CN102836088B - Cleansing cream containing tea saponin and preparation method thereof - Google Patents
Cleansing cream containing tea saponin and preparation method thereof Download PDFInfo
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- CN102836088B CN102836088B CN 201210334529 CN201210334529A CN102836088B CN 102836088 B CN102836088 B CN 102836088B CN 201210334529 CN201210334529 CN 201210334529 CN 201210334529 A CN201210334529 A CN 201210334529A CN 102836088 B CN102836088 B CN 102836088B
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Abstract
The invention relates to a cleansing cream containing tea saponin and a preparation method of the cleansing cream. The cleansing cream is composed of the following components by weight: 35 to 65% of main surfactant system, 4 to 15% of auxiliary surfactant system, 2 to 8% of thickening agent system, 0.1 to 0.4% of preservative, 0.1 to 0.4% of chelating agent, 0.1 to 0.4% of humectants, 0.1 to 0.4%of nutrient, 0.1 to 0.4% of essence and the balance of water. The cleansing cream provided by the invention has the advantages of tenderness, hard water resistance, good cleaning capacity and low cost etc., and meanwhile has the characteristics of being easy to degrade and green and environmental-friendly and the like.
Description
Technical field
The invention belongs to the skin nursing field, specifically relate to a kind of facial cleaning cream that contains tea saponin and preparation method thereof.
Background technology
Clean product is divided into the facial milk cleanser of the moving shape of semi-fluid and the facial cleaning cream of solid state by physical state.Be divided into oil-in-water type and surfactant type by emulsifying property.By the hydrophilic and oleophilic character of its cleaning agent chemical composition phase, can be divided into: (1) is based on the surfactant type of soap base or other surfactants; (2) based on the solvent-borne type of oiliness composition, wetting agent, ethanol and water equal solvent; (3) marginal oil-in-water oil-in-water type.
Clean product is by oil phase, the facial dirt of aqueous phase dissolved, and the recycling surfactant reduces the effect of skin surface tension force, reaches the purpose of moistening, infiltration, dispersion, solubilising, decontamination.Simultaneously, surfactant can produce foam, through the water flushing, and the easier dirt of taking away, and certain effect that makes skin lubrication is arranged.
In the preparation process of facial cleaning cream, need facial milk cleanser is thickened to paste.The foundation of thickener system generally has three kinds of methods: by liquid crystal thickening, adding emulsifying agent or the adding polymer of surfactant.Mating surface activating agent kind, factors such as the mastic state of investigation final products, the thixotropy when using and production cost are determined the scheme that thickener system is set up at last.
When formula materials such as option table surface-active agent, emulsifying agent, polymer, also should consider its degradability, to guarantee the environmental protection of product.
Clean product of simple oil-in-water type be because the infiltration function of disperseing the skin surface dirt, thus cleaning power a little less than, and almost can not produce foam.Clean product of soap base type is because the structure of its highly basic saponification though have very strong cleaning capacity, also has very strong zest to skin simultaneously.Clean product of surfactant mainly contains alkyl polyoxyethylene ether phosphate ester (MAP) type, succinate type, sodium taurocholate type in the market; the cleaning power of these clean product is moderate; also relatively gentleer to skin, but it has different separately defectives at aspects such as foaminess, stability, stripping and production costs.
Summary of the invention
In order to solve the deficiency that prior art exists, the invention provides a kind of facial cleaning cream that contains tea saponin and preparation method thereof.
