * 2013-09-26 2014-01-01 郑州机械研究所 Measuring device and method for measuring high temperature viscosity of liquid brazing filler metal by using measuring device
CN104359791A (en) * 2014-11-10 2015-02-18 上海市离心机械研究所有限公司 Device for measuring adhesive phase of wet mud
CN113447398A (en) * 2021-06-18 2021-09-28 沈阳理工大学 Testing device and testing method for steel fiber concrete fluidity representation

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1886793A1 (en) * 2006-08-11 2008-02-13 Karl Hehl Method and device for manufacturing a 3D object and use of a plastifying unit for its manufacture
WO2008074102A1 (en) * 2006-12-20 2008-06-26 National Institute Of Ocean Technology - Niot Campus Composition coating for biofouling protection
CN202916163U (en) * 2012-11-20 2013-05-01 沈阳理工大学 Device for testing kinetic viscosity of glass lubricating agent

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1886793A1 (en) * 2006-08-11 2008-02-13 Karl Hehl Method and device for manufacturing a 3D object and use of a plastifying unit for its manufacture
WO2008074102A1 (en) * 2006-12-20 2008-06-26 National Institute Of Ocean Technology - Niot Campus Composition coating for biofouling protection
CN202916163U (en) * 2012-11-20 2013-05-01 沈阳理工大学 Device for testing kinetic viscosity of glass lubricating agent

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103480974A (en) * 2013-09-26 2014-01-01 郑州机械研究所 Measuring device and method for measuring high temperature viscosity of liquid brazing filler metal by using measuring device
CN103480974B (en) * 2013-09-26 2015-12-02 郑州机械研究所 A kind of method measuring liquid solder high temperature viscosity
CN104359791A (en) * 2014-11-10 2015-02-18 上海市离心机械研究所有限公司 Device for measuring adhesive phase of wet mud
CN113447398A (en) * 2021-06-18 2021-09-28 沈阳理工大学 Testing device and testing method for steel fiber concrete fluidity representation

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Application publication date: 20130327