CN102754904A - Quince and hot pepper combined extractive and usage thereof for serving as tobacco additive - Google Patents
Quince and hot pepper combined extractive and usage thereof for serving as tobacco additive Download PDFInfo
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- CN102754904A CN102754904A CN2011101048822A CN201110104882A CN102754904A CN 102754904 A CN102754904 A CN 102754904A CN 2011101048822 A CN2011101048822 A CN 2011101048822A CN 201110104882 A CN201110104882 A CN 201110104882A CN 102754904 A CN102754904 A CN 102754904A
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- extract
- quince
- tobacco
- peppers
- feed liquid
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- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 43
- 235000017788 Cydonia oblonga Nutrition 0.000 title claims abstract description 37
- 239000000654 additive Substances 0.000 title claims abstract description 16
- 230000000996 additive effect Effects 0.000 title claims abstract description 11
- 240000008574 Capsicum frutescens Species 0.000 title abstract description 22
- 235000002568 Capsicum frutescens Nutrition 0.000 title abstract 5
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- 241000208125 Nicotiana Species 0.000 claims abstract description 42
- 239000007788 liquid Substances 0.000 claims abstract description 21
- 239000002994 raw material Substances 0.000 claims abstract description 15
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 9
- 238000001914 filtration Methods 0.000 claims abstract description 8
- 239000011347 resin Substances 0.000 claims abstract description 8
- 229920005989 resin Polymers 0.000 claims abstract description 8
- 239000000796 flavoring agent Substances 0.000 claims abstract description 7
- 238000000926 separation method Methods 0.000 claims abstract description 7
- 235000019634 flavors Nutrition 0.000 claims abstract description 5
- 239000002798 polar solvent Substances 0.000 claims abstract description 3
- 239000000284 extract Substances 0.000 claims description 55
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 47
- 235000002566 Capsicum Nutrition 0.000 claims description 46
- 235000019504 cigarettes Nutrition 0.000 claims description 34
- 235000019505 tobacco product Nutrition 0.000 claims description 23
- 239000001390 capsicum minimum Substances 0.000 claims description 20
- 241000758706 Piperaceae Species 0.000 claims description 19
- 229940069774 quince extract Drugs 0.000 claims description 19
- 238000000605 extraction Methods 0.000 claims description 16
- 239000002131 composite material Substances 0.000 claims description 15
- 229940116257 pepper extract Drugs 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 8
- 239000002904 solvent Substances 0.000 claims description 8
- 239000006002 Pepper Substances 0.000 claims description 7
- 235000016761 Piper aduncum Nutrition 0.000 claims description 7
- 235000017804 Piper guineense Nutrition 0.000 claims description 7
- 235000008184 Piper nigrum Nutrition 0.000 claims description 7
- 239000006227 byproduct Substances 0.000 claims description 7
- 239000000779 smoke Substances 0.000 claims description 6
- 239000003480 eluent Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 238000002955 isolation Methods 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims description 2
- 241000208293 Capsicum Species 0.000 claims 5
- 150000001875 compounds Chemical class 0.000 claims 5
- 244000203593 Piper nigrum Species 0.000 claims 1
- 235000012658 paprika extract Nutrition 0.000 claims 1
- 239000001688 paprika extract Substances 0.000 claims 1
- 238000005096 rolling process Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 6
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 4
- 239000003546 flue gas Substances 0.000 abstract description 4
- 230000000391 smoking effect Effects 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 3
- 239000007789 gas Substances 0.000 abstract description 2
- 239000002304 perfume Substances 0.000 abstract description 2
- 230000002411 adverse Effects 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 239000002085 irritant Substances 0.000 abstract 1
- 231100000021 irritant Toxicity 0.000 abstract 1
- 230000029058 respiratory gaseous exchange Effects 0.000 abstract 1
- 241000722363 Piper Species 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 238000001704 evaporation Methods 0.000 description 5
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000004939 coking Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 235000013355 food flavoring agent Nutrition 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention relates to the application of natural vegetation extractive in tobacco and particularly relates to a quince and hot pepper combined extractive and the usage of the quince and hot pepper combined extractive for serving as a tobacco additive. Quince and hot pepper are adopted as extracting raw materials and polar solvent is taken as an extracting agent so as to carry out extracting reaction, extracted residual products are separated out by adopting a big hole resin column separation technology, then the extracted feed liquid is concentrated to be under an extractum state, the extracting agent is used for re-dissolution, then filtering separation is performed, and obtained feed liquid is the extractive provided by the invention. The extractive provided by the invention can effectively enhance flavor during tobacco smoking, has rich perfume, is breathing, and enhances the massive feel of flue gas; and tobacco is endowed with unique odor nuance and note by the quince and hot pepper combined extractive. While the mouthfeel of the tobacco is improved, adverse impacts such as the introduction of miscellaneous gases, increment of irritant activity and the like can be avoided.