A kind of facial cleaning cream that contains tea saponin, described facial cleaning cream is made up of the component of following weight percent: master meter surfactant system 35～65%, auxilliary surfactant system 4～15%, thickener system 2～8%, antiseptic 0.1～0.4%, chelating agen 0.1～0.4%, wetting agent 0.1～0.4%, nutrient 0.1～0.4%, essence 0.1～0.4%, remainder are water;
Described master meter surfactant system is by N-acyl amino acids and the alkylsulfonate analog anion surfactants is composite forms, wherein, the mass ratio of N-acylamino acid analog anion surfactants and alkylsulfonate analog anion surfactants is 0.8～1.2:1;
Described auxilliary surfactant system is formed by tea saponin, fatty alcohol polyethenoxy ether class anion surfactant and betaines surfactant compound, wherein, the mass ratio of tea saponin, fatty alcohol polyethenoxy ether class anion surfactant and betaines surfactant is: 0.8～1.2:0.8～1.2:1.5～2.3;
Described thickener system is by hydroxypropyl starch phosphate ester (Structure XL), polyacrylic rheology modifier and the polyoxyethylene rheology modifier is composite forms, wherein, the mass ratio of hydroxypropyl starch phosphate ester, polyacrylic rheology modifier and polyoxyethylene rheology modifier is 1.8～2.2:1.3～1.6:0.3～0.4.
Preferably, described N-acylamino acid analog anion surfactants is one or more combination in any in cocoyl N-methyltaurine sodium (Igepon TC), cocoyl sodium glutamate (SCG), the sodium lauroyl sarcosine (LSS).
Preferably, described alkylsulfonate analog anion surfactants is one or more combination in any in cocoyl sodium isethionate (SCI), alkyl sulfosuccinate disodium (DAS), the cocoyl monomester succinate disodium sulfonate (DCS).
Preferably, described fatty alcohol polyethenoxy ether class anion surfactant is fatty alcohol-polyoxyethylene ether (3) sulfosuccinic acid monoesters disodium (MES) or dodecyl polyethenoxy ether sodium sulfate (AES).
Preferably, described betaines surfactant is cocamido propyl betaine (CAB).
Preferably, described polyacrylic rheology modifier is carbomer SF-1 or carbomer EDT2020.
Preferably, described polyoxyethylene rheology modifier is polyethylene glycol 6000 (PEG6000).
Preferably, described facial cleaning cream is made up of following components by part by weight: the master meter surfactant system: 20 parts in cocoyl N-methyltaurine sodium, 20 parts of cocoyl sodium isethionates; Auxilliary surfactant system: 2 parts of tea saponins, 3 parts of fatty alcohol-polyoxyethylene ether (3) sulfosuccinic acid monoesters disodiums, 5 parts of cocamido propyl betaine; Thickener system: 3 parts of hydroxypropyl starch phosphate esters, 2 parts of carbomer SF-1,0.5 part of polyethylene glycol 6000; 0.2 part of wetting agent; 0.2 part in essence; 0.2 part of chelating agen; 0.2 part of antiseptic; 0.2 part of nutrient; 43.5 parts of deionized waters.
A kind of preparation method that contains the facial cleaning cream of tea saponin, described preparation method comprises the steps:
(1) with N-acyl amino acids and the composite master meter surfactant system that forms of alkylsulfonate analog anion surfactants; Tea saponin, fatty alcohol polyethenoxy ether class anion surfactant and betaines surfactant compound are formed auxilliary surfactant system; The composite thickener system that forms of hydroxypropyl starch phosphate ester, polyacrylic rheology modifier and polyoxyethylene rheology modifier;
(2) add deionized water in the agitated kettle, add thickener system and wetting agent when being heated to 55～65 ℃;
(3) be heated with stirring to 70～80 ℃, add the master meter surfactant system;
(4) stir insulation after 15～30 minutes, add auxilliary surfactant system;
(5) be cooled to 45～55 ℃, add essence, chelating agen, antiseptic and nutrient respectively;
(6) be cooled to 35～45 ℃, insulated and stirred 50～70 minutes namely makes described facial cleaning cream.
