CN102873774A - Online mortar recovery method in silicon industry - Google Patents

Online mortar recovery method in silicon industry Download PDF

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Publication number
CN102873774A
CN102873774A CN2012101022070A CN201210102207A CN102873774A CN 102873774 A CN102873774 A CN 102873774A CN 2012101022070 A CN2012101022070 A CN 2012101022070A CN 201210102207 A CN201210102207 A CN 201210102207A CN 102873774 A CN102873774 A CN 102873774A
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China
Prior art keywords
mortar
self
knockout drum
mixer pot
motor
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Pending
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CN2012101022070A
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Chinese (zh)
Inventor
胡占林
王学卫
李艳
刘洋
曹永兴
刘锐
刘珺
朱志鹏
靳倞
安万里
张继强
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SHENYANG LINTON PRECISION MACHINE CO Ltd
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SHENYANG LINTON PRECISION MACHINE CO Ltd
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Priority to CN2012101022070A priority Critical patent/CN102873774A/en
Publication of CN102873774A publication Critical patent/CN102873774A/en
Pending legal-status Critical Current

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Abstract

The invention discloses an online mortar recovery method in silicon industry. The online mortar recovery method is mainly characterized in that a solid phase port of a primary separation centrifugal machine is connected with a separating tank, and a self-circulation loop of the separating tank is switched to a recovery cooling liquid adding loop through motor-driven valves. A blending tank forms a self-circulation loop with the motor-driven valves, a pneumatic diaphragm pump, a mass flowmeter and the like. The self-circulation loop of the blending tank and the self-circulation loop of the separating tank share one pneumatic diaphragm pump and one quality flowmeter. Mortar is conveyed into the blending tank after the mortar density reaches a set value and the blending tank sends out a signal allowing mortar loading. Recovery cooling liquid is added into the separating tank after the conveying is finished. The online mortar recovery method has the advantages that by adoption of blending and separating technologies, the use ratio of the primary separation centrifugal machine reaches over 98% and the handling capacity is improved by about one time. Meanwhile, the performance of recycled mortar is well guaranteed and the uniformity degree of matching is improved.

