CN102935392A - Horizontally fixing device of diffusion vessel and use method of horizontally fixing device - Google Patents

Horizontally fixing device of diffusion vessel and use method of horizontally fixing device Download PDF

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Publication number
CN102935392A
CN102935392A CN2012104771413A CN201210477141A CN102935392A CN 102935392 A CN102935392 A CN 102935392A CN 2012104771413 A CN2012104771413 A CN 2012104771413A CN 201210477141 A CN201210477141 A CN 201210477141A CN 102935392 A CN102935392 A CN 102935392A
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China
Prior art keywords
support bar
diffusion boat
base
elevating lever
pressing plate
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CN2012104771413A
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CN102935392B (en
Inventor
魏建林
张柏松
徐长英
郑福丽
田叶
马征
王学君
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Institute of Agricultural Resources and Environment of Shandong Academy of Agricultural Sciences
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Institute of Agricultural Resources and Environment of Shandong Academy of Agricultural Sciences
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Priority to CN201210477141.3A priority Critical patent/CN102935392B/en
Publication of CN102935392A publication Critical patent/CN102935392A/en
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Publication of CN102935392B publication Critical patent/CN102935392B/en
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Abstract

The invention discloses a horizontally fixing device of a diffusion vessel and a use method of the horizontally fixing device, belonging to the technical field of soil detectors. The horizontally fixing device comprises a base, a supporting rod, a lifting rod and a press plate and is characterized in that the supporting rod is a hollow straight rod, wherein the hollow straight rod is vertically and fixedly arranged on the edge of the base, and the middle upper part of the supporting rod is provided with a fixing screw; the lifting rod is of a right-angle L shape, a vertical part of the lifting rod is inserted into the supporting rod and can move in the supporting rod up and down, and the fixing screw of the supporting rod can be used for fixing the vertical part of the lifting rod; and the end part of a transverse part of the lifting rod is provided with a spring, the lower part of the spring is fixedly connected with the press plate in a horizontal direction, and the press plate is arranged above the base and opposites to the base. The horizontally fixing device of the diffusion plate, disclosed by the invention has the advantages of simple structure, convenience and safety in use and easiness in operation, and solves the technical problem of operation failure because an inside solution and an outside solution are easy to mix when alkali-hydrolysable nitrogen in soil is determined by a diffusion absorption method.

