CN102746930B - Grease used specially for sintering machine in metallurgical industry and preparation method thereof - Google Patents
Grease used specially for sintering machine in metallurgical industry and preparation method thereof Download PDFInfo
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- CN102746930B CN102746930B CN201210214194.6A CN201210214194A CN102746930B CN 102746930 B CN102746930 B CN 102746930B CN 201210214194 A CN201210214194 A CN 201210214194A CN 102746930 B CN102746930 B CN 102746930B
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- 239000004519 grease Substances 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 238000005245 sintering Methods 0.000 title abstract description 10
- 239000002199 base oil Substances 0.000 claims abstract description 40
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 28
- 239000003112 inhibitor Substances 0.000 claims abstract description 25
- 238000003756 stirring Methods 0.000 claims abstract description 21
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims abstract description 18
- REYJJPSVUYRZGE-UHFFFAOYSA-N Octadecylamine Chemical compound CCCCCCCCCCCCCCCCCCN REYJJPSVUYRZGE-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims description 29
- 230000003647 oxidation Effects 0.000 claims description 29
- 238000007254 oxidation reaction Methods 0.000 claims description 29
- 230000001050 lubricating effect Effects 0.000 claims description 28
- 239000007866 anti-wear additive Substances 0.000 claims description 24
- 238000007127 saponification reaction Methods 0.000 claims description 12
- 238000005272 metallurgy Methods 0.000 claims description 11
- 239000003921 oil Substances 0.000 claims description 10
- NSOXQYCFHDMMGV-UHFFFAOYSA-N Tetrakis(2-hydroxypropyl)ethylenediamine Chemical compound CC(O)CN(CC(C)O)CCN(CC(C)O)CC(C)O NSOXQYCFHDMMGV-UHFFFAOYSA-N 0.000 claims description 8
- -1 alkenyl succinic acid, Chemical group 0.000 claims description 7
- 150000002148 esters Chemical class 0.000 claims description 5
- 239000002480 mineral oil Substances 0.000 claims description 5
- 235000010446 mineral oil Nutrition 0.000 claims description 5
- 238000007670 refining Methods 0.000 claims description 5
- 229920002367 Polyisobutene Polymers 0.000 claims description 4
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 4
- YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 claims description 4
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 claims description 4
- 239000012964 benzotriazole Substances 0.000 claims description 4
- 238000007599 discharging Methods 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N pentanoic acid group Chemical group C(CCCC)(=O)O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 claims description 4
- WUUHFRRPHJEEKV-UHFFFAOYSA-N tripotassium borate Chemical group [K+].[K+].[K+].[O-]B([O-])[O-] WUUHFRRPHJEEKV-UHFFFAOYSA-N 0.000 claims description 4
- 238000005461 lubrication Methods 0.000 abstract description 5
- 238000000137 annealing Methods 0.000 abstract description 3
- 238000002791 soaking Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 2
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 abstract 2
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 abstract 2
- 239000003963 antioxidant agent Substances 0.000 abstract 2
- 230000003078 antioxidant effect Effects 0.000 abstract 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 abstract 2
- 230000007547 defect Effects 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical group OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 6
- 238000007789 sealing Methods 0.000 description 6
- 239000000084 colloidal system Substances 0.000 description 4
- 238000005086 pumping Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 230000003245 working effect Effects 0.000 description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 3
- 239000000428 dust Substances 0.000 description 3
- 239000000344 soap Substances 0.000 description 3
- 239000001384 succinic acid Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 230000000903 blocking effect Effects 0.000 description 2
- 238000004939 coking Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910021645 metal ion Inorganic materials 0.000 description 2
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000005554 pickling Methods 0.000 description 1
- 238000012019 product validation Methods 0.000 description 1
- 230000001846 repelling effect Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Landscapes
- Lubricants (AREA)
Abstract
The invention discloses grease used specially for a sintering machine in a metallurgical industry and a preparation method thereof. The grease used specially for a sintering machine comprises: by weight, 3 to 6% of octadecylamine, 2 to 5% of aniline, 1 to 3% of ethanediamine, 2 to 3% of diphenylmethane-4,4'-diisocyanate (MDI), 50 to 70% of base oil A, 20 to 30% of base oil B, 0.5 to 1% of an antioxidant A, 2 to 4% of an antioxidant B, 1 to 2% of a rust inhibitor A, 2 to 3% of a rust inhibitor B, 2 to 5% of an extreme-pressure anti-wear agent A, 2 to 4% of an extreme-pressure anti-wear agent B, and 10 to 20% of a tackifier. In preparation, the raw materials are mixed by stirring in a certain order according to different temperatures and then are treated by related processes. The grease used specially for a sintering machine overcomes defects of the existing grease and is suitable for lubrication of bearings at different positions of an elastic slide of a large-scale sintering machine in a metallurgical industry and for lubrication of other high-temperature devices such as a soaking pit furnace, an annealing furnace and a drying furnace.
