CN102846497B - Mineral mud washing facial mask - Google Patents

Mineral mud washing facial mask Download PDF

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CN102846497B
CN102846497B CN 201210383655 CN201210383655A CN102846497B CN 102846497 B CN102846497 B CN 102846497B CN 201210383655 CN201210383655 CN 201210383655 CN 201210383655 A CN201210383655 A CN 201210383655A CN 102846497 B CN102846497 B CN 102846497B
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mineral
slurry
mud
water
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CN102846497A (en
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戴跃锋
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HUNAN YUJIA COSMETICS MANUFACTURING CO., LTD.
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HUNAN YUNIFANG BIOLOGICAL TECHNOLOGY Co Ltd
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Abstract

The invention belongs to the field of facial masks and particularly provides a mineral mud washing facial mask which comprises the following components in parts by weight: 20-80 parts of mineral mud, 5-60 parts of mineral mud essence water, 10-40 parts of deionized water, 1-20 parts of humectant, 0.5-5 parts of thickening emulsifier and 0.1-1 part of anticorrosive. The facial mask takes mineral mud as a main raw material and can be used for deeply cleaning, shrinking pores and balancing oil production; and by utilizing the facial mask, natural mineral substances can be used for nourishing and activating skins, and strengthening the skin elasticity.

Description

A kind of slurry of mineral washing facial film
Technical field
The invention belongs to the facial film field, specifically provide a kind of have preserve moisture, the slurry of mineral of Bearberry Extract washing facial film.
Background technology
At cosmetic mask product apoplexy due to endogenous wind, subsides formula facial film is arranged, film forming facial film, powder facial film, Gypsum Fibrosum facial film, mud mask etc.Common mud mask is in that to smear ductility relatively poor, the conventional mud face pack prescription is to utilize dry volcanic mud or Kaolin to utilize deionized water to reconcile into the paste product, on smearing property, mildness and the energy consumption in production technology and the production technology many bottlenecks are arranged, can occur in the prescription stirring inhomogeneous fine particulate material, the mastic of product is adjusted dispensing viscosity by thickened systems.
Summary of the invention
At the deficiencies in the prior art, the present invention aims to provide a kind of slurry of mineral washing facial film, is main material with the slurry of mineral, and this facial film can be received fine, soft fur hole Bergamot Mint Extract by deep layer cleaning; Natural mineral matter nutrition skin-active strengthens skin elasticity, strengthens the natural defence capability of skin.
For achieving the above object, technical scheme of the present invention is:
A kind of slurry of mineral is washed facial film, comprises the composition of following weight portion:
20 parts-80 parts of slurry of minerals
5 parts-60 parts in slurry of mineral elite water
10 parts-40 parts of deionized waters
1 part-20 parts of wetting agents
0.5 part-5 parts of thickener/emulsifiers
0.1 part-1 part of antiseptic;
Wherein, the preparation method of described slurry of mineral and slurry of mineral elite water is: the stone gallbladder between the granite of gathering with beachhead town under the snowy peak mountain range, Longhui County, Hunan Province is raw material, and concrete steps are:
(1) air slaking: be that 10 ℃-40 ℃, humidity are air slaking 30-45 days under the environment of 10%-50% in temperature with the stone gallbladder;
(2) pre-soaking: the stone gallbladder after the air slaking is soaked in water 5 ℃-40 ℃ of soaking temperatures, soak time 25 minutes-35 minutes;
(3) physics is rough: the stone gallbladder after will soaking is beaten, and gets particle diameter<1000 purpose stone gallbladder powder ends;
(4) adding water mixes: with the end washing of above-mentioned stone gallbladder powder, add then water stir mixture; Washing temperature is 5 ℃-40 ℃, and water consumption is 3-4 times of stone gallbladder granular mass; Described mixture leaves standstill the back layering, removes mud and the impurity of bottom, keeps the troubled liquor that the middle part contains mud in suspension;
(5) just heavy: as described troubled liquor to be precipitated 30-40 days, control 5 ℃-40 ℃ of precipitation temperatures simultaneously; The layering of described troubled liquor post precipitation, the water a that separates the upper strata is standby, makes solid content>45% of the mud phase a of lower floor, gets mud one time;
