CN102962851A - Multi-purpose glove box - Google Patents

Multi-purpose glove box Download PDF

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Publication number
CN102962851A
CN102962851A CN2012105331637A CN201210533163A CN102962851A CN 102962851 A CN102962851 A CN 102962851A CN 2012105331637 A CN2012105331637 A CN 2012105331637A CN 201210533163 A CN201210533163 A CN 201210533163A CN 102962851 A CN102962851 A CN 102962851A
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China
Prior art keywords
casing
drying
environment
case
inert gas
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CN2012105331637A
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CN102962851B (en
Inventor
苏荣军
苏钰
王军霞
梁多平
郭城
李静文
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Harbin University of Commerce
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Harbin University of Commerce
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Abstract

The conventional glove box has the defects of single purpose and narrow application range. The invention discloses a glove box capable of creating various internal environments through simple transformation. The glove box comprises a box body, interfaces, an ultraviolet lamp and a ventilation pipe, different from other glove boxes, the glove box provided by the invention is characterized in that gloves are communicated with the box body through special connecting ports so as to be convenient to vacuumize; drying and hypoxia in the box body are realized through a unique agent combination and a multi-stage drying and deoxidizing device; and if an filtration, adsorption, sterilization or disinfection agent is adopted, the interior of the box can be sterile, dustless or full of inert gas. The glove box has the advantages of easiness in manufacturing, low cost, good air tightness, vacuumizing capability, multiple purposes, convenience in transformation, high drying and deoxidizing degree and good effect, allows the means of dust filtration, sterilization, disinfection, heat preservation and the like to be used in combination, can create an inert gas environment, can be used for treating harmful gases, is scientific and environment-friendly, and can be used in scientific experiment work in the field of chemistry, biology, medicine, electronics, interdiscipline or the like.