Description
Technical field
The present invention relates to a natural plant extract of tobacco products in the application, in particular to a quince and pepper-extract of tobacco products and their use as an additive uses.
Background technology
" Chinese style cigarette " core competitiveness is to form the selling point style, embodies personalization and differentiation, adapts to sucking of Chinese consumers in general and is accustomed to and consumer need.The Chinese style cigarette is Chinese style cigarette product " soul " with essence and flavoring agent, is the secret place that " Chinese style cigarette " style characteristic forms.Flavoring and casing scientifically in cigarette, the important means of the personalized style of outstanding cigarette product just.Simultaneously, in order to improve the security of smoking, lowering harm and decreasing coking becomes an important component part of " Chinese style cigarette ".When reducing coke tar in cigarette, promote and improve flue gas concentration and fragrance, also only by means of the flavoring and casing technology.Along with going deep into of Chinese style cigarette lowering harm and decreasing coking work, reinforced its importance that demonstrates further of tobacco flavoring.From the natural herbal plant, extracting essence and flavoring agent, be used for cigarette to succession Chinese herbal medicine in thousand, let healthy theory along with the refined perfume (or spice) of cigarette, move towards the consumer together, is one of basic research of development " Chinese style cigarette ".
Quince rich in carbohydrates, but also has its own special fragrance unique style, with a prospect of tobacco flavor, but its high content of tannin and pectin, the suction will affect the taste of cigarettes, so that the aroma boring.And contain abundant alkaloid in the capsicum, and alkaloidal reasonable utilization can be regulated the flue gas state, promotes the cigarette quality, but capsicum also can bring strong impulse to the oral cavity.Currently there are no quinces and pepper cigarette additives are used in the literature.And in our study, we found that simply obtained by conventional extraction process separate quince extract or pepper extract, has a negative effect, can not meet the requirements for use as additive cigarette.
Summary of the invention
The object of the present invention is for the deficiencies of the prior art, to provide a complex and peppers quince extract and as additive in tobacco products.
Technical scheme of the present invention is achieved in that it is to adopt to use Wen Quince and capsicum for extracting raw material; With the polar solvent is extractant, carries out abstraction reaction, adopts the macroporous resin column isolation technics will extract byproduct and separates; Again the feed liquid of extracting is concentrated into the medicinal extract shape; Use extractant Hui Rong, isolated by filtration once more, the gained feed liquid is extract of the present invention.
The technical scheme of the present invention are preferred: the extraction agent is a mass percentage of 40 to 95% aqueous ethanol; quince and peppers weight ratio of 5 to 10:1; extractant to extract the reaction and extraction of raw materials the weight ratio of 5 to 10:1
Preparation method of the present invention is: adopt and use Wen Quince and capsicum for extracting raw material, may further comprise the steps: extractant is 5～10: 1 with the weight ratio of extracting raw material, extracts 1～5 hour at 50～90 ℃; After isolating feed liquid; Feed liquid is concentrated into 1/6 of original volume, and with AB-8 macroreticular resin separation concentrated solution, the eluent of collecting ethanol mass percent concentration 50-60% is concentrated into the medicinal extract shape; Return molten medicinal extract with 5～10 times of extractants; The isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more, promptly obtains Wen Quince and the capsicum composite extract of Ben Faming.
The preparation method of the present invention, preferred are: peppers quince and the weight ratio of 5 to 10:1.Described extractant is that mass percent is 40～95% ethanol water.
The invention relates to the use of additives in tobacco products, it is the quinces and pepper-extract added to cigarette tobacco that is added to tobacco in the quinces and pepper-extract tobacco accounted for 0.01% by weight to 0.05%, in tobacco products suction effectively when flavoring and aroma rich, through the hair, increasing the flue gas solid sense.Which is added to tobacco in the quinces and pepper-extract is preferably 0.02% by weight of the tobacco accounted for ~ 0.04%.