Description

Online mortar recovery method in the silicon industry
Technical field
The present invention relates to online mortar recovery method in the mortar manufacturing technology, particularly a kind of photovoltaic industry in a kind of photovoltaic industry silicon industry.
Background technology
Along with the fast development of national economy, photovoltaic industry emerging rapidly, also gradually forms scale in China as a kind of novel energy industry all over the world.And main material is monocrystalline silicon piece and polysilicon chip in photovoltaic energy.In the production process of monocrystalline silicon piece and polysilicon chip, consume a large amount of mortars by SiC and PEG mediation.And SiC and PEG cost are expensive, and along with the continuous decrease of solar silicon wafers cutting industry profit, silicon chip cutting enterprise need to carry out recycling to mortar.For reducing production costs, reduce waste and old mortar discharging, the demand of mortar recycling has just appearred.
Summary of the invention
The objective of the invention is the deficiency that exists in the above-mentioned technology, online mortar recovery method in a kind of silicon industry is provided.Not only can realize the automatic production operation that mortar reclaims, and done further improvement on the basis of original mortar online recycling, adopt to be in harmonious proportion and the technology of separating, the utilization rate of first separation centrifuge is reached more than 98%, treating capacity has improved nearly one times on original basis.Guaranteed well simultaneously the performance of regeneration mortar, i.e. proportioning and the uniformity.
The object of the present invention is achieved like this, comprises mortar online recycling device in the silicon industry, it is characterized in that, the first separation solid phase falls into knockout drum, and added a certain amount of recovery cooling fluid in the knockout drum before the first separation.In the first separation process, if Mixer pot not in harmonic process, the mortar self-loopa in the knockout drum.Detect slurry density in the self-loopa process, after slurry density reached setting value, this setting value was higher than and is in harmonious proportion the slurry density setting value, and at this moment motor-driven valve switches to the mediation pattern, was added being in harmonious proportion the mortar of aequum in the Mixer pot by knockout drum.From reclaim flow container, add again after having added and reclaim cooling fluid.This moment, Mixer pot entered harmonic process, mortar in the Mixer pot begins self-loopa, in the self-loopa process, detect slurry density, the weight of mortar in the Mixer pot that detects according to the slurry density that detects and weighing device behind the setting-up time, the make new advances required addition of cooling fluid of calculating, and beginning is added new cooling fluid in Mixer pot.Added rear continuation and in mortar self-loopa process, detected slurry density, detect qualified after, add new mortar in the Mixer pot by new mortar jar, add finish after beginning by the mortar can of Mixer pot to finished pot.At this moment motor-driven valve has switched to the self-loopa pattern of knockout drum.
Mortar online recycling device in the silicon industry of the present invention, the anti-locking apparatus of gear pump, weighing device, peristaltic pump, pneumatic diaphragm pump, electric-control system, stirring motor, motor-driven valve, dust arrester, mist collector, mass flowmenter, ultrasonic level gage, pulsation of comprising mortar Mixer pot, knockout drum, flow container, reclaim flow container, head tank, new mortar jar, finished pot, first separation centrifuge, secondary separation centrifuge, suction conveyor, the new cooling fluid of interpolation being used.
The invention has the beneficial effects as follows, adopt to be in harmonious proportion and the technology of separating, the utilization rate of first separation centrifuge is reached more than 98%, and treating capacity has improved nearly one times on original basis.Guarantee well simultaneously the performance of regeneration mortar, improved the uniformity of proportioning.
Description of drawings
Fig. 1 is apparatus structure schematic diagram of the present invention
Fig. 2 is the top view of Fig. 1
Fig. 3 is process chart of the present invention
By Fig. 1-2 as can be known, device of the present invention is by centrifuge feed pump 1, motor-driven valve 2(A), centrifuge 3, motor-driven valve 2(B), motor-driven valve 2(D), a not good liquor fills with 6, draining bucket 7, new mortar jar 8; Motor-driven valve 2(C); New cooling fluid 10, ultrasonic level gage 11; Agitator 12(A); Mist collector 13; Reclaim flow container 14; Knockout drum 15; Weighing device 16; Agitator 12(B); Mixer pot 18; Motor-driven valve 2(E); Pneumatic diaphragm pump 20; Magnetic valve 21; The anti-locking apparatus 22 of pulsation; Mass flowmenter 23; Finished pot 24; Motor-driven valve 2(F) forms.New mortar jar 8, recovery flow container 14, knockout drum 15, Mixer pot 18, not good liquor filling 6 and finished pot 24 are fixed on the underframe by lower margin; Agitator 12A and 12B install respectively in knockout drum and the Mixer pot; Each motor-driven valve 2A, 2B, 2C, 2D, 2E, 2F are installed in separately on the pipeline; Weighing device 16 is installed on the Mixer pot; Mist collector 13 is installed on the pump support; No. one time centrifuge 3 is installed on the side underframe; Mass flowmenter 23 is installed on the flowmeter support; Pneumatic diaphragm pump 20 is installed on the pump support; On new mortar jar, recovery flow container, knockout drum, Mixer pot and the finished pot ultrasonic level gage 11 is installed.