Description

A kind of multi-purpose glove case apparatus
Technical field
What multi-purpose glove case apparatus of the present invention related to is a kind of box body device that can build multiple special operational environment in case.So-called particular surroundings can be dry, hypoxic air environment, aseptic, dust-free air environment or inert gas environment.Can put into various materials, reagent, instrument, mini-plant and instrument in the described casing and consist of different functional devices, people's arm can carry out manual operations by the company gloves in case.
Background technology
Along with the development of science and technology, in the scientific experiments such as chemistry, biology, medicine and pharmacology, physics, electronics, need more and more special operating environment.For example in the electrochemical research field, during the assembling lithium ion battery, lithium electrode is very active, and easily oxidation under the environment of oxygen is being arranged, and is also easily rotten with airborne water molecule reaction.The electrolyte that is used is easily suction decomposition also.Therefore must guarantee that the interior air of control box is very dry and oxygen content is lower.The chemical reaction that also has need to carry out under inert gas shielding; In the research experiment of biology, medicine and pharmacology, often need aseptic, a dustless clean lab space; In some electronic device processing experiment, also need the inert gas shielding environment of drying, anaerobic.In these cases, just need the airtight casing that can create these particular surroundings.During experiment, experimenter's arm is with gloves to stretch in the casing by the gloves interface, carries out the operation that needs through glass.
Learn that from market survey and patent searching document the glove box that exists at present roughly can be divided three classes.
First kind glove box is that the mode that adopts air circulation to purify is come air cleaner drying in the guard box.Want continuous operation work, mostly be connected with more expensive dehumidifier, certain maintenance operation expense etc. is arranged; Be CN03253101.X such as application number, and the patent of N96218352.0.The assistant of making pottery in addition flag, Zheng Gang delivers " Baogang science and technology " fourth phase in 1997<manufacturing and the check of high-vacuum gloves case〉and what report in the literary composition is a kind of stainless glove box of taking out high vacuum (3X10-3Pa), is mainly used in the ndfeb magnet production line.Vacuum is far longer than the present invention, and its small volume, cost are very high.
The Equations of The Second Kind glove box is to adopt to vacuumize first the mode that is filled with again inert gas and build the action required environment.The use inert gas is effective, but an operation that vacuumizes will be arranged, and requires the casing air-tightness good and the very high structural strength of bearing atmospheric pressure arranged.What have also carries vaccum-pumping equipment, complicated and expensive.The relative cost of this class glove box is all higher; Be CN200510007424.1 such as application number, the patent of CN02219258.1.
The 3rd class glove box is to come sterilization with the built-in ultraviolet sterilization lamp of case, with the environment in the purifying box.Can only be used for the small test of biology, chemistry or medicine and pharmacology, build the sterile working environment, institute's tool function is relatively single, is the patent of CN200720063134.3 such as application number.Other Joseph Yam, Gu Jiansheng, Wang Lijuan etc. delivered<use for laboratory small-sized hand casing in the 4th phase of " university chemistry " calendar year 2001〉in the literary composition, be a compact simplified device of making of vacuum desiccator, the operating space is very limited, and purposes is narrower.Li Jianqiu, Xiong Dexin, Wu Xiaoyan, in<development of compact simplified anaerobism glove box and examination〉literary composition that Xu Dianxia etc. delivered in " the Chinese microecology magazine " fifth phase in 1998, described is a kind of ventilation of bleeding, can heat temperature adjustment, can produce the hydrogen oxygen consumption and make the glove box that anaerobic environment is cultivated microorganism.Volume is little, and purposes is comparatively single.Also have other be simple glove box housing utility model patent such as application number be CN200520007967.9.
Also have the first kind and Equations of The Second Kind are combined, as Zhang Ziwei " electromechanical integration " the 5th phase in 2003 deliver<seal box be that a collection is dried, vacuumized, inflated with nitrogen, the equipment that is welded as a whole.This equipment is for the technique that encapsulates by manual welding behind the precise electronic components and parts gas injection.Casing adopts stainless steel to make, and casing welding steel circle is adopted in service ports, glove port sealing, the hole that screws on the steel ring, and the mode that then adds rubber gasket seals.Its sealing is tighter, can accept the relatively high requirement that vacuumizes, and cost is also higher.
Along with the development of science and technology, the experimental study of multidisciplinary intersection is also more and more, and the glove box that has simultaneously several functions has been had new demand now.
Summary of the invention
For the problems referred to above; the problem to be solved in the present invention is: a kind of multi-purpose glove case apparatus is provided, and after the simple transformation configuration, it can build multiple special operating environment; as: aseptic, dustless clean environment, drying, the air ambient of hypoxemia or the environment under the inert gas shielding etc.Can be applicable to the experimental study field of the multiple fields such as chemistry, biology, medicine and pharmacology, electronics or multidisciplinary intersection.It also should have easy to manufacture, cost is low, good airproof performance, the characteristics such as easy to use.
For solving the problems of the technologies described above, the present invention is achieved in that
What glove box of the present invention related to is a kind of casing (4) (such as accompanying drawing 1) that can create the special operational environment.According to action need, this particular surroundings can be dry, low-oxygen gas environment, aseptic, dustfree environment or inert gas environment.Can put into various materials, reagent, mini-plant and instrument in the described casing (4) and can carry out manual operations at case.
For reaching this purpose, the inventor has carried out following design especially through test of many times: 1. designed special gloves operation connector (12), so that can vacuumize.2. designed unique and complete dry cycle device (comprising medicament and equipment), drying efficiency is high, and effect is remarkable.3. designed multiple different configuration in case, the configuration in the casing (4) can be built different environment through simple transformation, and is convenient and swift.
This glove box device formation is divided into fixation kit and convertible assembly two large classes.Fixation kit comprises three parts of facility structure fixing on casing, gloves and casing connector and casing and the bottom surface.Convertible assembly is divided into three covers, is used with fixation kit respectively, can build different operating environments, such as drying, the environment (I) of hypoxemia, aseptic, dustless environment (II) and inert gas environment (III).See accompanying drawing and following description of drawings for details.
Description of drawings
Fig. 1 is the structural representation of multi-purpose glove case apparatus of the present invention
Comprising:
1. sieve tray 2. dryings 3. hooks 4. casings 5. uviol lamps 6. illuminating lamps 7. receptacles
8. scavenge trunk 9. material instruments are imported and exported and seal cover 10. attaching plugs 11. air pumps
12. gloves and casing connector (14~19) 13. sieve aperture glass plates
1. 2. 3. 4. phosphorus pentoxide of calcium oxide of molecular sieve of silica gel.
 
Fig. 2 is the structural representation of described gloves and casing connector (12)
Comprising with lower member:
14. inner joint 15. band flange collar interfaces 16. gloves 17. external tapping seal covers 18. fit sealing cushion rubbers 19. adhesive seal cushion rubbers.
 
Fig. 3 is the air circulation drying apparatus structural representation in the casing (4)
Comprising with lower member:
1. sieve tray 2. dryings 11. air pumps 20. rubber snap rings
1. the 2. 3. dehydrating agent such as calcium oxide of molecular sieve of silica gel.
 