Preferably, described preparation method specifically comprises the steps:
(1) gets 32 parts of Igepon TC, 2 parts of SCI and 11 parts of DCS and be made into the master meter surfactant system; Get 3 parts of tea saponins, 3 parts of AES and 6 parts of CAB and be made into auxilliary surfactant system; Get 4 parts of Structure XL, 3 parts of EDT2020 and 1 part of PEG6000 and be made into thickener system;
(2) add 33.8 parts of deionized waters in the agitated kettle, add thickener system and 0.2 part of wetting agent when being heated to 60 ℃;
(3) be heated with stirring to 78 ℃, add the master meter surfactant system;
(4) stir insulation 20 minutes, add auxilliary surfactant system;
(5) be cooled to 48 ℃, add 0.3 part of essence respectively, 0.4 part of chelating agen, 0.2 portion of antiseptic and 0.1 part of nutrient;
When (6) being cooled to 42 ℃, insulated and stirred 60 minutes namely makes described facial cleaning cream.
Antiseptic described in the present invention can be selected methyl hydroxybenzoate, phenoxyethanol for use; Described chelating agen can be selected disodiumedetate (EDTA disodium) for use; Described wetting agent can be selected glycerol, propylene glycol, 1,3 butylene glycol, sorbitol, PEG400, Polyethylene Glycol 800 etc. for use; Described nutrient can be selected D-panthenol, glycyrrhizic acid dipotassium for use.
Each component (raw material) of facial cleaning cream of the present invention all can obtain by commercial sources.
Tea saponin (Tea Saponin) is a kind of pentacyclic triterpenoid that extracts from the tea seed cake after the Camellia oil squeezing, is made up of sugared body, ruscogenin and organic acid.It is a kind of natural non-ionic surface active agent of function admirable, not only has good emulsifying, foaming, dispersion, infiltration, lubricated isoreactivity effect, but also has antiinflammatory, analgesia, sterilization, pharmacological action such as antipruritic.
Master meter surfactant system of the present invention has anti-hard water, the stable and good characteristics of foaminess; Auxilliary surfactant system have improve foaming power and viscosity, to the good bland characteristics of skin affinity; Thickener system have in polyelectrolyte thickening property strong, shear the back recover viscosity performance height, good stability, skin sense good, can improve foam quality, have characteristics such as biodegradability concurrently.
The present invention has gentleness, anti-hard water, good, the low cost and other advantages of cleaning power, also has characteristics such as easy degraded, environmental protection simultaneously.
The specific embodiment
The invention will be further described below in conjunction with specific embodiment, but protection scope of the present invention is not limited to this.
Embodiment 1
Get 20 parts of Igepon TC and 20 parts of SCI are made into the master meter surfactant system; Get 2 parts of tea saponins, 3 parts of MES and 5 parts of CAB and be made into auxilliary surfactant system; Get 3 parts of Structure XL, 2 parts of SF-1 and 0.5 part of PEG6000 and be made into thickener system; Add 43.5 parts of deionized waters in the agitated kettle, add thickener system and 0.2 part of wetting agent when being heated to 60 ℃; Continue to be heated with stirring to 78 ℃, add the master meter surfactant system; Stir insulation 20 minutes, add auxilliary surfactant system; Cool to 48 ℃, add 0.2 part of essence respectively, 0.2 part of chelating agen, 0.2 portion of antiseptic and 0.2 part of nutrient; When continuing to be cooled to 42 ℃, insulated and stirred 60 minutes namely makes described facial cleaning cream.
Embodiment 2
Get 30 parts of SCG, 19 parts of SCI and 9 parts of DCS and be made into the master meter surfactant system; Get 1 part of tea saponin, 1 part of MES and 2 parts of CAB and be made into auxilliary surfactant system; Get 2.5 parts of Structure XL, 2 parts of SF-1 and 0.4 part of PEG6000 and be made into thickener system; Add 31.5 parts of deionized waters in the agitated kettle, add thickener system and 0.4 part of wetting agent when being heated to 60 ℃; Continue to be heated with stirring to 78 ℃, add the master meter surfactant system; Stir insulation 20 minutes, add auxilliary surfactant system; Cool to 48 ℃, add 0.4 part of essence respectively, 0.2 part of chelating agen, 0.2 portion of antiseptic and 0.4 part of nutrient; When continuing to be cooled to 42 ℃, insulated and stirred 60 minutes namely makes described facial cleaning cream.
