CN102793656B - Firming anti-wrinkle essence cosmetic and preparation method - Google Patents
Firming anti-wrinkle essence cosmetic and preparation method Download PDFInfo
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- CN102793656B CN102793656B CN 201210285658 CN201210285658A CN102793656B CN 102793656 B CN102793656 B CN 102793656B CN 201210285658 CN201210285658 CN 201210285658 CN 201210285658 A CN201210285658 A CN 201210285658A CN 102793656 B CN102793656 B CN 102793656B
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Abstract
The invention discloses a firming anti-wrinkle essence cosmetic and a preparation method, and the cosmetic comprises the following ingredients by weight: a) a firming anti-wrinkle ingredient, b) an oil phase ingredient, c) a water phase ingredient, d) triethanolamine and e) an auxiliary agent ingredient; the preparation method comprises the following steps: heating the C phase to the temperature of 60-95 DEG C, insulating to the temperature of 75-85 DEG C, completely stirring and dissolving; heating the B phase to the temperature of 60-80 DEG C, completely stirring and dissolving; sucking the C phase into an emulsification pot, then sucking the B phase slowly into the emulsification pot, homogenizing the mixture for 5 to 15 minutes, keeping the temperature and stirring the mixture for 5 to 15 minutes, and vacuumizing the mixture to reduce the temperature; adding the D phase and the A phase when the temperature is between 55 and 65 DEG C, homogenizing the mixture for 2 to 3 minutes, and stirring the mixture evenly; adding the E phase when the temperature is between 35 and 45 DEG C, and stirring the mixture evenly to obtain the firming anti-wrinkle essence cosmetic. The obtained firming anti-wrinkle essence cosmetic can reduce the wrinkle and prevent the generation of wrinkle, and enables firming, smoothness, tenderness and softness of the skin.
Description
[technical field]
The present invention relates to a kind of re-surface intensive wrinkle correct cosmetics that compact, the invention still further relates to a kind of method for preparing these re-surface intensive wrinkle correct cosmetics that compact, belong to the cosmetics technical field.
[background technology]
Skin aging is a kind of gradual physiological process, direct cutaneous outward appearance and function of continuing.Wrinkle is a kind of sign of skin aging performance, is referred to as " annual ring of life ".Along with people's raising of quality of life, the anti-aging skin removed wrinkle that compacts, return to the topic that the youth has become consumers in general to pay close attention to.
In recent years, use the natural physiological active material to improve skin and occur that because relaxing the anti-aging anti-wrinkle cosmetic that compacts of wrinkle more and more paid attention to by people, its safety and effect also become the emphasis that consumer and producer pay close attention to naturally.
Skin aging is except the factor that self organism aging process skin cell proliferation, metabolism slow down, and the impact of environmental factors is also very large.Skin is the natural cover for defense of resisting the external environment infringement.Yet its long term exposure, in external environment, unavoidably can sustain damage, wherein the nocuous factor of tool is ultraviolet, infrared ray, pollution and flue dust.Dermal exposure is when external environment, cell can constantly produce free radical, these free radicals can injure epidermis and corium (damage of oxidisability comprises oil peroxidation and weakens the skin defense function), cause skin premature aging (skin wrinkle occurs and becomes lax), especially long term exposure in the position of sunlight and reaction minimizing.
Ultraviolet radiation can make free-radical contents in skin increase, and also can cause elastin laminin and collagen degradation, makes the skin roughening, lacks flexibility, lax, forms wrinkle.
Existing crease-resistant anti-aging cosmetics kind is a lot, but its effect generally all not obvious or security performance have to be assessedly, successful is all sought by consumer and producer constantly, natural safe crease-resistant anti-aging cosmetics.
[summary of the invention]
The objective of the invention is to overcome the deficiencies in the prior art, a kind of successful is provided, instant effect, the natural safe re-surface intensive wrinkle correct cosmetics that compact.
Another object of the present invention is for a kind of preparation method of these re-surface intensive wrinkle correct cosmetics that compact is provided.
The present invention to achieve these goals, by the following technical solutions:
A kind of re-surface intensive wrinkle correct cosmetics that compact is characterized in that percentage composition comprises following component by weight:
A, crease-resistant component compacts
B, oil phase components
Hydrolecithin 0.1～2.0%
Cyclomethicone 1.0～5.0%
Fertility 2, 2-Oxydiphenol 0.2～5.0%
C, water component
D, triethanolamine 0.1～0.5%
E, auxiliary agent component 0.3～1.0%.