Summary of the invention describes in detail
In conjunction with above-mentioned accompanying drawing and explanation, the below is described in detail.
It is as follows to introduce first fixation kit.
1. the size of casing and material: the feature of described casing (4) is to adopt transparent organic glass to make casing, and high strength bonding glue bond is adopted in each slab joint place, consists of a confined space, and size is approximately: wide X height=80 X of long X 60 X 60 cm 3Also can only have casing front and end face lucite, all the other each faces are airtight with stainless steel, galvanized iron sheet or other, some strength and corrosion-resistant material are arranged.According to concrete condition and the requirement of experiment, transparent plastic film also can be sticked in the chest the inside, and periodic replacement to reduce corrosive gas to the corrosion of casing, prolongs the service life of casing.
2. the structure of gloves and casing connector: there is gloves and the casing connector (12) (such as accompanying drawing 2) of a particular design casing (4) front, socket air-locked, the industrial acid and alkali-resistance emgloves of a pair of (16) on the mouth, and material is butyl rubber.Described gloves and casing connector (12) are the circular holes of opening two diameter 15 cm at the front panel of casing (4), are bonded with special-purpose outstanding inner joint at institute's tapping, comprise being with externally threaded inner joint (14) and band flange collar interface (15).It is upper and pressed by the fit sealing cushion rubber (18) of its overcoat and be fixed on the flange collar that emgloves (16) is enclosed within band flange collar interface (15).Fit sealing cushion rubber (18) material be acrylonitrile-butadiene rubber, size plays the sealing fixation for just in time closely being stuck in after pulling open in the flange collar groove on the band flange collar interface (15).Other has tapped external tapping seal cover (17) only to need low degree to vacuumize, use when taking a breath at casing (4).External tapping seal cover (17) can by screwed on inner joint (14), scribble the vaseline sealant between the screw thread.When vacuumizing, change the winding teflon seal tape between the screw thread into, to guarantee the larger pressure of ability, conveniently vacuumize.Contact position at casing and external tapping seal cover (17) is stained with sealing rubber ring (19), plays sealing function when vacuumizing, and its material is acrylonitrile-butadiene rubber.External tapping seal cover (17) be advisable closely cooperating with internal-and external diameter size dimension and the width of externally threaded inner joint (14) and band flange collar interface (15), reduce the slit as far as possible, the mismachining tolerance surplus that keeps minimum gets final product.Above-mentioned this special gloves and casing connector (12) had both conveniently put on one's gloves and had operated in case, can stack gloves again, cover the vacuum (being about 0.05 atm) of taking out behind the external tapping seal cover (17) to a certain degree, the shortcoming of having avoided general glove box not vacuumize can satisfy the needs of multiple different occasions.
3. fixing facility structure on casing and the bottom surface: (4) two sides of casing leave respectively that a material instrument is imported and exported and with seal cover (9), about 25 cm of its diameter also scribble the vaseline sealant between the external screw thread of carving on the inlet and outlet connectors and the internal thread that covers.When vacuumizing, also change the winding teflon seal tape between the screw thread into, to guarantee the larger pressure of ability, conveniently vacuumize.Also be stained with the sealing rubber ring in similar (19) in the contact position of casing and two seal covers (9), when vacuumizing, play sealing function.The forward lower comer of casing (4) left surface and the rear upper angle of right flank are respectively established a scavenge trunk (8) and are with valve; The uviol lamp (5) that illuminating lamp (6) is arranged on casing (4) inner top surface and only when sterilization, open; The upper right corner, the interior back of casing (4) is equipped with receptacle (7), and lead-in wire seals with PUR by place, the hole on the casing, and two medial surfaces have support hook (3) in the case, can hang small instruments and tools.Left surface middle part horizontal level is equipped with supporting bable tops in the case, is used for placing light article, as is put in 4. phosphorus pentoxide of drier in the culture dish.Casing (4) end added have up and down ventilative sieve aperture poly (methyl methacrylate) plate (13), as the operating table surface in the case, sieve diameter is about 2~3 mm, and is densely arranged.Optionally can place drier, deoxidier, adsorbent etc. under it.
Next introduce convertible assembly, it refers to the different series apparatus combination of disposing for building different operating environments in casing.The below is respectively described below such as drying, the environment (I) of hypoxemia, aseptic, dustless environment (II) and inert gas environment (III) by different operating environments.