(6) two is heavy: a described mud is precipitated 15-30 days again, and 5 ℃-40 ℃ of control precipitation temperatures, a described mud post precipitation layering again, the water b that separates the upper strata is standby, makes solid content>60% of the mud phase b of lower floor, gets secondary mud;
(7) dry: be 40 ℃-60 ℃ with described secondary mud in temperature, dried 10-15 days under the environment of humidity<50%, make mud solid content>80%, must dry mud;
(8) mud ageing: be 5 ℃-40 ℃ with the described mud that dries in temperature, ageing got slurry of mineral more than 30 days under the environment of humidity<50%;
(9) elite water ageing: merging described water a and water b is 5 ℃-40 ℃ in temperature, and ageing got mineral elite water more than 30 days under the environment of humidity<50%.
Described wetting agent is preferably selected from butanediol or propylene glycol.
Described thickener/emulsifier is preferably selected from 2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers or polyacrylamide/C 13-C 14Isoparaffin/laureth-7.
Described antiseptic is preferably selected from phenoxyethanol/ethylhexyl glycerol or imidazolidinyl urea.
Preferably in described slurry of mineral washing facial film, add 1-20 part functional additive.Described functional additive is preferably left-handed VC.
Water of the present invention can adopt the natural selenium-rich spring water of Longhui Xuefeng Shan Mountain.
The preparation method of described slurry of mineral washing facial film by described proportioning, is added in slurry of mineral, slurry of mineral elite water among the primary response pot A, and the control temperature is 75 ℃-85 ℃, stirs 50 min-60min; Deionized water is heated to 70 ℃-80 ℃ in prewired pot B, adds wetting agent and thickener/emulsifier then successively, stir; Again the material among the prewired pot B is transferred among the primary response pot A, washes prewired pot B with deionized water, and deionized water is transferred among the primary response pot A, continue to stir 55 min-65min; Cool to 45 ℃-50 ℃ again, add functional additive and antiseptic then, stir 25 min-35min, cooling discharging gets slurry of mineral washing facial film.
Compared with prior art, advantage of the present invention is:
1, uses beachhead slurry of mineral and mineral elite water in the prescription of the present invention, because the independent body of raw material and pure manual preparation technology, allowing the trace element of slurry of mineral and mineral elite water be in free state is present in the prescription, more useful effect can help the skin deep layer cleaning, easily adsorb unnecessary oils and fats and blackhead in skin, and remarkable efficient conditioning balance skin profit is secreted, the convergence pore, improve greasy skin matter, make skin fine and smooth saturating clean, salubrious smooth saturating.
2, needn't be become the technology of mastic by solid material in the course of processing, reduce energy consumption and running cost, the mastic quality of its prepared is gentle fine and smooth, and various effective ingredient can be dissolved in the prescription fast, and finished product is easy to smear.
The specific embodiment
Below in conjunction with the specific embodiment, the present invention will be further explained and invention, but the present invention is not limited to the described scope of embodiment.
Embodiment 1:The preparation of slurry of mineral and mineral elite water
The preparation method of a kind of slurry of mineral and mineral elite water is raw material with the stone gallbladder between the granite of beachhead town collection under the snowy peak mountain range, Longhui, comprises following concrete steps:
(1) air slaking: 30 ℃ of temperature, humidity is air slaking 40 days under 45% the environment with the stone gallbladder;
(2) pre-soaking: the stone gallbladder after the air slaking is soaked in water 30 ℃ of soaking temperatures, soak time 30 minutes;
(3) physics is rough: manual the beating 500 times of mallet that stone gallbladder after will soaking tree core is done makes particle diameter 400 orders-900 purpose stone gallbladder powder end;
(4) adding water mixes: with the end washing of above-mentioned stone gallbladder powder, add then water stir mixture; Washing temperature is 30 ℃, and water consumption is 3 times of stone gallbladder granule; Described mixture leaves standstill the back layering, removes mud and the impurity of bottom, keeps the troubled liquor that the middle part contains mud in suspension;