Embodiment 3
Get 10 parts of SCG, 8 parts of LSS and 18 parts of DCS and be made into the master meter surfactant system; Get 4 parts of tea saponins, 3 parts of AES and 8 parts of CAB and be made into auxilliary surfactant system; Get 2.2 parts of Structure XL, 1.6 parts of EDT2020 and 0.4 part of PEG6000 and be made into thickener system; Add 43.9 parts of deionized waters in the agitated kettle, add thickener system and 0.1 part of wetting agent when being heated to 60 ℃; Continue to be heated with stirring to 78 ℃, add the master meter surfactant system; Stir insulation 20 minutes, add auxilliary surfactant system; Cool to 48 ℃, add 0.1 part of essence respectively, 0.1 part of chelating agen, 0.4 portion of antiseptic and 0.2 part of nutrient; When continuing to be cooled to 42 ℃, insulated and stirred 60 minutes namely makes described facial cleaning cream.
Embodiment 4
Get 32 parts of Igepon TC, 2 parts of SCI and 11 parts of DCS and be made into the master meter surfactant system; Get 3 parts of tea saponins, 3 parts of AES and 6 parts of CAB and be made into auxilliary surfactant system; Get 4 parts of Structure XL, 3 parts of EDT2020 and 1 part of PEG6000 and be made into thickener system; Add 33.8 parts of deionized waters in the agitated kettle, add thickener system and 0.2 part of wetting agent when being heated to 60 ℃; Continue to be heated with stirring to 78 ℃, add the master meter surfactant system; Stir insulation 20 minutes, add auxilliary surfactant system; Cool to 48 ℃, add 0.3 part of essence respectively, 0.4 part of chelating agen, 0.2 portion of antiseptic and 0.1 part of nutrient; When continuing to be cooled to 42 ℃, insulated and stirred 60 minutes namely makes described facial cleaning cream.
Embodiment 5
Get 7 parts of Igepon TC, 7 parts of SCG, 6 parts of LSS and 24 parts of DAS and be made into the master meter surfactant system; Get 3 parts of tea saponins, 2 parts of MES and 4 parts of CAB and be made into auxilliary surfactant system; Get 2.0 parts of Structure XL, 1.5 parts of SF-1 and 0.3 part of PEG6000 and be made into thickener system; Add 42.1 parts of deionized waters in the agitated kettle, add thickener system and 0.2 part of wetting agent when being heated to 60 ℃; Continue to be heated with stirring to 78 ℃, add the master meter surfactant system; Stir insulation 20 minutes, add auxilliary surfactant system; Cool to 48 ℃, add 0.2 part of essence respectively, 0.3 part of chelating agen, 0.1 portion of antiseptic and 0.3 part of nutrient; When continuing to be cooled to 42 ℃, insulated and stirred 60 minutes namely makes described facial cleaning cream.
Antiseptic described in above-described embodiment is selected methyl hydroxybenzoate for use; Described chelating agen is selected the EDTA disodium for use; Described wetting agent is selected 1,3 butylene glycol for use; Described nutrient is selected D-panthenol for use.
Use demonstration continuously through several not specific users, facial cleaning cream pasty consistence of the present invention varies with temperature not quite, is applied to during use that thixotropy is good on hand, and foam enriches fine and closely woven flexible, and gentleness is not dazzling, easily rinses well, and it is refreshing clean, not tight that skin is washed the back.