A kind of re-surface intensive wrinkle correct cosmetics that compact as above is characterized in that percentage composition comprises following component by weight:
A, crease-resistant component compacts
B, oil phase components
Hydrolecithin 0.1～1.5%
Cyclomethicone 2.0～4.0%
Fertility 2, 2-Oxydiphenol 0.5～4.5%
C, water component
D, triethanolamine 0.1～0.4%
E, auxiliary agent component 0.3～0.8%.
A kind of re-surface intensive wrinkle correct cosmetics that compact as above is characterized in that percentage composition comprises following component by weight:
A, crease-resistant component compacts
B, oil phase components
Hydrolecithin 0.5～1.0%
Cyclomethicone 2.5～3.5%
Fertility 2, 2-Oxydiphenol 1.5～3.5%
C, water component
D, triethanolamine 0.2～0.3%
E, auxiliary agent component 0.4～0.7%.
A kind of re-surface intensive wrinkle correct cosmetics that compact as above, is characterized in that described fertility 2, 2-Oxydiphenol is PEG/PPG-70/30 fertility 2, 2-Oxydiphenol.
A kind of re-surface intensive wrinkle correct cosmetics that compact as above, is characterized in that described auxiliary agent component is one or both mixture in essence, antiseptic.
A kind of method for preparing the described re-surface intensive wrinkle correct cosmetics that compact of claim 1 is characterized in that comprising the following steps:
(1) C is warmed up to 60～95 ℃ mutually, insulation is to 75～85 ℃, and stirring and dissolving is complete;
(2) B is warmed up to 60～80 ℃ mutually, stirring and dissolving is complete;
(3) first by C phase suction emulsifying pot, then suction B phase slowly, homogenizing 5～15min, insulated and stirred 5～15min, evacuation cooling;
Add the D phase in the time of (4) 55～65 ℃, the A phase, homogenizing 2～3min, stir;
Add the E phase in the time of (5) 35～45 ℃, stir, get final product.
In the present invention, the crease-resistant component that compacts is the major function additive.Wherein:
Tremella extract and hydrolytic collagen synergism, the biochemically active composition that viscous polysaccharide body in Tremella extract and micromolecular hydrolytic collagen (molecular weight is about 1000) are combined into, hydrolytic collagen is attached on vegetalitas mucopolysaccharide molecule, reach the more depths of epidermal area, make skin obtain more permanent moisturizing wrinkle removing effect.
The hydrolytic collagen of Tremella viscous polysaccharide body and nanorize can form the thin film of layer of transparent on skin, and can on skin, form obvious firming effect within the extremely short time.
Oat polypeptide is a kind of plant complex that is derived from Herba bromi japonici, comprises avenin and avenabeta glucosan.It has very outstanding moistening effect, and the instant effect of tightening up and softening tiny wrinkle, strengthen skin care, improves the ability of skin opposing environmental stimuli, also has the antiageing effect texts.
The advanced technologies production of oat polypeptide based on unique, with protein and the beta glucan of water extraction avenia part.The avenin extracted comprises: albumin and globulin; The avenabeta glucosan extracted is in the field of activity of polysaccharide.
The cosmetics function of oat polypeptide have following some:
Bao Shi & Softening skin: the albumen of high molecular and avenabeta glucosan can guarantee its performance of keeping humidity and the film forming ability of protectiveness, the outward appearance of can also film forming giving skin smooth.
Excellent film forming function: oat polypeptide contains avenin and avenabeta glucosan, can, in film forming under low concentration, play the effect of embedding or isolation small-molecule substance, fast Transport Activities composition or time controlled released.
Aging resistance: oat polypeptide is proved to be to have the effect of improving skin coarseness and free radical resisting and can suppress and prevent skin aging, improves the skin surface situation.
Reduce skin coarseness: after using oat polypeptide, skin texture improves.
Free radical resisting:
The experimental data of issuing according to some researchers is presented at the local free radical scavenger (compound that can suppress radical reaction) that uses in the infringement that reduces the skin vigorous oxidation has protective effect to skin; life-time service can significantly suppress thinning of skin and flexibility decrease; the slow down formation of wrinkle, and some damages are also had to repair.The variable concentrations oat polypeptide is removed the ability difference to hydroxy radical, and concentration increases removes strong free radical ability enhancing.10% oat polypeptide reaches 60% to the hydroxy radical suppression ratio.