(5) just heavy: described troubled liquor is precipitated 35 days, 25 ℃ of control mud temperature, the layering of described troubled liquor post precipitation, the water a that separates the upper strata is standby, makes solid content>45% of the mud phase a of lower floor, gets mud one time;
(6) two is heavy: a described mud is precipitated 25 days again, and 30 ℃ of control mud temperature, the layering of described troubled liquor post precipitation, the water b that separates the upper strata is standby, makes solid content>60% of the mud phase b of lower floor, gets secondary mud;
(7) dry: with the temperature of described secondary mud at 45 ℃, dried under the environment of humidity<50% 10 days, make and to dry mud by mud solid content>80%;
(8) mud ageing: under 35 ℃ temperature, and ageing got slurry of mineral more than 30 days under the environment of humidity<50% with the described mud that dries;
(9) elite water ageing: merge described water a and water b under 30 ℃ temperature, and ageing 30 days under the environment of humidity<50%, get mineral elite water.
The pH value 7.1-7.3 of slurry of mineral and mineral elite water satisfies the cosmetic material demand.
Embodiment 2: the preparation of slurry of mineral washing facial film
The prescription of this slurry of mineral washing facial film is: according to listed as parts by weight,
Natural beachhead slurry of mineral: 60 parts
Slurry of mineral elite water: 5 parts
Deionized water: 23.6 parts
Wetting agent: propylene glycol: 10 parts
1.5 parts of thickener/emulsifiers: polyacrylamide/C13-C14 isoparaffin/laureth-7:
Antiseptic: imidazolidinyl urea: 0.3 part
Concrete technology is as follows:
According to described ratio with natural beachhead slurry of mineral, slurry of mineral elite water is added among the primary response pot A in regular turn, temperature is controlled to be 80 ℃ of heated at constant temperature, stir 6-8 commentaries on classics/min, stir 60min, 15 parts of deionized waters are heated to 75 ℃ in prewired pot B, mixing speed is 30 commentaries on classics/min, add thickening agent and propylene glycol successively, prewired pot stirs, prewired pot component is transferred among the primary response pot A, washes prewired pot B with 8.6 parts of deionizations, and it is transferred among the primary response pot A, improve velocity of rotation and be increased to 10-12 commentaries on classics/min, continue to stir 60min, lasting stirring cools to 45 ℃, adds antiseptic, stir 30mi with same rotating speed, become semi-finished product to leave standstill fill to be detected to the room temperature discharging.
Embodiment 3: the preparation of the slurry of mineral of whitening washing facial film
The prescription of this slurry of mineral washing facial film is, calculates by weight,
Natural beachhead slurry of mineral: 75 parts
Slurry of mineral elite water: 6 parts
Deionized water: 9.5 parts
Wetting agent: butanediol: 6 parts
Thickener/emulsifier: 2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers: 1.5 parts
Functional additive: left-handed VC:2 part
Antiseptic: phenoxyethanol/ethylhexyl glycerol: 0.6 part
Concrete technology is as follows:
With natural beachhead slurry of mineral; slurry of mineral elite water is added among the primary response pot A in regular turn; temperature is controlled to be 85 ℃ of heated at constant temperature; stir 6-8 commentaries on classics/min; stir 60min; 5 parts of deionized waters are heated to 75 ℃ in prewired pot B; mixing speed is 30 commentaries on classics/min; add butanediol successively; 2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers; stir at prewired pot; prewired pot component is transferred among the primary response pot A, washes prewired pot B with 4.5 parts of deionizations, and it is transferred among the primary response pot A; improve velocity of rotation and be increased to 10-12 commentaries on classics/min; continue to stir 60min, lasting stirring cools to 45 ℃-50 ℃, adds 2 parts of left-handed VC and 0.6 part of phenoxyethanol/ethylhexyl glycerol gradually.Stir 30min with same rotating speed, become semi-finished product to leave standstill fill to be detected to the room temperature discharging.
The product of embodiment 2 and embodiment 3 is for to satisfy the mud mask of national operative norm " QB/T 2872 ", and its physical and chemical index and microbiological indicator meet national cosmetic 20007 standards, specifically see Table 1-table 2:
Figure DEST_PATH_IMAGE001
Figure 817242DEST_PATH_IMAGE002
Slurry of mineral washing facial film belongs to range of viscosities at the mastic of 8000-15000mpa.s, and the pH value span of control is at 6.5-8.5.