One time flow container 6 is used for depositing the liquid after the centrifuge separation No. one time; Draining bucket 7 is used for the liquid after storage equipment cleans; Magnetic valve 21 is used for the source of the gas of the anti-gentle moving membrane pump of locking apparatus of control pulsation; Ultrasonic level gage 11 is for detection of liquid level in the tank.
As shown in Figure 2, the solid phase mouth of first separation centrifuge is connected in knockout drum, and knockout drum consists of self circular loop by motor-driven valve, pneumatic diaphragm pump, mass flowmenter etc.The self circular loop of knockout drum switches to by motor-driven valve and reclaims cooling fluid interpolation loop.Mixer pot consists of self circular loop by motor-driven valve, pneumatic diaphragm pump, mass flowmenter etc.The self circular loop of Mixer pot and the self circular loop of knockout drum share a pneumatic diaphragm pump and mass flowmenter.Mortar in the knockout drum detects slurry density in the self-loopa process, send allow to load in the backward Mixer pot of mortar signal and transport mortar when slurry density reaches setting value and Mixer pot.Transport to add in the complete backward knockout drum and reclaim cooling fluid.Mortar in the Mixer pot detects slurry density in the self-loopa process, determine to be in harmonious proportion addition with new cooling fluid by the slurry density that detects and mortar weight.
Mortar online recycling operation process is, cleans the place when motor-driven valve 2E switches to, and motor-driven valve 2F switches to Mixer pot circulation place, motor-driven valve 2C switches to the knockout drum place, and motor-driven valve 2B switches to the knockout drum place, at this moment, pneumatic diaphragm pump 20 starts, the recovery cooling fluid of adding in the knockout drum.Add complete motor-driven valve 2E and switch to the flow process place, motor-driven valve 2C switches to the knockout drum place, and at this moment, centrifuge starts, and enters centrifuge feed pump 1 beginning feed after the production status.While pneumatic diaphragm pump startup, the mortar in the knockout drum 15 begins self-loopa, and detects the density of mortar in the knockout drum in the self-loopa process.When the density that detects reached setting value, pneumatic diaphragm pump stopped, and stops rear motor-driven valve 2A and switches to Mixer pot 18 circulations place.After switching put in place, pneumatic diaphragm pump 20 started, and beginning is added mortar by knockout drum in Mixer pot, add complete rear pneumatic diaphragm pump and stop.Pneumatic diaphragm pump stops rear motor-driven valve 2E and switches to clean place, motor-driven valve 2A switches to the knockout drum place, after the motor-driven valve switching puts in place, the pneumatic diaphragm pump startup, beginning is added recovery cooling fluid 14 in knockout drum 15, add complete rear pneumatic diaphragm pump and stop, motor-driven valve 2E switches to the flow process place, knockout drum agitator 12A work.Motor-driven valve 2C switches to Mixer pot 18 places, motor-driven valve 2A switches to the Mixer pot place, after the motor-driven valve switching puts in place, the pneumatic diaphragm pump startup, mortar in the Mixer pot begins self-loopa by agitator 12B, the micro-spray dust that produces enters in the mist collector 13, in the self-loopa process, detect the density of mortar in the Mixer pot, the weighing scale of mortar is calculated to be blended into and is set the required new cooling fluid addition of density in the Mixer pot that electric-control system detects by the density that detects and by weighing device 16 behind the setting-up time, and beginning is added new cooling fluid 10 in Mixer pot.Added the slurry density that detects by the anti-locking apparatus 22 of pulsing, mass flowmenter 23 after the new cooling fluid qualified, beginning is added new mortar in Mixer pot, adding complete rear pneumatic diaphragm pump stops, motor-driven valve 2F switches to regeneration mortar cartage department, switches the rear pneumatic diaphragm pump unlatching beginning that puts in place and carries out can by Mixer pot to finished pot 24.After can finished, pneumatic diaphragm pump stopped, and motor-driven valve 2C switches to the knockout drum place, motor-driven valve 2F switches to Mixer pot circulation place, and motor-driven valve 2A switches to knockout drum 15 places, switches the rear pneumatic diaphragm pump that puts in place and opens, mortar begins self-loopa in the knockout drum, detects the density of mortar in the self-loopa process.