The present invention compared with prior art, has following advantage:
1. for aging and tired out skin, can find out significantly after use that catabiosis slows down, and the microgroove of skin surface also reduces.Prevent that wrinkle from producing, and make that skin seems smoothly, delicacy, soft.
2. can make to damage skin and become at short notice more level and smooth.
3. can form a meticulous thin film in cortical surface, make it have obvious firming effect, than other products, its effect is more rapid, and bright obvious effect was arranged about 15-30 minute.Use after 15 minutes, after wrinkle depth reduces 14%, 30 minute, wrinkle depth reduces 20%.
[specific embodiment]
Below in conjunction with specific embodiment, the invention will be further described:
Embodiment 1:
A kind of re-surface intensive wrinkle correct cosmetics that compact of the present invention, it comprises following component by weight percentage:
A, crease-resistant component compacts
B, oil phase components
Hydrolecithin 1.0%
Cyclomethicone 3.0%
Fertility 2, 2-Oxydiphenol 2.5%
C, water component
D, triethanolamine 0.3%
E, auxiliary agent component 0.7%
Wherein the auxiliary agent component is essence 0.4%, antiseptic 0.3%.
The compact preparation of re-surface intensive wrinkle correct cosmetics of this enforcement completes by following steps:
(1) C is warmed up to 85 ℃ mutually, insulation is to 80 ℃, and stirring and dissolving is complete;
(2) B is warmed up to 70 ℃ mutually, stirring and dissolving is complete;
(3) first by C phase suction emulsifying pot, then suction B phase slowly, homogenizing 10min, insulated and stirred 10min, evacuation cooling;
Add the D phase in the time of (4) 60 ℃, the A phase, homogenizing 3min, stir;
Add the E phase in the time of (5) 40 ℃, stir, obtain the present embodiment product.
Below with table 1, list compact each composition weight percentage composition of re-surface intensive wrinkle correct cosmetics embodiment 2-embodiment 7 of the present invention:
The preparation method of embodiment 2 comprises the following steps:
(1) C is warmed up to 60 ℃ mutually, insulation is to 75 ℃, and stirring and dissolving is complete;
(2) B is warmed up to 60 ℃ mutually, stirring and dissolving is complete;
(3) first by C phase suction emulsifying pot, then suction B phase slowly, homogenizing 5min, insulated and stirred 5min, evacuation cooling;
Add the D phase in the time of (4) 55 ℃, the A phase, homogenizing 2min, stir;
Add the E phase in the time of (5) 35 ℃, stir, obtain the present embodiment product.
The preparation method of embodiment 3 comprises the following steps:
(1) C is warmed up to 65 ℃ mutually, insulation is to 78 ℃, and stirring and dissolving is complete;
(2) B is warmed up to 65 ℃ mutually, stirring and dissolving is complete;
(3) first by C phase suction emulsifying pot, then suction B phase slowly, homogenizing 8min, insulated and stirred 8min, evacuation cooling;
Add the D phase in the time of (4) 58 ℃, the A phase, homogenizing 3min, stir;
Add the E phase in the time of (5) 38 ℃, stir, obtain the present embodiment product.
The preparation method of embodiment 4 comprises the following steps:
(1) C is warmed up to 70 ℃ mutually, insulation is to 80 ℃, and stirring and dissolving is complete;
(2) B is warmed up to 70 ℃ mutually, stirring and dissolving is complete;
(3) first by C phase suction emulsifying pot, then suction B phase slowly, homogenizing 10min, insulated and stirred 10min, evacuation cooling;
Add the D phase in the time of (4) 60 ℃, the A phase, homogenizing 3min, stir;
Add the E phase in the time of (5) 40 ℃, stir, obtain the present embodiment product.
The preparation method of embodiment 5 comprises the following steps:
(1) C is warmed up to 75 ℃ mutually, insulation is to 85 ℃, and stirring and dissolving is complete;
(2) B is warmed up to 75 ℃ mutually, stirring and dissolving is complete;
(3) first by C phase suction emulsifying pot, then suction B phase slowly, homogenizing 12min, insulated and stirred 12min, evacuation cooling;
Add the D phase in the time of (4) 65 ℃, the A phase, homogenizing 2min, stir;
Add the E phase in the time of (5) 45 ℃, stir, obtain the present embodiment product.
