CN102863904A - Moldproof softening and brightening agent for cleaning leather and preparation method thereof - Google Patents
Moldproof softening and brightening agent for cleaning leather and preparation method thereof Download PDFInfo
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- CN102863904A CN102863904A CN2012103446373A CN201210344637A CN102863904A CN 102863904 A CN102863904 A CN 102863904A CN 2012103446373 A CN2012103446373 A CN 2012103446373A CN 201210344637 A CN201210344637 A CN 201210344637A CN 102863904 A CN102863904 A CN 102863904A
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Abstract
The invention discloses a moldproof softening and brightening agent for cleaning leather and a preparation method thereof. The moldproof softening and brightening agent for cleaning leather is prepared from surfactant, brightener, oleic acid, animal fat leather greasing agent, fluorosilicon oil, triethanolamine, mold preventive, essence and deionized water in certain mass ratio. The preparation method comprises the following steps: preparing raw materials, mixing oil phases, mixing water phases, mixing oil and water, and filtering and filling. Due to the addition of the fluorosilicon oil and multiple assistants, the moldproof softening and brightening agent for cleaning leather has favorable effects on cleaning and nourishing leather, can endow the leather with the characteristics of smoothness, softness, water resistance, wear resistance, mold resistance and the like.
Description
Technical field
The present invention relates to household chemicals field, be specifically related to gentle bright dose of a kind of leather cleaning mildew-resistant and preparation method thereof.
Background technology
Along with improving constantly of living standards of the people, people require also to improve constantly to the nursing efficacy of leatherware (leather shoes, suitcase, leather sofa), and this just requires to improve the beauty decoration comprehensive function of leather.Leather care products is main raw material mainly with wax, solvent, dyestuff on the market now, add again that some help to clean, the auxiliary agent of glazing etc., leather is prone to the embrittlement that hardens behind this nursing agent life-time service, and the catabiosis such as dry and cracked broken skin are not ideal to the nourishing effect of leather.In addition, both at home and abroad the trend at the covering with paint glazing of leather is the disposable improvement of finishing cleaning and the mildew-resistant effect of leather, and give simultaneously that leather is smooth, soft, waterproof, the characteristics such as wear-resisting.Most product efficacy on the market are more single, do not reach above-mentioned composite effect.Therefore, be necessary leather cleaning nursing agent of the prior art is filled a prescription and the improvement of related production technique.
Summary of the invention
The object of the invention is to overcome the defective that exists in the prior art, design a kind of leather cleaning nourish effective, can give that leather is smooth, soft, gentle bright dose of the leather cleaning mildew-resistant of the characteristics such as waterproof, wear-resisting, mildew-resistant, another object of the present invention is to design soften bright dose preparation method of a kind of leather cleaning mildew-resistant.
For achieving the above object, technical scheme of the present invention provides gentle bright dose of a kind of leather cleaning mildew-resistant, it is characterized in that, the composition that described leather cleaning mildew-resistant is gentle bright dose and the weight percent of component are:
Tensio-active agent 1 ~ 15%
Brightening agent 2 ~ 12%
Oleic acid 1 ~ 2%
Animal tallow leather fat 2.5 ~ 15%
Fluorine containing silicone oil 2 ~ 5%
Trolamine 0.5% ~ 2.0%
Mould inhibitor 0.05 ~ 0.3%
Essence 0 ~ 0.3%
The deionized water surplus
The weight percent sum of each component is 100%, and described tensio-active agent is the combination of nonionogenic tenside, cats product and anion surfactant.
Wherein, the weight percent of nonionogenic tenside is 0.5 ~ 10% in gentle bright dose of the described leather cleaning mildew-resistant, and the weight percent of cats product is 1 ~ 5% in gentle bright dose of the described leather cleaning mildew-resistant.
Preferably, described nonionogenic tenside is selected from a kind of in alkylphenol polyoxyethylene, fatty alcohol-polyoxyethylene ether and the sorbitan fatty acid ester, and described cats product is long-chain monoalkyl quaternary ammonium salt cationic surfactant.