Description

The horizontal fixture of a kind of diffusion boat and using method thereof
Technical field
The present invention relates to the horizontal fixture of a kind of diffusion boat, dependent territory earth checkout gear technical field.
Background technology
The soil alkali-hydrolyzable nitrogen comprises labile, the fairly simple organic nitrogen of appearance in inorganic nitrogen and the part organic matter, and it is the summation of the protein of ammonium nitrogen, nitrate nitrogen, amino acid, acid amides and facile hydrolysis.It can reflect at no distant date nitrogen supply situation of soil, so be called again soil available nitrogen.Measure the content of soil alkali-hydrolyzable nitrogen to understanding the confession nitrogen ability of soil, instruct the rational application of fertilizer to have definite meaning.Therefore the alkali-hydrolyzable nitrogen that how can measure fast and accurately in the soil is problem in the soil and fertilizer research field always.Comparatively commonly used is to adopt the diffusion absorption method at present, normal operation glass diffusion boat, the inside and outside chamber of ware body adds respectively boric acid and soil sample, smear the sealants such as alkaline glycerine at the external edge of ware, the cover plate that frosted glass is made covers and rotates for several times, make ware limit and frosted glass cover plate fully bonding, gradually rotate again and remove the frosted glass cover plate on one side, add alkali lye at the diffusion boat exocoel after exposing a slit, then cover tightly immediately, tight with the rubber band circle again, the frosted glass cover plate is fixed, to guarantee with the diffusion boat sealing fully.Put into subsequently insulating box and placed 24 hours, then take out dismantle rubber band and frosted glass, the boric acid absorption liquid is carried out titration.This assay method result is stable, equipment is simple, but in operating process especially when bundle is torn rubber band open, need to guarantee diffusion boat careful operation on horizontal plane, the careless slightly mixing that just can cause interior exocoel solution, so that operation failure, rework rate is high, and time-consuming.The horizontal fixture of diffusion boat is not also appeared in the newspapers at present.
Summary of the invention
For solving the problems of the technologies described above, for the defective described in the background technology and deficiency, the invention provides the horizontal fixture of a kind of diffusion boat, to realize that the diffusion boat seal process easily and fast, finish safely.
Technical scheme of the present invention is as follows:
The horizontal fixture of a kind of diffusion boat comprises base, support bar, elevating lever and pressing plate, it is characterized in that, support bar is the straight-bar of hollow, is vertically fixed on the base edge, and the support bar middle and upper part is provided with fixed screw; Elevating lever is at right angles L shaped, and the vertical component of elevating lever inserts in the support bar, and can do in support bar and move up and down, and the fixed screw on the support bar can be fixed the vertical component of elevating lever; The end of elevating lever lateral part is provided with spring, and spring lower horizontal direction is fixedly connected with pressing plate, and pressing plate is positioned at base top and relative with base.
The present invention is preferred, and described pressing plate bottom surface is covered with one deck cushion pad, and further preferred, described cushion pad is valve rubber.Cushion pad effectively cushions pressing plate for the pressure of diffusion boat, and guarantee pressing plate to the diffusion boat surface stressed evenly, prevent from damaging diffusion boat.
The present invention is preferred, and the height of described support bar is 0.5~2cm, and the height of the vertical component of elevating lever is less than the height of support bar.
The present invention is preferred, and the width of described pressing plate is greater than mistress's diameter of diffusion boat.
Described base, support bar, elevating lever and pressing plate are metal material or rigid plastics material.
The present invention also provides the using method of the horizontal fixture of a kind of diffusion boat, may further comprise the steps:
(1), will be stamped the diffusion boat that frosted glass cover plate, inside contain testing sample and reagent and place on the base of the horizontal fixture of diffusion boat,
(2), unclamp fixed screw, adjust the elevating lever height, the vertical component of elevating lever is done in support bar and is moved up and down, when pressing plate contacts with the frosted glass cover plate, the fixed screw on the screwed support bar; The elastic force of spring is horizontally fixed on the base frosted glass cover plate and diffusion boat simultaneously,
(3), frosted glass cover plate and the diffusion boat that fixes moved in the insulating box together with the horizontal fixture of diffusion boat, for subsequent use.
The present invention is preferred, and the diffusion boat in the step (1) is the multilayer diffusion boat, and the multilayer diffusion boat is stacked placing on the base up and down.
The invention has the beneficial effects as follows:
1, the present invention is simple in structure, convenient fixing, the frosted glass cover plate can be fixed on the diffusion boat by the up-down adjustment elevating lever and by the elastic force of spring, to guarantee the diffusion boat sealing fully, in fixation procedure, diffusion boat is on the horizontal plane always, prevents the diffusion boat inclination and causes diffusion boat inner room and mistress's solution to mix, solve the interior mistress's solution of alkali-hydrolyzable nitrogen of measuring in the soil with the diffusion absorption method and be easy to mix, caused the technical problem of operation failure.The horizontal fixture of diffusion boat of the present invention is the accuracy rate original text fixedly, safety easy to use, and easily operation is time saving and energy saving, has improved operating efficiency.
2, convenient disassembly of the present invention unclamps fixed screw, and to the adjusted elevating lever, level is taken off diffusion boat and got final product.
3, pressing plate of the present invention bottom surface is covered with one deck cushion pad, and cushion pad effectively cushions pressing plate for the pressure of diffusion boat, and guarantee pressing plate to the diffusion boat surface stressed evenly.
Description of drawings
Fig. 1 is structural representation of the present invention;
Wherein: 1, base, 2, support bar, 3, elevating lever, 4, the elevating lever lateral part, 5, spring, 6, pressing plate, 7, fixed screw, 8, valve rubber.
The specific embodiment
The invention will be further described below in conjunction with drawings and Examples, but be not limited to this.
Embodiment 1:
The horizontal fixture of a kind of diffusion boat, structure comprise base 1, support bar 2 and elevating lever 3 as shown in Figure 1, and support bar 2 is the straight-bar of hollow, are vertically fixed on base 1 edge, and support bar 2 middle and upper parts are provided with fixed screw 7; Elevating lever 3 is at right angles L shaped, and the vertical component of elevating lever 3 inserts in the support bar 2, and can do in support bar 2 and move up and down, and the fixed screw 7 on the support bar 2 can be fixed the vertical component of elevating lever 3; The end of elevating lever lateral part 4 is provided with spring 5, and spring 5 lower horizontal directions are fixedly connected with pressing plate 6, and pressing plate 6 is positioned at base 1 top and relative with base 1.
The bottom surface of pressing plate 6 is covered with one deck valve rubber 8, valve rubber 8 effectively the buffering pressing plates for the pressure of diffusion boat, and guarantee pressing plate to the diffusion boat surface stressed evenly, prevent from damaging diffusion boat.
The height of support bar 2 is 0.5cm, and the height of the vertical component of elevating lever 3 is less than the height of support bar 2.
For making 6 pairs of diffusion boats of pressing plate stressed evenly, the width of pressing plate 6 is greater than mistress's diameter of diffusion boat.
Base 1, support bar 2, elevating lever 3 and pressing plate 6 all adopt metal material.
Embodiment 2:
The horizontal fixture of a kind of diffusion boat as described in Example 1, difference is: the height of support bar 2 is 2cm.
Embodiment 3:
The using method of the horizontal fixture of embodiment 1 described diffusion boat may further comprise the steps:
1, will be stamped the diffusion boat that frosted glass cover plate, inside contain testing sample and reagent and place on the base 1 of the horizontal fixture of diffusion boat,
2, unclamp fixed screw 7, adjust elevating lever 3 height, the vertical component of elevating lever 3 is done in support bar 2 and is moved up and down, when pressing plate 6 contacts with the frosted glass cover plate, and the fixed screw 7 on the screwed support bar 2; The elastic force of spring is horizontally fixed on the base frosted glass cover plate and diffusion boat simultaneously,
3, frosted glass cover plate and the diffusion boat that fixes moved in the insulating box together with the horizontal fixture of diffusion boat, for subsequent use.