I: as when needing the environment (I) of drying, hypoxemia, can install at casing (4) inner bottom surface rear portion gas drier (enlarged drawing is seen accompanying drawing 3) additional, include the low vibrate air circulating pump (11) of small-sized low noise and connecting drying (2), the medicament ware on the supporting bable tops on air outlet place placement lucite kit and the side.Described drying (2) shape as shown in Figure 3, material is polyethylene, head is the cone transition, main body is cylinder, diameter 12 cm.Be divided into two spaces by the sieve tray of three similar sieve trays (1) in the described cylinder, sieve diameter is about 2~3 mm, and is densely arranged.Two kinds of drier of each minute three layers of placement in two spaces in cylinder: 1. silica gel (irregular particle, about 3 mm of equivalent diameter~6 mm) and 2. molecular sieve (cylindrical pellet, diameter are approximately 3~4 mm, and length is approximately 8~12 mm); Next-door neighbour's drying (2) afterbody has 90 ° of angles of multilayer sector lucite box (see figure 3), and the covering of the fan radius is about 10 cm, and bulk storage 3. white powder calcium oxide of drier on it; The supporting bable tops at left surface middle part is placed and is filled the 4. culture dish of phosphorus pentoxide of drier in casing (4); The lower drier of bulk storage dressing in a plurality of culture dishes of sieve aperture poly (methyl methacrylate) plate (13) in casing (4) be phosphorus pentoxide (be white spherical granule, particle diameter is about 0.2~0.6 mm) 4..In addition can be if necessary in above-mentioned every different medicament combination of putting, to reach different purposes, as placing the iron series deoxidizers powder to remove oxygen in the culture dish that bulk storage down of the sieve aperture poly (methyl methacrylate) plate (13) in casing (4).The arranged in order such as supporting bable tops of left surface have been followed the flowing law of air in microenvironment and have been arranged in the box (3.) at above-mentioned vavuum pump (11), drying (2), case angle and the case.It has built an air circulation stream in casing, be conducive to air circulation in the case, the aridity homogeneous of air.During above-mentioned medicament put in order, different dehydrating agents is pressed water separation capability from low to high (1.-2.-3.-4.), is arranged in order along the outlet air circulation stream out by air pump (11), and was scientific and reasonable, saves medicament.Last 4. locate and table top under phosphorus pentoxide can with airborne hydrone generation intense reaction, reach very high aridity.Above-mentioned configuration and order are to determine behind air circulation drying experiment repeatedly, can reach very high degree of drying, fast drying, and efficient is high, and very strong science is arranged.So design the multi-stage drying device that arranges, drying efficiency and strong, the oxygen scavenger deoxidation effect is also fine, also saves medicament and expense.Through suitably running, can realize the interior environment of case of drying, hypoxemia.
II: if when needing aseptic, dustless environment (II), during such as biological, pharmaceutically Bacteria Culture, domestication experiment, then remove above-mentioned drying (2) and various drier and deoxidier.There is pollution to need to purify if advance air in the case, be stained with the rubber snap ring (20) (seeing accompanying drawing 3) that the butadiene-styrene rubber of trough of belt is made at air pump (11) air inlet place, can connect a dust bin of being made by multilayer filter membrane, the lower bulk storage of sieve aperture poly (methyl methacrylate) plate (13) that also can be on casing (4) bottom surface is loaded on the dusty gas adsorbent activity carbon (graininess in a plurality of culture dishes a bit, equivalent diameter 0.4~0.8 mm), be used for filtration, clean air.Uviol lamp (5) can be used for sterilizing.Put into the article that are unsuitable for uviol lamp (5) sterilization such as microorganism etc. such as needs, can wrap up the black paper of thick layer, put into again case.After uviol lamp (5) sterilization finishes, open and use again.Also can as required, in casing (4), put into other disinfectant.Can build so needed aseptic, dustless environment.If any experiment when needing a gaseous environment that is higher than environment temperature, can in casing (4), put into small-sized heater.
III: if when needing inert gas environment (III), if any the experiments such as chemical reaction (high polymer anionic polymerisation), fabrication of electronic components, above-mentioned irrelevant apparatus or material can be taken out.Two scavenge trunks (8) and valve on described casing (4) lateral surface be need to use, external inert gas steel cylinder and vavuum pump.The gloves of casing (4) front are wanted smooth stacking, and external tapping seal cover (17) will be screwed on the inner joint (14), keep sealing.Carry out repetitious minuent and vacuumize and put into inert gas, can realize the inert gas environment in the case.Observe the deformation extent of gloves when vacuumizing, decide suitable vacuum, in time close vavuum pump and open gas valve.If require the inert gas degree higher in the experiment, and experiment generation pernicious gas itself, can in experiment, keep providing continuously inert gas, another scavenge trunk point is opened the valve exhaust.The waste gas of discharging can be linked in sequence acid solution, alkali lye or activated carbon absorbing column by reacting to absorb the absorption pernicious gas, allow what discharge is inert gas after purifying again.Described acid solution is sulfuric acid weak solution (quality is than concentration 5%~20%), and alkali lye is sodium hydroxide solution (quality is than concentration 3%~10%) or calcium hydroxide supersaturated solution, and activated carbon is graininess (2~6 millimeters of granularity).
 