Wherein, described brightening agent is selected from least a in E wax, carnauba wax and the beeswax.
Preferably, described brightening agent comprises E wax, carnauba wax and beeswax, the weight percent of E wax is 1 ~ 5% in gentle bright dose of the described leather cleaning mildew-resistant, and the weight percent of carnauba wax is 1 ~ 3% in gentle bright dose of the described leather cleaning mildew-resistant, and the beeswax weight percent is 1 ~ 4%.。
Wherein, described animal tallow leather fat comprises lanolin and dark seal oil, and the weight percent of lanolin is 2 ~ 5% in gentle bright dose of the described leather cleaning mildew-resistant, and the gentle bright dose of mesopelagic leopard Weight ratio of oil of described leather cleaning mildew-resistant is 0.5 ~ 10%.
Wherein, described mould inhibitor is selected from least a in BIT and the nano phase ag_2 o leather fungicide.
Technical scheme of the present invention also provides the preparation method of gentle bright dose of a kind of leather cleaning mildew-resistant, it is characterized in that described preparation method is:
S1: according to the configuration of the weight percent described in the claim 1 raw material;
S2: fat-soluble ingredient, brightening agent, oleic acid, animal tallow leather fat, fluorine containing silicone oil in the tensio-active agent are joined the oil phase pot, be warming up to 90 ~ 93 ℃, stirred under this temperature 10 ~ 15 minutes, raw material evenly obtains oil mixture after the fusing;
S3: deionized water is joined in the water pot, be warming up to 90 ~ 93 ℃, add water soluble ingredient and trolamine in the tensio-active agent, stirred 10 ~ 15 minutes, obtain aqueous mixture after the dissolving evenly;
S4: gained aqueous mixture among the S3 is joined in the emulsification pot, start stirring, then the oil mixture with gained among the S2 joins in the emulsification pot, and homogenizing emulsifying is cooled to 40 ~ 43 ℃ after 30 ~ 40 minutes, add mould inhibitor and essence, restir left standstill after 10 ~ 15 minutes;
S5: the product of gained among the S4 is filled in the packaging vessel.
Wherein, the speed that stirs among the described S4 is 70 ~ 90r/min.
Advantage of the present invention and beneficial effect are: added fluorine containing silicone oil in this invention prescription, contained active group wherein, can interact between the molecule, simultaneously can with leather surface on amino, the carboxyl isopolarity radical reaction of collagen, produce great bounding force and can form one deck organosilicone elastic film at leather surface, this tunic can make leather smooth, and soft feel(ing) strengthens, waterproof antiwear;
The glazing of brightening agent has persistence, with the wetting action of fluorine containing silicone oil mixing and emulsifying and tensio-active agent, and the glazing better effects if;
In inventing prescription, add lanolin and dark seal oil, utilize the animal grease reinforcement of pure natural to the nourishing effect of leather, the nano phase ag_2 o mould inhibitor can significantly improve the anti-mold effect of leather, thereby makes gentle bright dose of this leather cleaning mildew-resistant reach the MULTIPLE COMPOSITE effect.
Embodiment
Below in conjunction with embodiment, the specific embodiment of the present invention is further described.Following examples only are used for technical scheme of the present invention more clearly is described, and can not limit protection scope of the present invention with this.
Embodiment 1
The composition of gentle bright dose of leather cleaning mildew-resistant and the weight percent of component are among the embodiment 1:
Fatty alcohol-polyoxyethylene ether 5%
Palmityl trimethyl ammonium chloride 2%
E wax 3%
Carnauba wax 2%
Oleic acid 1.5%
Lanolin 3.5%
Dark seal oil 6%
Fluorine containing silicone oil 4%
Trolamine 1.5%
Nano phase ag_2 o leather fungicide 0.1%
BIT 0.05%
Essence 0.15%
The deionized water surplus
The weight percent sum of each component is 100%.