Description
Technical field
The present invention relates to lubricating grease field, be specifically related to a kind of lubricating grease that is exclusively used in metallurgy industry sinter machine and preparation method thereof.
Background technology
The sintering work Production Flow Chart of sinter machine is longer, and equipment is comparatively numerous and diverse, adds that it,, in special working conditions such as high temperature, many dirt, heavy duty and sour gas environment, makes it quite harsh to the requirement of lubricating grease.The sintering work of sinter machine is to realize by high negative pressure operation, and the aeroseal sheet of sinter machine has deadweight and elastic force, under pressure, produces wearing and tearing and distortion, thereby on contact surface, produce gap owing to sliding, and causes gas leakage.This phenomenon is except outside the Pass having with physical construction, and also the factor such as the temperature in sintering process (temperature of sealing element is up to 200 DEG C of left and right) and raw material, agglomerate dust is relevant with agglomerate.Under high temperature lubricating grease softening, flow out and cause for fat fault bad for fat, and dust is sneaked into the poor sealing that causes etc. and all can be accelerated the inordinate wear of hermetic unit.
Seal device of sintering machine is generally supplied with for fat device by automatic with lubricating grease, current considerable smelter adopts traditional soap base class lubricating grease, but the high-temperature behavior of this class lubricating grease is poor, easily softening loss, contact surface produces gap, pressure reduction destroys the sealed structure that lubricating grease forms, leaks gas, and accelerated wear test, do not reach requirement lubricated and sealing, and soap base class lubricating grease metal ion, at high temperature easy coking and blocking pipeline, pumping is poor.Cause air leak rate of air curtain large so in use find bad lubricating, slideway serious wear, production efficiency is low, it is reported, the maximum air leak rate of air curtain of external sinter machine is no more than 30%, and the air leak rate of air curtain of the sinter machine of domestic current running is generally 40-60%, except will improving equipment, also need to strengthen the improvement to PERFORMANCE OF GREASES.
In recent years, along with China's metallurgy industry develop rapidly, the energy-saving and cost-reducing problem that becomes concern.The lubricating grease that sinter machine is used is not had higher requirement, and sinter machine lubricating grease should have good high-temperature behavior, and vaporization losses reduces, thinning under high temperature, do not run off and not oxidizable, plays good lubricated and sealing function; Require to there is higher supporting capacity and friction resistant performance simultaneously, meet equipment lubricated requirement under many dirt and impact load; There is good barrier propterty, prevent acid attack gas pickling metallic surface; Have good pump-conveying property and low coking tendency, not blocking pipeline, meets and concentrates for grease lubrication system; There is longer work-ing life etc.
Summary of the invention
The object of this invention is to provide lubricating grease being exclusively used in by metallurgy industry sinter machine and preparation method thereof, overcome prior art weak point, product is applicable to the lubricated of the high temperature services such as each position bearing of elastic slideway of metallurgical industry large-type sinterer and other soaking pit, annealing furnace, stoving oven.
The technical solution used in the present invention is as follows:
A kind of lubricating grease that is exclusively used in metallurgy industry sinter machine, the weight percent of the each component of its constitutive material is: stearylamine 3-6%, aniline 2-5%, quadrol 1-3%, MDI 2～3%, base oil A 50～70%, base oil B 20～30%, oxidation inhibitor A 0.5～1%, oxidation inhibitor B2～4%, rust-preventive agent A 1～2%, rust-preventive agent B2～3%, extreme pressure anti-wear additives A 2～5%, extreme pressure anti-wear additives B 2～4%, tackifier 10～20%, described tackifier are low-molecular-weight polyisobutylene.