In sum, the present invention has following advantage.
1. the distinctive gloves interface structure design that can take out low vacuum of the present invention conveniently converts air in the case to inert gas environment.
2. drying, device for deoxidizing and medicament scientific allocation are reasonable, and drying and deoxidation efficient and degree are high, also save medicament and expense.
3. when making up dustless, gnotobasis, can select according to circumstances one of means such as filter dirt, sterilization, sterilization and insulation or be used in combination, very flexible.
4. casing and interior accessory is easy to manufacture, cost is low, good airproof performance, easy to use.
5. through simple configuration conversion, can make multiple use, build multiple special operating environment, as: dry, hypoxic air environment, aseptic, dustless clean environment or the environment under the inert gas shielding etc.
6. also be equipped with the pernicious gas disposal method, scientific and reasonable, make things convenient for environmental protection.
Need in the field of scientific studies such as chemistry, biology, medicine and pharmacology, physics, electronics or multidisciplinary intersection can be applicable to the situation of special experimental situation, be suitable in applications such as above-mentioned fields.
 
The specific embodiment
Embodiment 1: at environment dress lithium battery dry, hypoxemia.
Select the interior configuration of the needed case of environment (I) of the drying described in the explanation, hypoxemia.Import and export 9 from the material instrument of casing 4 sides and put into the required material of packed battery, such as lithium, electrolyte, barrier film, battery container, electrode wires, glue rifle, battery carrier, take the photograph material and the instruments such as son, the dry good silica gel of regeneration and molecular sieve, screwing hermetic lid 9.By gloves drying is installed.Open first air pump 11, allow circulated air through the drier in the drying 2 1. silica gel and 2. molecular sieve carried out drying in 10~20 minutes.Open again afterwards the lucite box at angle in the casing 4 interior left sides and culture dish everywhere, allow drier 3. calcium oxide, 4. phosphorus pentoxide and iron series deoxidizers powder are exposed in the air, participate in dry and deoxidation process 10~20 minutes.Close afterwards air pump 11, but continue exposed drier 3. calcium oxide, 4. phosphorus pentoxide and deoxidier.Can obtain the interior environment of case of drying, hypoxemia this moment, the operation that begins to install battery.Behind the EO, cover tightly the bottle cap of various materials, culture dish is everywhere built or drier, deoxidier are recovered in the bottle, in order to avoid further react consumption meaninglessly.Take out the product battery, build seal cover 9.In the aforesaid operations process, such as the needs illumination, can open illuminating lamp 6.Two scavenge trunks and valve on uviol lamp 5 and described casing 4 lateral surfaces keep closing always.The drying of this kind multilevel drying, device for deoxidizing and medicament configuration and deoxidation efficient and degree are high, also save medicament and expense.
Embodiment 2: build aseptic, dustless environment (II).
When the experiment of some biology, medicine and pharmacology, need aseptic, a dustless environment.Select configuration in the needed case of aseptic, dustless environment (II) described in the explanation this moment.Import and export 9 from the material instrument of casing 4 sides and put into experiment required material and the instrument done, screwing hermetic lid 9.Dust bin described in will illustrating by gloves is received on the air inlet 20 of air pump 11, sees Fig. 3, and activated carbon is put into the culture dish everywhere of casing 4, opens air pump 11, begins to purify air, and leaves after opening uviol lamp 5, and indoor can not have the people.If the experiment material that has such as some biological sample, in the time of can not being subjected to the ultraviolet ray irradiation, protect with the black wrapper, put into again case.Return to close air pump 11 and uviol lamp 5 after 15~20 minutes, so just can build needed aseptic, dustless environment.Then just can carry out experimental implementation.Two scavenge trunks 8 and valve on described casing 4 lateral surfaces keep closing always.When practical operation, can select according to circumstances one of means such as filter dirt, sterilization, sterilization and insulation or be used in combination, very flexible.
Embodiment 3: build inert gas environment (III).
If any the experiments such as chemical reaction (such as the high polymer anionic polymerisation), fabrication of electronic components, need inert gas environment, and produce pernicious gas in the experiment.Select configuration in the needed case of inert gas environment (III) described in the explanation this moment.Import and export 9 from the material instrument of casing 4 sides and put into experiment required material and the instrument done, screwing hermetic lid 9.On the folded mouth planes that are flat on flange collar interface 15 of gloves 16, then with external tapping seal cover 17 turn-knobs on inner joint 14.One in the scavenge trunk 8 connects the inert gas steel cylinder, closes first it; Take out in the case air to not too high vacuum with vavuum pump by another scavenge trunk, this vacuum can be born with article, gloves 16 etc. in casing 4 and the case and is advisable, and certain safe clearance is stayed in the deformation of observable gloves 16 and deciding.Then close vavuum pump, open pressure-reducing valve and scavenge trunk valve on the inert gas pipeline, casing 4 is inflated to the front pressure state of bleeding.Repeat again that this bleeds, twice to three times of gas replenishment process, can reach requirement, chemistry or the electronics test specimen that can begin to do are made experiment.In experiment, keep providing continuously inert gas, and the point amount is opened the scavenge trunk valve exhaust of the other end.The waste gas of discharging is linked in sequence acid solution, alkali lye or activated carbon absorption bottle in order to absorb the Adsorption pernicious gas, and the inert gas after purifying is entered ventilation shaft.From then on can find out in the process, the distinctive gloves interface structure design that can take out low vacuum of the present invention, convenient in order to change air into inert gas environment, also be furnished with the pernicious gas disposal method to vacuumizing in the casing 4, scientific and reasonable, makes things convenient for environmental protection.
Above-described embodiment is described the use of apparatus of the present invention, is not that purposes of the present invention and scope are limited.Under the prerequisite that does not break away from design philosophy of the present invention, the various changes and modifications that the professional and technical personnel makes the multi-purpose glove case apparatus among the present invention in this area all belong to protection scope of the present invention.