The preparation method that the leather cleaning mildew-resistant is gentle bright dose is:
S1: according to above-mentioned weight percent configuration raw material;
S2: fatty alcohol-polyoxyethylene ether, E wax, carnauba wax, oleic acid, lanolin, dark seal oil, fluorine containing silicone oil are joined the oil phase pot, be warming up to 90 ℃, stirred 10 minutes under this temperature, raw material evenly obtains oil mixture after the fusing;
S3: deionized water is joined in the water pot, be warming up to 90 ℃, add palmityl trimethyl ammonium chloride and trolamine, stirred 10 minutes, obtain aqueous mixture after the dissolving evenly;
S4: gained aqueous mixture among the S3 is joined in the emulsification pot, start stirring, then the oil mixture with gained among the S2 joins in the emulsification pot, homogenizing emulsifying is cooled to 40 ℃ after 30 minutes, add nano phase ag_2 o leather fungicide, 1,2-benzisothiazole-3-ketone and essence, restir left standstill after 10 minutes;
S5: the product of gained among the S4 is filled in the packaging vessel.
Wherein, the speed that stirs among the S4 is 70r/min.
Embodiment 2:
The composition of gentle bright dose of leather cleaning mildew-resistant and the weight percent of component are among the embodiment 2:
Sorbitan fatty acid ester 3%
Octadecyl trimethyl ammonium chloride 3%
E wax 4%
Carnauba wax 1%
Oleic acid 1%
Lanolin 2%
Dark seal oil 10%
Fluorine containing silicone oil 2.5%
Trolamine 1%
Nano phase ag_2 o leather fungicide 0.05%
BIT 0.1%
Essence 0.3%
The deionized water surplus
The weight percent sum of each component is 100%.
The preparation method that the leather cleaning mildew-resistant is gentle bright dose is:
S1: according to above-mentioned weight percent configuration raw material;
S2: sorbitan fatty acid ester, E wax, carnauba wax, oleic acid, lanolin, dark seal oil, fluorine containing silicone oil are joined the oil phase pot, be warming up to 95 ℃, stirred 15 minutes under this temperature, raw material evenly obtains oil mixture after the fusing;
S3: deionized water is joined in the water pot, be warming up to 95 ℃, add octadecyl trimethyl ammonium chloride and trolamine, stirred 15 minutes, obtain aqueous mixture after the dissolving evenly;
S4: gained aqueous mixture among the S3 is joined in the emulsification pot, start stirring, then the oil mixture with gained among the S2 joins in the emulsification pot, homogenizing emulsifying is cooled to 45 ℃ after 35 minutes, add nano phase ag_2 o leather fungicide, 1,2-benzisothiazole-3-ketone and essence, restir left standstill after 15 minutes;
S5: the product of gained among the S4 is filled in the packaging vessel.
Wherein, the speed that stirs among the S4 is 80r/min.
Embodiment 3:
The composition of gentle bright dose of leather cleaning mildew-resistant and the weight percent of component are among the embodiment 3:
Alkylphenol polyoxyethylene 6%
Palmityl trimethyl ammonium chloride 4%
Beeswax 5%
Carnauba wax 3%
Oleic acid 2%
Lanolin 5%
Dark seal oil 4.5%
Fluorine containing silicone oil 5%
Trolamine 2%
Nano phase ag_2 o leather fungicide 0.2%
BIT 0.1%
Essence 0.25%
The deionized water surplus
The weight percent sum of each component is 100%.
The preparation method that the leather cleaning mildew-resistant is gentle bright dose is:
S1: according to above-mentioned weight percent configuration raw material;
S2: alkylphenol polyoxyethylene, beeswax, carnauba wax, oleic acid, lanolin, dark seal oil, fluorine containing silicone oil are joined the oil phase pot, be warming up to 93 ℃, stirred 10 minutes under this temperature, raw material evenly obtains oil mixture after the fusing;
S3: deionized water is joined in the water pot, be warming up to 93 ℃, add palmityl trimethyl ammonium chloride and trolamine, stirred 10 minutes, obtain aqueous mixture after the dissolving evenly;
S4: gained aqueous mixture among the S3 is joined in the emulsification pot, start stirring, then the oil mixture with gained among the S2 joins in the emulsification pot, homogenizing emulsifying is cooled to 42 ℃ after 40 minutes, add nano phase ag_2 o leather fungicide, 1,2-benzisothiazole-3-ketone and essence, restir left standstill after 10 minutes;
S5: the product of gained among the S4 is filled in the packaging vessel.