Claims (6)

1. a slurry of mineral washing facial film is characterized in that, comprises the composition of following weight portion:
20 parts-80 parts of slurry of minerals
5 parts-60 parts in slurry of mineral elite water
10 parts-40 parts of deionized waters
1 part-20 parts of wetting agents
0.5 part-5 parts of thickener/emulsifiers
0.1 part-1 part of antiseptic;
Described thickener/emulsifier be selected from 2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers or
Polyacrylamide/C 13-C 14Isoparaffin/laureth-7;
Wherein, the preparation method of described slurry of mineral and slurry of mineral elite water is: the stone gallbladder between the granite of gathering with beachhead town under the snowy peak mountain range, Longhui County, Hunan Province is raw material, and concrete steps are:
(1) air slaking: be that 10 ℃-40 ℃, humidity are air slaking 30-45 days under the environment of 10%-50% in temperature with the stone gallbladder;
(2) pre-soaking: the stone gallbladder after the air slaking is soaked in water 5 ℃-40 ℃ of soaking temperatures, soak time 25 minutes-35 minutes;
(3) physics is rough: the stone gallbladder after will soaking is beaten, and gets particle diameter<1000 purpose stone gallbladder powder ends;
(4) adding water mixes: with the end washing of above-mentioned stone gallbladder powder, add then water stir mixture; Washing temperature is 5 ℃-40 ℃, and water consumption is 3-4 times of stone gallbladder granular mass; Described mixture leaves standstill the back layering, removes mud and the impurity of bottom, keeps the troubled liquor that the middle part contains mud in suspension;
(5) just heavy: as described troubled liquor to be precipitated 30-40 days, control 5 ℃-40 ℃ of precipitation temperatures simultaneously; The layering of described troubled liquor post precipitation, the water a that separates the upper strata is standby, makes solid content>45% of the mud phase a of lower floor, gets mud one time;
(6) two is heavy: a described mud is precipitated 15-30 days again, and 5 ℃-40 ℃ of control precipitation temperatures, a described mud post precipitation layering again, the water b that separates the upper strata is standby, makes solid content>60% of the mud phase b of lower floor, gets secondary mud;
(7) dry: be 40 ℃-60 ℃ with described secondary mud in temperature, dried 10-15 days under the environment of humidity<50%, make mud solid content>80%, must dry mud;
(8) mud ageing: be 5 ℃-40 ℃ with the described mud that dries in temperature, ageing got slurry of mineral more than 30 days under the environment of humidity<50%;
(9) elite water ageing: merging described water a and water b is 5 ℃-40 ℃ in temperature, and ageing got mineral elite water more than 30 days under the environment of humidity<50%.
2. according to the described slurry of mineral washing of claim 1 facial film, it is characterized in that described wetting agent is selected from butanediol or propylene glycol.
3. according to the described slurry of mineral washing of claim 1 facial film, it is characterized in that described antiseptic is selected from phenoxyethanol/ethylhexyl glycerol or imidazolidinyl urea.
4. according to the described slurry of mineral washing of claim 1 facial film, it is characterized in that, in described slurry of mineral washing facial film, add 1-20 part functional additive.
5. according to the described slurry of mineral washing of claim 5 facial film, it is characterized in that described functional additive is left-handed VC.
6. the preparation method of the described slurry of mineral washing of one of claim 1-6 facial film is characterized in that, by described proportioning, slurry of mineral, slurry of mineral elite water is added among the primary response pot A, and the control temperature is 75 ℃-85 ℃, stirs 50 min-60min; Deionized water is heated to 70 ℃-80 ℃ in prewired pot B, adds wetting agent and thickener/emulsifier then successively, stir; Again the material among the prewired pot B is transferred among the primary response pot A, washes prewired pot B with deionized water, and deionized water is transferred among the primary response pot A, continue to stir 55 min-65min, cool then to 45 ℃-50 ℃; Add functional additive and antiseptic again, stir 25 min-35min, cooling discharging gets slurry of mineral washing facial film.
CN 201210383655 2012-10-11 2012-10-11 Mineral mud washing facial mask Active CN102846497B (en)

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Publication number Priority date Publication date Assignee Title
CN104800105A (en) * 2014-01-29 2015-07-29 李珍 Songhua stone mask and preparation method thereof
CN104546613A (en) * 2015-01-20 2015-04-29 王雪林 Mineral-plant nanometer facial mask
CN106137803A (en) * 2015-03-31 2016-11-23 佛山市禾才科技服务有限公司 A kind of Sage Extract heating facial film
CN108403479A (en) * 2018-04-17 2018-08-17 五池(珠海)日化科技有限公司 A kind of anti-wrinkle whitening antiallergy volcano clay mask and preparation method thereof
CN111329770A (en) * 2018-12-18 2020-06-26 抚顺金达莱生物科技有限公司 Deep-sea volcano sulfur paste mask cream and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1137888A (en) * 1995-06-12 1996-12-18 路有利 Pack cream made of volcano cold spring mineral mud
CN102210641A (en) * 2010-04-08 2011-10-12 周想燕 Negative ion beauty care mask and manufacturing method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1137888A (en) * 1995-06-12 1996-12-18 路有利 Pack cream made of volcano cold spring mineral mud
CN102210641A (en) * 2010-04-08 2011-10-12 周想燕 Negative ion beauty care mask and manufacturing method thereof

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