Claims (6)

1. multi-purpose glove case apparatus, it is characterized in that: be a kind ofly can in case, create multiple special operational environment, and can carry out therein manual casing, different apparatus or material change the outfit in casing, can build different operating environments, the environment (I) that comprises drying, hypoxemia, aseptic, dustless environment (II) and inert gas environment (III), described casing adopt transparent organic glass to make.
2. casing according to claim 1, it is characterized in that: there is gloves and the casing connector of particular design the casing front, it is the circular hole of opening two diameter 15 cm at the front panel of casing, be bonded with special-purpose outstanding inner joint at institute's tapping, comprise and be with externally threaded inner joint and band flange collar interface, emgloves is enclosed within pressing on the flange collar interface and by the fit sealing cushion rubber of its overcoat and being fixed on the flange collar, also has tapped external tapping seal cover, need low degree to vacuumize at casing, use during ventilation, when vacuumizing, twine again teflon seal tape between the screw thread, to guarantee the larger pressure of ability, be stained with the sealing rubber ring of acrylonitrile-butadiene rubber material in the contact position of casing and external tapping seal cover, play sealing function when vacuumizing, above-mentioned this special gloves and casing connector had both conveniently put on one's gloves and had operated in case, can stack gloves again, cover the vacuum of taking out behind the external tapping seal cover to a certain degree, vacuum can reach about 0.05 atm.
3. multi-purpose glove case apparatus according to claim 1, it is characterized in that: two sides of described casing open respectively that material instrument is imported and exported and with seal cover, its diameter is approximately 25 cm, between lid and the interface vaseline sealant is arranged also, teflon seal tape, cover and reach between the casing and be stained with sealing rubber ring, there are two scavenge trunks the casing side and are with valve, the uviol lamp that illuminating lamp is arranged on the casing inner top surface and only when sterilization, open, be equipped with receptacle in the casing, used lead-in wire seals with PUR by the casing place, medial surface is equipped with supporting bable tops in the case, be used for placing light article such as 4. phosphorus pentoxide of the drier that is put in culture dish, the casing inner bottom surface is added to have ventilative up and down sieve aperture poly (methyl methacrylate) plate to operate table top, sieve diameter is about 2~3 mm, densely arranged, its lower drier of optionally can placing, deoxidier, adsorbent etc.
4. drying according to claim 1, the environment of hypoxemia (I), it is characterized in that: install gas drier additional at casing inner bottom surface rear portion, include the low vibrate air circulating pump of small-sized low noise, drying, the lucite kit is placed at the air outlet place, the medicament ware is arranged on the supporting bable tops on the side, described drying material is polyethylene, diameter 12 cm, in three sieve trays are arranged, 1. silica gel (the irregular particle of two kinds of drier of mating formation respectively, about 3 mm of equivalent diameter~6 mm) and 2. molecular sieve (cylindrical pellet, diameter is approximately 3~4 mm, length is approximately 8~12 mm), next-door neighbour's drying afterbody has 90 ° of angles of multilayer sector lucite box, bulk storage 3. white powder calcium oxide of drier on it, 4. phosphorus pentoxide (white spherical granule of the drier of bulk storage dressing in a plurality of culture dishes under the sieve aperture poly (methyl methacrylate) plate in casing, particle diameter is about 0.2~0.6 mm), supporting bable tops placement at the box inside face fills the 4. culture dish of phosphorus pentoxide of drier, above-mentioned medicament optionally can change Powdered iron series deoxidizers into to remove oxygen, above-mentioned vavuum pump, drying, medicament configuration sequence (1.-2.-3.-4.) in the box at case angle and the case, in casing, built an air circulation stream, be conducive to air circulation in the case, drying and deoxidation, phosphorus pentoxide can with airborne hydrone generation intense reaction, obtain very high aridity, so design the multi-stage drying device that arranges, drying efficiency and strong, the oxygen scavenger deoxidation effect is also fine, save medicament and expense, said apparatus can be realized drying through suitably running, environment in the case of hypoxemia.
5. according to claim 1 aseptic, dustless environment (II), it is characterized in that: remove the drying described in the claims 4, various drier and deoxidier, on the rubber ring with draw-in groove that the air pump air inlet is stained with, connect a dust bin of being made by multilayer filter membrane, bulk storage is loaded on the pollutant absorbent activated carbon (graininess in a plurality of culture dishes a bit under the sieve aperture poly (methyl methacrylate) plate on tank floor, equivalent diameter 0.4~0.8 mm), be used for filtering, clean air, uviol lamp can be used for sterilizing, like this through suitably running, can build needed aseptic, dustless clean environment, also can be as required, in casing, put into other disinfectant, perhaps put into small-sized heater, improve the temperature inside the box.
6. according to claim inert gas environment claimed in claim 1 (III), it is characterized in that: the special apparatus described in the claims 4 and 5 or material are taken out, two scavenge trunks on the casing lateral surface are distinguished external inert gas steel cylinder and vavuum pump, the gloves of casing front are wanted smooth stacking, the external tapping seal cover is screwed in and keeps sealing on the inner joint, carry out repetitious minuent and vacuumize and put into inert gas, can realize the inert gas environment in the case, if experiment produces pernicious gas in the case, can in experiment, provide continuously inert gas by one in the scavenge trunk, another scavenge trunk point is opened the valve exhaust, the waste gas of the discharging sour absorption liquid that to be linked in sequence, alkali absorption liquid or active carbon adsorption filter gas cylinder, to adsorb pernicious gas and pollutant by reactive absorption, the inert gas after the purification is discharged again.
CN201210533163.7A 2012-12-11 2012-12-11 Multi-purpose glove box Expired - Fee Related CN102962851B (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN201210533163.7A CN102962851B (en) 2012-12-11 2012-12-11 Multi-purpose glove box