Claims (6)

1. online mortar recovery method in the silicon industry, comprise mortar online recycling device in the silicon industry, it is characterized in that, the first separation solid phase falls into knockout drum, added a certain amount of recovery cooling fluid in the knockout drum before the first separation, in the first separation process, Mixer pot is not in harmonic process, mortar self-loopa in the knockout drum, in the self-loopa process, detect slurry density, after slurry density reaches setting value, this setting value is higher than mediation slurry density setting value, at this moment electronic valve actuation valve switches to the mediation pattern, added in the Mixer pot by knockout drum and to be in harmonious proportion the mortar of aequum, from reclaim flow container, add again after having added and reclaim cooling fluid, this moment, Mixer pot entered harmonic process, mortar in the Mixer pot begins self-loopa, in the self-loopa process, detect slurry density, the weight of mortar in the Mixer pot that detects according to the slurry density that detects and weighing device behind the setting-up time, the make new advances required addition of cooling fluid of calculating, and beginning is added new cooling fluid in Mixer pot, add rear continuation and in mortar self-loopa process, detected slurry density, detect qualified after, in Mixer pot, add new mortar by new mortar jar, beginning was by the mortar can of Mixer pot to finished pot after interpolation was finished, and at this moment motor-driven valve has switched to the self-loopa pattern of knockout drum.
2. a device of implementing the method for claim 1 is, the anti-locking apparatus of gear pump, weighing device, peristaltic pump, pneumatic diaphragm pump, electric-control system, stirring motor, motor-driven valve, dust arrester, mist collector, mass flowmenter, ultrasonic level gage, pulsation of comprising mortar Mixer pot, knockout drum, flow container, reclaim flow container, head tank, new mortar jar, finished pot, first separation centrifuge, secondary separation centrifuge, suction conveyor, the new cooling fluid of interpolation being used; It is characterized in that, new mortar jar (8), recovery flow container (14), knockout drum (15), Mixer pot (18), not good liquor filling (6) and finished pot (24) are fixed on the underframe by lower margin; Agitator (12A) and (12B) install respectively in knockout drum and the Mixer pot; Each motor-driven valve (2A), (2B), (2C), (2D), (2E), (2F) are installed in separately on the pipeline; Weighing device (16) is installed on the Mixer pot; Mist collector (13) is installed on the pump support; A centrifuge (3) is installed on the side underframe; Mass flowmenter (23) is installed on the flowmeter support; Pneumatic diaphragm pump (20) is installed on the pump support; On new mortar jar, recovery flow container, knockout drum, Mixer pot and the finished pot ultrasonic level gage (11) is installed.
3. online mortar recovery method in a kind of silicon industry according to claim 1, it is characterized in that: the solid phase mouth of first separation centrifuge is connected in knockout drum, knockout drum consists of self circular loop by motor-driven valve, pneumatic diaphragm pump, mass flowmenter etc., and the self circular loop of knockout drum switches to by motor-driven valve and reclaims cooling fluid interpolation loop.
4. online mortar recovery method in a kind of silicon industry according to claim 1, it is characterized in that: Mixer pot consists of self circular loop by motor-driven valve, pneumatic diaphragm pump, mass flowmenter etc., and the self circular loop of Mixer pot and the self circular loop of knockout drum share a pneumatic diaphragm pump and mass flowmenter.
5. online mortar recovery method in a kind of silicon industry according to claim 1, it is characterized in that: the mortar in the knockout drum detects slurry density in the self-loopa process, send allow to load in the backward Mixer pot of mortar signal and transport mortar when slurry density reaches setting value and Mixer pot, transport to add in the complete backward knockout drum and reclaim cooling fluid.
6. online mortar recovery method in a kind of silicon industry according to claim 1, it is characterized in that: the mortar in the Mixer pot detects slurry density in the self-loopa process, determines to be in harmonious proportion addition with new cooling fluid by the slurry density that detects and mortar weight.
CN2012101022070A 2012-04-10 2012-04-10 Online mortar recovery method in silicon industry Pending CN102873774A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103273577A (en) * 2013-06-04 2013-09-04 台州市双辉机械设备有限公司 Circulating cooling device of multi-wire cutting machine and control method of circulating cooling device
CN103934910A (en) * 2014-05-08 2014-07-23 常州有则科技有限公司 Heat cycle mortar online recycling machine
CN106378876A (en) * 2016-09-23 2017-02-08 镇江环太硅科技有限公司 Diamond wire slicing cooling liquid integrated treatment method for sapphire and silicon wafers
CN109809670A (en) * 2019-04-09 2019-05-28 兰州天昊环保工程有限公司 A kind of drying device of power plant desulfurization denitration wastewater sludge
CN115404120A (en) * 2022-08-26 2022-11-29 江阴东为资源再生技术有限公司 Mortar recovery method, system, electronic device and storage medium

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202006519U (en) * 2011-01-17 2011-10-12 西安华晶电子技术股份有限公司 Mortar circulating and supplying system of multi-wire saw
CN102281991A (en) * 2009-01-15 2011-12-14 株式会社安永 Slurry regenerating device and method
CN202089492U (en) * 2011-06-02 2011-12-28 沈阳微研精密机器有限公司 Weighing module distribution structure of mortar recovery equipment

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102281991A (en) * 2009-01-15 2011-12-14 株式会社安永 Slurry regenerating device and method
CN202006519U (en) * 2011-01-17 2011-10-12 西安华晶电子技术股份有限公司 Mortar circulating and supplying system of multi-wire saw
CN202089492U (en) * 2011-06-02 2011-12-28 沈阳微研精密机器有限公司 Weighing module distribution structure of mortar recovery equipment

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103273577A (en) * 2013-06-04 2013-09-04 台州市双辉机械设备有限公司 Circulating cooling device of multi-wire cutting machine and control method of circulating cooling device
CN103273577B (en) * 2013-06-04 2015-11-18 台州市双辉机械设备有限公司 A kind of cooling back installation of multi-line cutting machine and control method thereof
CN103934910A (en) * 2014-05-08 2014-07-23 常州有则科技有限公司 Heat cycle mortar online recycling machine
CN103934910B (en) * 2014-05-08 2015-11-04 常州有则科技有限公司 Thermal cycle mortar online recycling machine
CN106378876A (en) * 2016-09-23 2017-02-08 镇江环太硅科技有限公司 Diamond wire slicing cooling liquid integrated treatment method for sapphire and silicon wafers
CN106378876B (en) * 2016-09-23 2019-02-05 镇江环太硅科技有限公司 A kind of sapphire and silicon wafer are sliced coolant liquid integrated sewage treatment method with diamond wire
CN109809670A (en) * 2019-04-09 2019-05-28 兰州天昊环保工程有限公司 A kind of drying device of power plant desulfurization denitration wastewater sludge
CN115404120A (en) * 2022-08-26 2022-11-29 江阴东为资源再生技术有限公司 Mortar recovery method, system, electronic device and storage medium

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Application publication date: 20130116