As the present invention is the use of additives in tobacco products, preferably quince and pepper-extract dissolved in 70% ethanol, the solution of complex and peppers quince extract ethanol was produced in the cigarette tobacco roll during spraying In tobacco, followed by evaporation of the solvent.
A series of patent applicants the smoking test results show that the addition of quince and pepper-extract when smoked tobacco products can effectively flavor and rich aroma, through the hair, thick smoke increased sense; and quinces quince and pepper-extract of tobacco products can also be given a unique fragrance reconcile nuances.And when improving the tobacco product mouthfeel, can avoid introducing negative effects such as assorted gas, increase excitant.
The present invention quinces and chilli extract complex opened up a new field of application, increasing the quinces and chilli new force and effect.Wen Quince and capsicum composite extract are as additive of tobacco product, and effect is obvious, and " Chinese style cigarette " goods of developing characteristic style are had good application prospects.
The specific embodiment
Through embodiment the present invention is done further explanation below.
Embodiment 1
Using the mass percentage of 95% aqueous ethanol as the extraction agent, the extraction of raw materials and peppers quince 10:1 weight ratio mixture.Extractant is 10: 1 with the weight ratio of extracting raw material, extracts 3 hours at 90 ℃, isolate feed liquid after; Feed liquid is concentrated into 1/6 of original volume; With AB-8 macroreticular resin separation concentrated solution, the eluent of collecting ethanol mass percent concentration 50-60% is concentrated into the medicinal extract shape, and using 10 times of weight, mass percents is that 95% ethanol water returns molten medicinal extract; Isolated by filtration byproduct once more; Feed liquid is concentrated into the medicinal extract shape once more, and the relative density of medicinal extract is 1.1, promptly obtains Wen Quince and the capsicum composite extract of Ben Faming.This extract can be used for additive of tobacco product.Is added in tobacco and pepper quinces complex extracts accounted for 0.04% of the weight of tobacco, tobacco products effectively when suction flavoring and aroma rich, through the hair, increasing a sense of thick smoke.Preferably Wen Quince and capsicum composite extract are dissolved in 70% the ethanol, roll and be sprayed in the process on the pipe tobacco dissolving alcohol solvent that Wen Quince and capsicum composite extract are arranged pipe tobacco, subsequently evaporating solvent in production of cigarettes.
Embodiment 2
Using the mass percentage of 40% aqueous ethanol as an extraction agent, extraction of raw materials and peppers quince 5:1 weight ratio mixture.Extractant is 8: 1 with the weight ratio of extracting raw material, extracts 4 hours at 50 ℃, isolate feed liquid after; Feed liquid is concentrated into 1/6 of original volume, and with AB-8 macroreticular resin separation concentrated solution, the eluent of collecting ethanol mass percent concentration 50-60% is concentrated into the medicinal extract shape; Relative density is 1.3; Using 8 times of weight, mass percents is that 40% ethanol water returns molten medicinal extract, and the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more; The relative density of medicinal extract is 1.3, promptly obtains Wen Quince and the capsicum composite extract of Ben Faming.This extract can be used for additive of tobacco product.Is added in tobacco and pepper quinces complex extracts accounted for 0.02% of the weight of tobacco, tobacco products effectively when suction flavoring and aroma rich, through the hair, increasing a sense of thick smoke.Preferably Wen Quince and capsicum composite extract are dissolved in 70% the ethanol, roll and be sprayed in the process on the pipe tobacco dissolving alcohol solvent that Wen Quince and capsicum composite extract are arranged pipe tobacco, subsequently evaporating solvent in production of cigarettes.