Wherein, the speed that stirs among the S4 is 90r/min.
Above-mentioned three embodiment gained leather cleaning mildew-resistant soften bright dose and are white or light yellow look emulsion liquid, and pH value is 6.0 ~ 9.0; Its cold-resistant stability is put 24h in the refrigerator of (5 ± 2 ℃), recover room temperature and observe, and not oily water separation can normally be used; Heat-resistant stability is placed 24h in the refrigerator of (40 ± 2 ℃), observe not oily water separation; Gloss increased value: 〉=10 gloss unit; Flexibility test 〉=0.1mm(experimental temperature: 23 ± 2 ℃, relative humidity 60 ± 5%, experimental subjects are that diameter is the test wrapper of 35mm); Non-volatile content (%) 〉=6; Anti-mold effect: 1 grade; On leather surface affect leather surface without wrinkle, aliquation expands and obviously fades.
The above only is preferred implementation of the present invention; should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (9)
1. a leather cleaning mildew-resistant softens bright dose, it is characterized in that the composition that described leather cleaning mildew-resistant is gentle bright dose and the weight percent of component are:
Tensio-active agent 1 ~ 15%
Brightening agent 2 ~ 12%
Oleic acid 1 ~ 2%
Animal tallow leather fat 2.5 ~ 15%
Fluorine containing silicone oil 2 ~ 5%
Trolamine 0.5% ~ 2.0%
Mould inhibitor 0.05 ~ 0.3%
Essence 0 ~ 0.3%
The deionized water surplus
The weight percent sum of each component is 100%, and described tensio-active agent is nonionogenic tenside and cats product combination.
2. the leather cleaning mildew-resistant described in according to claim 1 is gentle bright dose, it is characterized in that, the weight percent of nonionogenic tenside is 0.5 ~ 10% in gentle bright dose of the described leather cleaning mildew-resistant, and the weight percent of cats product is 1 ~ 5% in gentle bright dose of the described leather cleaning mildew-resistant.
3. the leather cleaning mildew-resistant described in according to claim 2 is gentle bright dose, it is characterized in that, described nonionogenic tenside is selected from a kind of in alkylphenol polyoxyethylene, fatty alcohol-polyoxyethylene ether and the sorbitan fatty acid ester, and described cats product is long-chain monoalkyl quaternary ammonium salt cationic surfactant.
4. the leather cleaning mildew-resistant described in according to claim 1 is gentle bright dose, it is characterized in that, described brightening agent is selected from least a in E wax, carnauba wax and the beeswax.
5. leather cleaning mildew-resistant according to claim 4 is gentle bright dose, it is characterized in that, described brightening agent comprises E wax, carnauba wax and beeswax, the weight percent of E wax is 1 ~ 5% in gentle bright dose of the described leather cleaning mildew-resistant, the weight percent of carnauba wax is 1 ~ 3% in gentle bright dose of the described leather cleaning mildew-resistant, and the beeswax weight percent is 1 ~ 4%.
6. leather cleaning mildew-resistant according to claim 1 is gentle bright dose, it is characterized in that, described animal tallow leather fat comprises lanolin and dark seal oil, the weight percent of lanolin is 2 ~ 5% in gentle bright dose of the described leather cleaning mildew-resistant, and the gentle bright dose of mesopelagic leopard Weight ratio of oil of described leather cleaning mildew-resistant is 0.5 ~ 10%.
7. leather cleaning mildew-resistant according to claim 1 is gentle bright dose, it is characterized in that, described mould inhibitor is selected from least a in BIT and the nano phase ag_2 o leather fungicide.