Claims (6)

1. the horizontal fixture of diffusion boat comprises base, support bar, elevating lever and pressing plate, it is characterized in that, support bar is the straight-bar of hollow, is vertically fixed on the base edge, and the support bar middle and upper part is provided with fixed screw; Elevating lever is at right angles L shaped, and the vertical component of elevating lever inserts in the support bar, and can do in support bar and move up and down, and the fixed screw on the support bar can be fixed the vertical component of elevating lever; The end of elevating lever lateral part has been provided with spring, and spring lower horizontal direction is fixedly connected with pressing plate, and pressing plate is positioned at base top and relative with base.
2. the horizontal fixture of diffusion boat according to claim 1, it is characterized in that: described pressing plate bottom surface is covered with one deck cushion pad, and further preferred, described cushion pad is valve rubber.
3. the horizontal fixture of diffusion boat according to claim 2, it is characterized in that: the height of described support bar is 0.5~2cm, and the height of the vertical component of elevating lever is less than the height of support bar.
4. the horizontal fixture of diffusion boat according to claim 2, it is characterized in that: the width of described pressing plate is greater than mistress's diameter of diffusion boat.
5. the horizontal fixture of diffusion boat according to claim 2, it is characterized in that: described base, support bar, elevating lever and pressing plate are metal material or rigid plastics material.
6. the using method of the horizontal fixture of diffusion boat as claimed in claim 1 may further comprise the steps:
(1), will be stamped the diffusion boat that frosted glass cover plate, inside contain testing sample and reagent and place on the base of the horizontal fixture of diffusion boat,
(2), unclamp fixed screw, adjust the elevating lever height, the vertical component of elevating lever is done in support bar and is moved up and down, when pressing plate is pressed in the diffusion boat level on the base, fixed screw on the screwed support bar, frosted glass cover plate and diffusion boat are horizontally fixed on the base simultaneously
(3), frosted glass cover plate and the diffusion boat that fixes moved in the insulating box together with the horizontal fixture of diffusion boat, for subsequent use.
CN201210477141.3A 2012-11-21 2012-11-21 Horizontally fixing device of diffusion vessel and use method of horizontally fixing device Expired - Fee Related CN102935392B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109470835A (en) * 2018-10-23 2019-03-15 中国科学院合肥物质科学研究院 A kind of Soil K+adsorption alkali-hydrolyzable nitrogen processing unit
CN112505292A (en) * 2020-11-17 2021-03-16 中国环境科学研究院 Culture device and culture method for nitrogen hydrolysis experiment

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5998202A (en) * 1997-02-26 1999-12-07 Synthecon, Inc. Multiple chamber diffusion vessel
CN201243891Y (en) * 2008-09-02 2009-05-27 周柯秋成 Rack for placing dishware
CN201648393U (en) * 2010-04-14 2010-11-24 张桂玲 Culture dish retainer
CN202533320U (en) * 2012-05-07 2012-11-14 景德镇陶瓷学院 Fixture for ceramic ware

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5998202A (en) * 1997-02-26 1999-12-07 Synthecon, Inc. Multiple chamber diffusion vessel
CN201243891Y (en) * 2008-09-02 2009-05-27 周柯秋成 Rack for placing dishware
CN201648393U (en) * 2010-04-14 2010-11-24 张桂玲 Culture dish retainer
CN202533320U (en) * 2012-05-07 2012-11-14 景德镇陶瓷学院 Fixture for ceramic ware

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109470835A (en) * 2018-10-23 2019-03-15 中国科学院合肥物质科学研究院 A kind of Soil K+adsorption alkali-hydrolyzable nitrogen processing unit
CN112505292A (en) * 2020-11-17 2021-03-16 中国环境科学研究院 Culture device and culture method for nitrogen hydrolysis experiment

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