Embodiment 3
Using the mass percentage of 75% aqueous ethanol as an extraction agent, extraction of raw materials and peppers quince 8:1 weight ratio mixture.Extractant is 10: 1 with the weight ratio of extracting raw material, extracts 2 hours at 60 ℃, isolate feed liquid after; Feed liquid is concentrated into 1/6 of original volume, and with AB-8 macroreticular resin separation concentrated solution, the eluent of collecting ethanol mass percent concentration 50-60% is concentrated into the medicinal extract shape; Relative density is 1.2; Using 5 times of weight, mass percents is that 75% ethanol water returns molten medicinal extract, and the isolated by filtration byproduct is concentrated into the medicinal extract shape once more with feed liquid once more; The relative density of medicinal extract is 1.2, promptly obtains Wen Quince and the capsicum composite extract of Ben Faming.This extract can be used for additive of tobacco product.Is added in tobacco and pepper quinces composite extract ratio of 0.05% by weight of tobacco, tobacco products effectively when suction flavoring and aroma rich, through the hair, increasing a sense of thick smoke.Preferably Wen Quince and capsicum composite extract are dissolved in 70% the ethanol, roll and be sprayed in the process on the pipe tobacco dissolving alcohol solvent that Wen Quince and capsicum composite extract are arranged pipe tobacco, subsequently evaporating solvent in production of cigarettes.
Embodiment 4 adds the extract that is obtained in the pipe tobacco of cigarette
Extract rolled in the pipe tobacco of production of cigarettes add pipe tobacco in the process.Is added to the shredded tobacco and peppers complex quince extract, representing 0.03% of the weight of the tobacco.The specific method is to first quince and pepper-extract was dissolved in ethanol, the solution of complex and peppers quince extract uniformly sprayed on tobacco dilute ethanol, followed by evaporation of ethanol.Pipe tobacco rolls into test sample cigarette through cigarette machine.
Effect experiment in embodiment 5 cigarette smokes
Take at a temperature of 22 ℃ ± 1 ℃ and relative humidity (RH) 60% ± 2% under 40 grams of tobacco product equilibrated in duplicate 0.04% of its mass weighed quinces and pepper-extract with 70% ethanol After dilution with throat spray nozzle evenly on tobacco, flavored and unregulated cigarettes silk sample was placed in temperature 22 ℃ ± 1 ℃ and RH60% ± 2% of the equilibrium constant temperature and humidity chamber for 48 hours, with a cigarette lighter to fill respectively, flavored and non-flavored cigarettes made from tobacco, and then at 22 ℃ ± 1 ℃ and RH60% ± 2% equilibrated for 48 hours, please cigarettes sensory evaluation panel evaluated suck.
Staff agreed that the smoking join quinces and pepper-extract when smoked tobacco products can effectively flavor and rich aroma, through the hair, thick smoke increased sense; and quinces and pepper extracts can also be complex gives a unique fragrant cigarette reconcile nuances.
Claims (10)
1. Wen Quince and capsicum composite extract, it is to adopt to use Wen Quince and capsicum for the extraction raw material, is extractant with the polar solvent; Carry out abstraction reaction; Adopt the macroporous resin column isolation technics will extract byproduct and separate, again the feed liquid of extracting is concentrated into the medicinal extract shape, use extractant Hui Rong; Isolated by filtration once more, the gained feed liquid is extract of the present invention.
(2) as claimed in claim 1, wherein the compound and peppers quince extract, wherein the extraction agent is a mass percentage of 40 to 95% aqueous ethanol.
3 according to claim 1, wherein the compound and peppers quince extract, quince and peppers wherein the weight ratio of 5 to 10:1.
As claimed in claim 1, wherein the compound and peppers quince extract, wherein the extraction agent and the reaction is extracted raw material for extraction in a weight ratio of 5 to 10:1.
5. the method for distilling of Wen Quince and capsicum composite extract, it is adopted and uses Wen Quince and capsicum is to extract raw material, may further comprise the steps: extractant is 5～10: 1 with the weight ratio of extraction raw material; Extracted 1～5 hour at 50～90 ℃, isolate feed liquid after, feed liquid is concentrated into 1/6 of original volume; With AB-8 macroreticular resin separation concentrated solution; The eluent of collecting ethanol mass percent concentration 50-60% is concentrated into the medicinal extract shape, returns molten medicinal extract with 5～10 times of extractants, once more the isolated by filtration byproduct; Feed liquid is concentrated into the medicinal extract shape once more, promptly obtains Wen Quince and the capsicum composite extract of Ben Faming.
As claimed in claim 5 and peppers quince extract complex extraction method and peppers quince wherein the weight ratio of 5 to 10:1.
As claimed in claim 5, wherein the compound quince extract and paprika extract, wherein the extraction agent is a mass percentage of 40 to 95% aqueous ethanol.