8. the preparation method of gentle bright dose of a leather cleaning mildew-resistant is characterized in that described preparation method is:
S1: according to the configuration of the weight percent described in the claim 1 raw material;
S2: fat-soluble ingredient, brightening agent, oleic acid, animal tallow leather fat, fluorine containing silicone oil in the tensio-active agent are joined the oil phase pot, be warming up to 90 ~ 93 ℃, stirred under this temperature 10 ~ 15 minutes, raw material evenly obtains oil mixture after the fusing;
S3: deionized water is joined in the water pot, be warming up to 90 ~ 93 ℃, add water soluble ingredient and trolamine in the tensio-active agent, stirred 10 ~ 15 minutes, obtain aqueous mixture after the dissolving evenly;
S4: gained aqueous mixture among the S3 is joined in the emulsification pot, start stirring, then the oil mixture with gained among the S2 joins in the emulsification pot, and homogenizing emulsifying is cooled to 40 ~ 43 ℃ after 30 ~ 40 minutes, add mould inhibitor and essence, restir left standstill after 10 ~ 15 minutes;
S5: the product of gained among the S4 is filled in the packaging vessel.
9. the preparation method of gentle bright dose of the leather cleaning mildew-resistant of smell gentleness according to claim 8 is characterized in that the speed that stirs among the described S4 is 70 ~ 90r/min.
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Cited By (11)
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| CN103666281A (en) * | 2013-11-22 | 2014-03-26 | 南通信一服饰有限公司 | Stain removal and leather softening shoe polish |
| CN103992744A (en) * | 2013-02-18 | 2014-08-20 | 刘祖学 | Efficient shoe polish |
| CN104878136A (en) * | 2015-05-20 | 2015-09-02 | 周淑华 | Leather maintenance agent and preparation method thereof |
| CN104878131A (en) * | 2015-05-20 | 2015-09-02 | 周淑华 | Genuine leather care agent and preparation method thereof |
| CN105419646A (en) * | 2015-12-03 | 2016-03-23 | 傅家兴 | Leather brightener |
| CN105543428A (en) * | 2016-03-04 | 2016-05-04 | 梁宁宁 | Leather care agent and preparation method thereof |
| CN106676212A (en) * | 2017-02-13 | 2017-05-17 | 东莞市隆威实业有限公司 | Composite used for leather product maintenance and leather product maintenance wet tissue |
| CN107603493A (en) * | 2017-08-31 | 2018-01-19 | 兰溪市拜瑞珂科技服务有限公司 | A kind of fungi-proofing light maintaining agent of fur clothing and preparation method thereof |
| CN107996568A (en) * | 2017-11-16 | 2018-05-08 | 浙江通天星集团股份有限公司 | The production method of environmental-friendly leather mould inhibitor |
| CN109266793A (en) * | 2018-09-14 | 2019-01-25 | 广州市佐力新材料科技有限公司 | A kind of nano leather nourishing essence cream and preparation method thereof |
| CN110684603A (en) * | 2019-09-26 | 2020-01-14 | 广东中联邦精细化工有限公司 | Leather cleaning agent and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103992744A (en) * | 2013-02-18 | 2014-08-20 | 刘祖学 | Efficient shoe polish |
| CN103666281A (en) * | 2013-11-22 | 2014-03-26 | 南通信一服饰有限公司 | Stain removal and leather softening shoe polish |
| CN104878136A (en) * | 2015-05-20 | 2015-09-02 | 周淑华 | Leather maintenance agent and preparation method thereof |
| CN104878131A (en) * | 2015-05-20 | 2015-09-02 | 周淑华 | Genuine leather care agent and preparation method thereof |
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| CN105543428A (en) * | 2016-03-04 | 2016-05-04 | 梁宁宁 | Leather care agent and preparation method thereof |
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| CN107603493A (en) * | 2017-08-31 | 2018-01-19 | 兰溪市拜瑞珂科技服务有限公司 | A kind of fungi-proofing light maintaining agent of fur clothing and preparation method thereof |
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| CN109266793A (en) * | 2018-09-14 | 2019-01-25 | 广州市佐力新材料科技有限公司 | A kind of nano leather nourishing essence cream and preparation method thereof |
| CN110684603A (en) * | 2019-09-26 | 2020-01-14 | 广东中联邦精细化工有限公司 | Leather cleaning agent and preparation method thereof |
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