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Cited By (29)

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CN103412109A (en) * 2013-07-30 2013-11-27 青岛华盛达物联科技有限公司 Isolated-type explosion-protection checking and mounting box for battery
CN104057468A (en) * 2014-06-25 2014-09-24 万英南 Reliable purification glove box
CN104070541A (en) * 2014-06-19 2014-10-01 袁洪林 Simple glove box and using method thereof
CN104097216A (en) * 2014-07-30 2014-10-15 万英南 Glove box system for removing hydrogen fluoride
CN104175333A (en) * 2014-07-22 2014-12-03 张德龙 Multifunctional glovebox purification device
CN104400796A (en) * 2014-10-14 2015-03-11 长沙米淇仪器设备有限公司 All-transparent vacuum glove box and application method thereof
CN105145353A (en) * 2015-08-08 2015-12-16 李沾云 Rapid inducing medium device for tissue culture of Alhagi sparsifolia Shap
CN105400694A (en) * 2015-12-21 2016-03-16 天津亿海生物科技有限公司 Cell culture system
CN105664661A (en) * 2016-03-29 2016-06-15 威格气体纯化科技(苏州)股份有限公司 Nitrogen-removing purification column and glove box
CN105688595A (en) * 2016-03-29 2016-06-22 威格气体纯化科技(苏州)股份有限公司 Ozone removal purifying column and glove box
CN105922289A (en) * 2016-05-31 2016-09-07 四川金域医学检验中心有限公司 Inspection device
CN106037938A (en) * 2016-06-25 2016-10-26 利辛县眼病防治所 Wearable glove device
CN106078809A (en) * 2016-05-31 2016-11-09 四川金域医学检验中心有限公司 A kind of small-size laboratory inspection equipment
CN106442934A (en) * 2016-09-28 2017-02-22 中国科学院亚热带农业生态研究所 Method and device for collecting nitrogen produced by soil denitrifying microorganisms
CN106493754A (en) * 2016-12-20 2017-03-15 河南华瑞高新材料科技股份有限公司 A kind of Double layer rotating pallet that may be installed in glove box
CN107174425A (en) * 2017-06-15 2017-09-19 中国人民解放军第四军医大学 Department of B urn critical patient special sterile Isolation bed
CN107863170A (en) * 2017-10-27 2018-03-30 中核四0四有限公司 MOX pellet preparation technology radiation protection methods
CN107881351A (en) * 2017-11-30 2018-04-06 广东先导先进材料股份有限公司 The device for deoxidizing and method of high purity arsenic
CN109109025A (en) * 2017-06-26 2019-01-01 天津大学 A kind of simple anaerobic operation case
CN109563456A (en) * 2016-07-27 2019-04-02 昕芙旎雅有限公司 Sterile gloves case
CN110470908A (en) * 2019-08-19 2019-11-19 天津大学 Solid electrode oxidation film is studied to the device and method of liquid-solid contact Resistance Influence
CN111240131A (en) * 2020-03-17 2020-06-05 中国科学院云南天文台 Manufacturing method of transparent hemispherical cover and transparent hemispherical cover
CN111452094A (en) * 2020-03-26 2020-07-28 上海微纳国际贸易有限公司 Operation method under working condition with pressure difference
CN111500428A (en) * 2020-04-08 2020-08-07 北京茵维德生物科技有限公司 Low-pressure biological culture device and method
CN112659191A (en) * 2019-10-16 2021-04-16 深圳市中认联科检测技术有限公司 Totally-enclosed battery disassembling equipment and method thereof
CN112691209A (en) * 2020-12-01 2021-04-23 苏州爱力想电子科技有限公司 Fixing device for operating gloves
CN113384423A (en) * 2021-07-09 2021-09-14 中国人民解放军海军军医大学第一附属医院 Simple sterile closed nude mouse operation assembly
CN113977640A (en) * 2021-12-08 2022-01-28 浙江立宇设备成套有限公司 Thick wall glove box
CN114407360A (en) * 2022-01-27 2022-04-29 南京铖联激光科技有限公司 Glove box for 3D printing