Claims (4)
1. facial cleaning cream that contains tea saponin, it is characterized in that: described facial cleaning cream is made up of the component of following weight percent: master meter surfactant system 35～65%, auxilliary surfactant system 4～15%, thickener system 2～8%, antiseptic 0.1～0.4%, chelating agen 0.1～0.4%, wetting agent 0.1～0.4%, nutrient 0.1～0.4%, essence 0.1～0.4%, remainder are water;
Described master meter surfactant system is by N-acyl amino acids and the alkylsulfonate analog anion surfactants is composite forms, wherein, the mass ratio of N-acylamino acid analog anion surfactants and alkylsulfonate analog anion surfactants is 0.8～1.2:1;
Described auxilliary surfactant system is formed by tea saponin, fatty alcohol polyethenoxy ether class anion surfactant and betaines surfactant compound, wherein, the mass ratio of tea saponin, fatty alcohol polyethenoxy ether class anion surfactant and betaines surfactant is: 0.8～1.2:0.8～1.2:1.5～2.3;
Described thickener system is by hydroxypropyl starch phosphate ester, polyacrylic rheology modifier and the polyoxyethylene rheology modifier is composite forms, wherein, the mass ratio of hydroxypropyl starch phosphate ester, polyacrylic rheology modifier and polyoxyethylene rheology modifier is 1.8～2.2:1.3～1.6:0.3～0.4;
Wherein, described N-acylamino acid analog anion surfactants is one or more combination in any in cocoyl N-methyltaurine sodium, cocoyl sodium glutamate, the sodium lauroyl sarcosine;
Described alkylsulfonate analog anion surfactants is one or more combination in any in cocoyl sodium isethionate, alkyl sulfosuccinate disodium, the cocoyl monomester succinate disodium sulfonate;
Described fatty alcohol polyethenoxy ether class anion surfactant is fatty alcohol-polyoxyethylene ether (3) sulfosuccinic acid monoesters disodium or dodecyl polyethenoxy ether sodium sulfate;
Described betaines surfactant is cocamido propyl betaine;
Described polyacrylic rheology modifier is carbomer SF-1 or carbomer EDT2020;
Described polyoxyethylene rheology modifier is polyethylene glycol 6000.
2. the facial cleaning cream that contains tea saponin according to claim 1, it is characterized in that: described facial cleaning cream is made up of following components by part by weight: the master meter surfactant system: 20 parts in cocoyl N-methyltaurine sodium, 20 parts of cocoyl sodium isethionates; Auxilliary surfactant system: 2 parts of tea saponins, 3 parts of fatty alcohol-polyoxyethylene ether (3) sulfosuccinic acid monoesters disodiums, 5 parts of cocamido propyl betaine; Thickener system: 3 parts of hydroxypropyl starch phosphate esters, 2 parts of carbomer SF-1,0.5 part of polyethylene glycol 6000; 0.2 part of wetting agent; 0.2 part in essence; 0.2 part of chelating agen; 0.2 part of antiseptic; 0.2 part of nutrient; 43.5 parts of deionized waters.
3. described preparation method that contains the facial cleaning cream of tea saponin of claim 1, it is characterized in that: described preparation method comprises the steps:
(1) with N-acyl amino acids and the composite master meter surfactant system that forms of alkylsulfonate analog anion surfactants; Tea saponin, fatty alcohol polyethenoxy ether class anion surfactant and betaines surfactant compound are formed auxilliary surfactant system; The composite thickener system that forms of hydroxypropyl starch phosphate ester, polyacrylic rheology modifier and polyoxyethylene rheology modifier;
(2) add deionized water in the agitated kettle, add thickener system and wetting agent when being heated to 55～65 ℃;
(3) be heated with stirring to 70～80 ℃, add the master meter surfactant system;
(4) stir insulation after 15～30 minutes, add auxilliary surfactant system;
(5) be cooled to 45～55 ℃, add essence, chelating agen, antiseptic and nutrient respectively;
(6) be cooled to 35～45 ℃, insulated and stirred 50～70 minutes namely makes described facial cleaning cream.