The preparation method of embodiment 6 comprises the following steps:
(1) C is warmed up to 80 ℃ mutually, insulation is to 75 ℃, and stirring and dissolving is complete;
(2) B is warmed up to 80 ℃ mutually, stirring and dissolving is complete;
(3) first by C phase suction emulsifying pot, then suction B phase slowly, homogenizing 15min, insulated and stirred 15min, evacuation cooling;
Add the D phase in the time of (4) 60 ℃, the A phase, homogenizing 2min, stir;
Add the E phase in the time of (5) 40 ℃, stir, obtain the present embodiment product.
The preparation method of embodiment 7 comprises the following steps:
(1) C is warmed up to 95 ℃ mutually, insulation is to 85 ℃, and stirring and dissolving is complete;
(2) B is warmed up to 80 ℃ mutually, stirring and dissolving is complete;
(3) first by C phase suction emulsifying pot, then suction B phase slowly, homogenizing 8min, insulated and stirred 8min, evacuation cooling;
Add the D phase in the time of (4) 60 ℃, the A phase, homogenizing 3min, stir;
Add the E phase in the time of (5) 40 ℃, stir, obtain the present embodiment product.
Repairing anti-wrinkle composite cosmetic to embodiment 1 to 7 is done some testing performance indexes, and its test is as follows:
1. outward appearance: translucent liquid
2.pH value: 4.0-7.0
3. viscosity: 1000-10000mpa.s
4. heat-resistant stability is investigated (48 ℃ * 24h): qualified
5. study on the stability (15 ℃ * 24h) resists cold: qualified
Properties of product evaluation test of the present invention is as follows:
One, irritation test:
Select 40 of 2.5～3kg healthy rabbits, every rabbit back left-right symmetric selects 20 places to shave a mao 2.5cm
2, with the own control test method(s), carry out, be coated with 0.5g product of the present invention or blank substrate at every turn, every day twice, the random administration in left side or right side, observe and record the reacting phenomenon of skin after 24h, 72h.
Result shows: is coated with after product 24h of the present invention, 72h the reaction such as the local excitations that have no skin rubefaction, dermexanthesis, water lump, illustrates that the present invention's re-surface intensive wrinkle correct cosmetics that compact are to be perfectly safe, without any untoward reaction.
Two, effect checking:
Select 140 volunteers that the facial wrinkles degree is close, be divided into seven groups, every group of 20 people, every group is further divided into two groups, 10 people of each group, and group's 1 use is without the blank placebo of the crease-resistant component that compacts, group 2 product of the present invention, product acts on eye, and each once, uses one month continuously sooner or later.
The wrinkle removal effect is described:
Obviously: dark stricture of vagina is unfolded not obvious, and microgroove disappears, and skin-tightening is flexible, and lax sense disappears;
Alleviate: dark crenulation degree alleviates, and microgroove is unfolded not obvious, skin-tightening, and lax sense disappears;
The slight improvement: microgroove alleviates, and skin is flexible, and lax sense disappears.
Result: in 70 examples, that uses product successful of the present invention accounts for 82.9%, and what effect was alleviated accounts for 17.1%, and effective percentage is 100% altogether, and all untoward reaction appears in none example of experimenter.
Claims (6)
1. re-surface intensive wrinkle correct cosmetics that compact is characterized in that each component of percentage composition meter is as follows by weight:
A, crease-resistant component compacts
B, oil phase components
Hydrolecithin 0.1～2.0%
Cyclomethicone 1.0～5.0%
Fertility 2, 2-Oxydiphenol 0.2～5.0%
C, water component
D, triethanolamine 0.1～0.5%
E, auxiliary agent component 0.3～1.0%.
2. a kind of re-surface intensive wrinkle correct cosmetics that compact according to claim 1 is characterized in that each component of percentage composition meter is as follows by weight:
A, crease-resistant component compacts
B, oil phase components
Hydrolecithin 0.1～1.5%
Cyclomethicone 2.0～4.0%
Fertility 2, 2-Oxydiphenol 0.5～4.5%
C, water component
D, triethanolamine 0.1～0.4%
E, auxiliary agent component 0.3～0.8%.
3. a kind of re-surface intensive wrinkle correct cosmetics that compact according to claim 2 is characterized in that each component of percentage composition meter is as follows by weight:
A, crease-resistant component compacts
B, oil phase components
Hydrolecithin 0.5～1.0%
Cyclomethicone 2.5～3.5%
Fertility 2, 2-Oxydiphenol 1.5～3.5%
C, water component
D, triethanolamine 0.2～0.3%
E, auxiliary agent component 0.4～0.7%.