8 A complex quinces and pepper extracts as the use of additives in tobacco products, it is the quinces and pepper-extract added to cigarette tobacco that is added to tobacco in the quinces and pepper-extract accounted for the weight of tobacco 0.01% to 0.05%, while the suction of tobacco products can effectively flavor and rich aroma, through the hair, increasing a sense of thick smoke.
As claimed in claim 8 and peppers complex quince extract of tobacco products as an additive, wherein the tobacco is added and peppers complex quince tobacco extract ratio by weight of from 0.02% to 0.04%.
A process according to claim 8 quince and pepper-extract of tobacco products as an additive, wherein the compound and peppers quince extract dissolved in 70% ethanol, the solution of complex and peppers quince extract ethanol solvent in the production of tobacco cigarette rolling tobacco on spraying process.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110104882.2A CN102754904B (en) | 2011-04-25 | 2011-04-25 | Quince and hot pepper combined extractive and usage thereof for serving as tobacco additive |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110104882.2A CN102754904B (en) | 2011-04-25 | 2011-04-25 | Quince and hot pepper combined extractive and usage thereof for serving as tobacco additive |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102754904A true CN102754904A (en) | 2012-10-31 |
| CN102754904B CN102754904B (en) | 2014-10-29 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201110104882.2A Active CN102754904B (en) | 2011-04-25 | 2011-04-25 | Quince and hot pepper combined extractive and usage thereof for serving as tobacco additive |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104997158A (en) * | 2015-05-29 | 2015-10-28 | 湖北中烟工业有限责任公司 | Preparation method and application of spicy tobacco flavor extract product |
| RU2590123C1 (en) * | 2015-04-10 | 2016-07-10 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| RU2593106C1 (en) * | 2015-04-10 | 2016-07-27 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| RU2593102C1 (en) * | 2015-04-20 | 2016-07-27 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| RU2594203C1 (en) * | 2015-05-20 | 2016-08-10 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| RU2599355C1 (en) * | 2015-05-20 | 2016-10-10 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Кубанский государственный технологический университет" | Method for production of hookah smoking composition |
| CN113679088A (en) * | 2021-09-08 | 2021-11-23 | 湖北中烟工业有限责任公司 | Preparation method of tobacco shreds with spicy taste in oral cavity |
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| CN101619028A (en) * | 2009-06-17 | 2010-01-06 | 张鹏 | Method for preparing capsicine monomer |
| CN101683182A (en) * | 2008-09-27 | 2010-03-31 | 湖北中烟工业有限责任公司 | Heartleaf houttuynia herb and radix isatidis compound extract and application thereof as additive of tobacco product |
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2011
- 2011-04-25 CN CN201110104882.2A patent/CN102754904B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101683182A (en) * | 2008-09-27 | 2010-03-31 | 湖北中烟工业有限责任公司 | Heartleaf houttuynia herb and radix isatidis compound extract and application thereof as additive of tobacco product |
| CN101619028A (en) * | 2009-06-17 | 2010-01-06 | 张鹏 | Method for preparing capsicine monomer |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2590123C1 (en) * | 2015-04-10 | 2016-07-10 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| RU2593106C1 (en) * | 2015-04-10 | 2016-07-27 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| RU2593102C1 (en) * | 2015-04-20 | 2016-07-27 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| RU2594203C1 (en) * | 2015-05-20 | 2016-08-10 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| RU2599355C1 (en) * | 2015-05-20 | 2016-10-10 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Кубанский государственный технологический университет" | Method for production of hookah smoking composition |
| CN104997158A (en) * | 2015-05-29 | 2015-10-28 | 湖北中烟工业有限责任公司 | Preparation method and application of spicy tobacco flavor extract product |
| CN104997158B (en) * | 2015-05-29 | 2017-01-18 | 湖北中烟工业有限责任公司 | Preparation method and application of spicy tobacco flavor extract product |
| CN113679088A (en) * | 2021-09-08 | 2021-11-23 | 湖北中烟工业有限责任公司 | Preparation method of tobacco shreds with spicy taste in oral cavity |
| CN113679088B (en) * | 2021-09-08 | 2022-05-13 | 湖北中烟工业有限责任公司 | Preparation method of tobacco shreds with spicy taste in oral cavity |
Also Published As
| Publication number | Publication date |
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| CN102754904B (en) | 2014-10-29 |
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