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CN2201940Y (en) * 1994-04-28 1995-06-28 廖白霞 Multi-functional gloves box
CN201046574Y (en) * 2007-05-08 2008-04-16 赵天从 Simple type glove box
CN101406854A (en) * 2008-11-06 2009-04-15 上海理工大学 Vacuum environment control box for preparing nano fluid
JP3163435U (en) * 2010-08-03 2010-10-14 株式会社コクゴ Gloves for glove box
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Cited By (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103412109A (en) * 2013-07-30 2013-11-27 青岛华盛达物联科技有限公司 Isolated-type explosion-protection checking and mounting box for battery
CN104070541B (en) * 2014-06-19 2016-03-23 袁洪林 A kind of Simple hand casing and using method thereof
CN104070541A (en) * 2014-06-19 2014-10-01 袁洪林 Simple glove box and using method thereof
CN104057468A (en) * 2014-06-25 2014-09-24 万英南 Reliable purification glove box
CN104057468B (en) * 2014-06-25 2016-05-25 万英南 A kind of glove box that purifies reliably
CN104175333A (en) * 2014-07-22 2014-12-03 张德龙 Multifunctional glovebox purification device
CN104175333B (en) * 2014-07-22 2016-04-20 威格气体纯化科技(苏州)股份有限公司 A kind of multifunctional hand casing purifier
CN104097216A (en) * 2014-07-30 2014-10-15 万英南 Glove box system for removing hydrogen fluoride
CN104400796A (en) * 2014-10-14 2015-03-11 长沙米淇仪器设备有限公司 All-transparent vacuum glove box and application method thereof
CN105145353A (en) * 2015-08-08 2015-12-16 李沾云 Rapid inducing medium device for tissue culture of Alhagi sparsifolia Shap
CN105400694A (en) * 2015-12-21 2016-03-16 天津亿海生物科技有限公司 Cell culture system
CN105664661A (en) * 2016-03-29 2016-06-15 威格气体纯化科技(苏州)股份有限公司 Nitrogen-removing purification column and glove box
CN105688595A (en) * 2016-03-29 2016-06-22 威格气体纯化科技(苏州)股份有限公司 Ozone removal purifying column and glove box
CN105922289A (en) * 2016-05-31 2016-09-07 四川金域医学检验中心有限公司 Inspection device
CN106078809A (en) * 2016-05-31 2016-11-09 四川金域医学检验中心有限公司 A kind of small-size laboratory inspection equipment
CN106037938A (en) * 2016-06-25 2016-10-26 利辛县眼病防治所 Wearable glove device
CN109563456A (en) * 2016-07-27 2019-04-02 昕芙旎雅有限公司 Sterile gloves case
CN106442934A (en) * 2016-09-28 2017-02-22 中国科学院亚热带农业生态研究所 Method and device for collecting nitrogen produced by soil denitrifying microorganisms
CN106493754B (en) * 2016-12-20 2018-11-13 河南华瑞高新材料有限公司 A kind of Double layer rotating pallet in glove box
CN106493754A (en) * 2016-12-20 2017-03-15 河南华瑞高新材料科技股份有限公司 A kind of Double layer rotating pallet that may be installed in glove box
CN107174425A (en) * 2017-06-15 2017-09-19 中国人民解放军第四军医大学 Department of B urn critical patient special sterile Isolation bed
CN109109025A (en) * 2017-06-26 2019-01-01 天津大学 A kind of simple anaerobic operation case
CN107863170A (en) * 2017-10-27 2018-03-30 中核四0四有限公司 MOX pellet preparation technology radiation protection methods
CN107881351A (en) * 2017-11-30 2018-04-06 广东先导先进材料股份有限公司 The device for deoxidizing and method of high purity arsenic
CN110470908A (en) * 2019-08-19 2019-11-19 天津大学 Solid electrode oxidation film is studied to the device and method of liquid-solid contact Resistance Influence
CN112659191A (en) * 2019-10-16 2021-04-16 深圳市中认联科检测技术有限公司 Totally-enclosed battery disassembling equipment and method thereof
CN112659191B (en) * 2019-10-16 2024-04-05 深圳市中认联科检测技术有限公司 Battery totally-enclosed disassembly equipment and method thereof
CN111240131A (en) * 2020-03-17 2020-06-05 中国科学院云南天文台 Manufacturing method of transparent hemispherical cover and transparent hemispherical cover
CN111452094A (en) * 2020-03-26 2020-07-28 上海微纳国际贸易有限公司 Operation method under working condition with pressure difference
CN111500428A (en) * 2020-04-08 2020-08-07 北京茵维德生物科技有限公司 Low-pressure biological culture device and method
CN112691209A (en) * 2020-12-01 2021-04-23 苏州爱力想电子科技有限公司 Fixing device for operating gloves
CN113384423A (en) * 2021-07-09 2021-09-14 中国人民解放军海军军医大学第一附属医院 Simple sterile closed nude mouse operation assembly
CN113977640A (en) * 2021-12-08 2022-01-28 浙江立宇设备成套有限公司 Thick wall glove box
CN114407360A (en) * 2022-01-27 2022-04-29 南京铖联激光科技有限公司 Glove box for 3D printing
CN114407360B (en) * 2022-01-27 2023-08-08 南京铖联激光科技有限公司 Glove box for 3D printing

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