4. the preparation method that contains the facial cleaning cream of tea saponin according to claim 3, it is characterized in that: described preparation method specifically comprises the steps:
(1) gets 32 parts of cocoyl N-methyltaurine sodium, 2 parts of cocoyl sodium isethionates and 11 parts of alkyl sulfosuccinate disodiums and be made into the master meter surfactant system; Get 3 parts of tea saponins, 3 parts of dodecyl polyethenoxy ether sodium sulfates and 6 parts of cocamido propyl betaine and be made into auxilliary surfactant system; Get 4 parts of hydroxypropyl starch phosphate esters, 3 parts of carbomer EDT2020 and 1 part of polyethylene glycol 6000 and be made into thickener system;
(2) add 33.8 parts of deionized waters in the agitated kettle, add thickener system and 0.2 part of wetting agent when being heated to 60 ℃;
(3) be heated with stirring to 78 ℃, add the master meter surfactant system;
(4) stir insulation 20 minutes, add auxilliary surfactant system;
(5) be cooled to 48 ℃, add 0.3 part of essence respectively, 0.4 part of chelating agen, 0.2 portion of antiseptic and 0.1 part of nutrient;
When (6) being cooled to 42 ℃, insulated and stirred 60 minutes namely makes described facial cleaning cream.
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| CN 201210334529 CN102836088B (en) | 2012-09-12 | 2012-09-12 | Cleansing cream containing tea saponin and preparation method thereof |
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| CN 201210334529 CN102836088B (en) | 2012-09-12 | 2012-09-12 | Cleansing cream containing tea saponin and preparation method thereof |
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| CN103961271B (en) * | 2014-01-08 | 2017-01-25 | 片仔癀（上海）生物科技研发有限公司 | Cleansing cream and preparation method thereof |
| CN103789096A (en) * | 2014-03-10 | 2014-05-14 | 天津澳锐泰环保科技有限公司 | Efficient environment-friendly solid-type food-grade non-toxic glass cleaning agent and preparation method thereof |
| CN105476950B (en) * | 2014-12-22 | 2017-07-07 | 吉林伊捷思化学有限公司 | Moisturizing foam mildy wash and preparation method thereof |
| CN105238599B (en) * | 2015-11-09 | 2018-11-27 | 重庆琥珀茶油有限公司 | A kind of amino acid tea oil face cleaning skin lotion soap |
| KR102157745B1 (en) | 2015-12-10 | 2020-09-21 | 로레알 | Composition for cleaning keratin materials with improved rinsing properties |
| CN105560154A (en) * | 2016-01-22 | 2016-05-11 | 柳州博泽科技有限公司 | Gentle facial cleanser capable of moistening skin and preparing method thereof |
| CN105997669A (en) * | 2016-06-18 | 2016-10-12 | 广州丹奇日用化工厂有限公司 | Facial cleansing cream containing Swiss chard polysaccharide and preparation method of facial cleansing cream |
| CN106311159A (en) * | 2016-09-08 | 2017-01-11 | 合肥智慧殿投资管理有限公司 | Composite filter material and preparation method and application thereof |
| CN106580729A (en) * | 2016-11-13 | 2017-04-26 | 何志德 | Preparation formula for novel amino acid face cleaning slice and preparation method thereof |
| CN107582427B (en) * | 2017-09-26 | 2019-01-25 | 广州宏度精细化工有限公司 | Non-soap base facial cleanser and preparation method thereof |
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| CN1349793A (en) * | 2001-11-06 | 2002-05-22 | 广东轻工职业技术学院 | Composite body wash containing tea component and its making process |
| CN100372521C (en) * | 2006-02-06 | 2008-03-05 | 高明全 | Bathing agent possessing health and medical function and its preparation method |
| CN100569214C (en) * | 2008-11-06 | 2009-12-16 | 郴州邦尔泰苏仙油脂有限公司 | Tea saponin shampoo and production technology |
| CN102144959B (en) * | 2011-04-19 | 2012-07-04 | 广州好迪集团有限公司 | Bath foam with nourishing and moisturizing functions |
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