4. according to claim 1 or 2 or 3 described a kind of re-surface intensive wrinkle correct cosmetics that compact, it is characterized in that described fertility 2, 2-Oxydiphenol is PEG/PPG-70/30 fertility 2, 2-Oxydiphenol.
5. according to claim 1 or 2 or 3 described a kind of re-surface intensive wrinkle correct cosmetics that compact, it is characterized in that described auxiliary agent component is one or both mixture in essence, antiseptic.
6. a method for preparing the described re-surface intensive wrinkle correct cosmetics that compact of claim 1 is characterized in that comprising the following steps:
(1) C is warmed up to 60～95 ℃ mutually, insulation is to 75～85 ℃, and stirring and dissolving is complete;
(2) B is warmed up to 60～80 ℃ mutually, stirring and dissolving is complete;
(3) first by C phase suction emulsifying pot, then suction B phase slowly, homogenizing 5～15min, insulated and stirred 5～15min, evacuation cooling;
Add the D phase in the time of (4) 55～65 ℃, the A phase, homogenizing 2～3min, stir;
Add the E phase in the time of (5) 35～45 ℃, stir, get final product.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210285658 CN102793656B (en) | 2012-08-10 | 2012-08-10 | Firming anti-wrinkle essence cosmetic and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210285658 CN102793656B (en) | 2012-08-10 | 2012-08-10 | Firming anti-wrinkle essence cosmetic and preparation method |
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| CN102793656A CN102793656A (en) | 2012-11-28 |
| CN102793656B true CN102793656B (en) | 2013-12-25 |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103054771A (en) * | 2012-12-21 | 2013-04-24 | 黎东宇 | Ultra-elastic water-locking facial mask essence and preparation method thereof |
| CN103637952B (en) * | 2013-12-10 | 2015-07-01 | 彭再辉 | Mask liquid for whitening hydrating mask paste and preparation method and application thereof |
| CN103655330B (en) * | 2014-01-23 | 2015-08-05 | 彭再辉 | A kind of man wakes up skin moisturizer and preparation method thereof |
| CN104758239A (en) * | 2015-04-24 | 2015-07-08 | 李丽琼 | Anti-wrinkle essence and preparation method |
| CN105125476B (en) * | 2015-10-19 | 2018-06-05 | 广州科玛生物科技股份有限公司 | A kind of anti-wrinkle essence and preparation method thereof |
| CN105640796B (en) * | 2016-01-13 | 2017-02-15 | 中山爱护日用品有限公司 | Composition with high moisture retention performance and application of composition to infant cream |
| CN106265149A (en) * | 2016-08-30 | 2017-01-04 | 广州君恒生物科技有限公司 | A kind of anti-wrinkle cream |
| CN107693406A (en) * | 2017-11-17 | 2018-02-16 | 皮光明 | Whitening is compacted plant essence cosmetics and preparation method thereof |
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| CN101590002A (en) * | 2009-06-23 | 2009-12-02 | 广州保税区雅兰国际化妆品有限公司 | A kind of repairing anti-wrinkle composite cosmetic and preparation method thereof |
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| CN102488627A (en) * | 2011-12-31 | 2012-06-13 | 上海宝姿化妆品有限公司 | Radiation-resistant and moisture-retention make-up base, lotion and water |
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| CN101590002A (en) * | 2009-06-23 | 2009-12-02 | 广州保税区雅兰国际化妆品有限公司 | A kind of repairing anti-wrinkle composite cosmetic and preparation method thereof |
| CN101590003A (en) * | 2009-06-23 | 2009-12-02 | 广州保税区雅兰国际化妆品有限公司 | A kind of whitening spot-relieving cream cosmetic and preparation method thereof |
| CN102488627A (en) * | 2011-12-31 | 2012-06-13 | 上海宝姿化妆品有限公司 | Radiation-resistant and moisture-retention make-up base, lotion and water |
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| CN102793656A (en) | 2012-11-28 |
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Effective date of registration: 20170524 Address after: 510000, No. 2, A zone, industrial road, Taihe village, Zhenlong, Baiyun District, Guangzhou, Guangdong Patentee after: GUANGZHOU AOLE COSMETICS CO.,LTD. Address before: 510000, Guangdong, Guangzhou Province, Baiyun District, long Cheng Park, Xia Industrial Avenue, West A District No. 2, Guangzhou City Ao Cosmetics Co., Ltd. Patentee before: Peng Zaihui |
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