Described base oil A is the mineral oil 150BS of high viscosity deep refining;
Described base oil B is the synthetic base oil of ester class;
Described oxidation inhibitor A is pentanoic;
Described oxidation inhibitor B is phosphoric acid fourth octyl group zinc salt;
Described rust-preventive agent A is benzotriazole;
Described rust-preventive agent B is alkenyl succinic acid;
Described extreme pressure anti-wear additives A is tritolyl phosphate;
Described extreme pressure anti-wear additives B is potassium borate;
Described preparation method, specifically comprises the following steps:
(1) press formula rate the base oil B of 60% base oil A and 40% is dropped in saponification still, and be warmed up to 60-80 DEG C;
(2) stearylamine of formula rate, aniline, quadrol are put in saponification still and stirred with the mixture of step (1), churning time is 5-10 minute;
(3) by formula rate, the base oil B of 40% base oil A and 60% is put in oil groove, and be warmed up to 70-90 DEG C;
(4) MDI of formula rate is put in oil groove, mix with the mixture of step (3), fully stir until entirely molten;
(5) mixture of step (4) is driven in saponification still, the mixture stirring with step (2) mixes, slowly heat up, require to start temperature at 60-90 DEG C, stir 30-50 minute, then the 1.5-3 hour that at the uniform velocity heats up, stops heat supply when temperature is increased to 160-250 DEG C;
(6) mixture step (5) being stirred is transferred to and is in harmonious proportion in still, in the time that temperature drops to 110-140 DEG C, adds oxidation inhibitor A and tackifier, stirs;
(7), in the time that temperature drops to 80-110 DEG C, oxidation inhibitor B, rust-preventive agent A, rust-preventive agent B, extreme pressure anti-wear additives A, extreme pressure anti-wear additives B are joined and be in harmonious proportion in still, and stir;
(8), by the mixture circulation shear of step (7) after 30-60 minute, under 20-35MPa pressure, homogeneous, degassed, discharging, obtain product.
Application note of the present invention:
Lubricating grease of the present invention is mainly applicable to the lubricated of the high temperature services such as each position bearing of elastic slideway of metallurgical industry large-type sinterer and other soaking pit, annealing furnace, stoving oven, also be applicable to bearing, gear, chain lubricated of various device under excessive temperature, heavy duty, low-speed conditions, as various rotary kilns or the tunnel kiln car bearing etc. of large-scale refractory factory, ceramics factory, electroceramics factory.Applicable temperature :-30 DEG C～220 DEG C
Beneficial effect of the present invention:
1, excellent resistance to elevated temperatures and oxidation stability: dropping point index is one of index directly perceived of its high-temperature behavior of reflection, and this product dropping point can reach more than 300 DEG C, can use under 220 DEG C of Working environments the long period; High-temperature oxidation stability is one of main use properties of lubricating grease, and lubricating grease used and have larger impact.The oxidation stability of lubricating grease is with to prepare grease thickener relevant with basic oil properties, and this product viscosifying agent, because of metal ion not, can be avoided the metal catalytic effect of base oil oxidation under high temperature, so have good high-temperature oxidation resistant stability.
2, excellent colloid stability and pumping: lubricating grease colloid stability is to weigh a tool important indicator of a lubricating grease use properties and shelf characteric quality.This product viscosifying agent is organism, has good affinity with base oil, contains aryl simultaneously, and adds a certain proportion of synthetic ester lubricant, so have excellent colloid stability; Sinter machine centralized lubrication system pumping line is very long, particularly needs in the winter time lubricated product to have good temperature pumping, even if this product, under the condition of-30 DEG C, also can meet the requirement of sinter machine centralized lubrication system.
3, excellent sealing property: not thinning under this product high temperature, do not run off, ferrous metal is kept to good adhesive capacity, under 220 DEG C of Working environments, use noncoking, can not cause slideway wearing and tearing, and water pouring loss is low, water repelling property is good, contacting with water, even mix with water after denseness reduce very littlely, can effectively get sealing function.
4, there is excellent lubricated and extreme pressure and antiwear behavior: the sintering work work low speed high temperature sliding friction of sinter machine, and with a large amount of dust, want to bear larger impact load simultaneously, the mineral oil of the high viscosity deep refining that this product is selected, under high loading, still can well form excellent oil film thickness, test shows, P
bmore than reaching 1000N, P
dmore than reaching 6000N.
5, the work-ing life of overlength: the high-temperature behavior of lubricating grease refers to lubricating grease bearing life at high temperature, the reflection of lubricating grease Integrated using performance, the level of the fundamental propertys such as colloid stability, mechanical stability and oxidation stability that can constitutionally reflection lubricating grease.This product is at the temperature of 160 DEG C, life-span reaches 1000 hours above (test method ASTM D 3336), there is good bearing working ability, there is longer work-ing life, be the more than 10 times of general soap base grease its work-ing life, therefore has high economic worth and use value.
Embodiment
Embodiment mono-: a kind of lubricating grease that is exclusively used in metallurgy industry sinter machine, the weight percent of the each component of its constitutive material is: stearylamine 3%, aniline 2%, quadrol 1%, MDI 2%, base oil A 50%, base oil B 20%, oxidation inhibitor A 0.5%, oxidation inhibitor B2%, rust-preventive agent A 1%, rust-preventive agent B2%, extreme pressure anti-wear additives A 2%, extreme pressure anti-wear additives B 2%, tackifier 12.5%.
Wherein, described base oil A is the mineral oil 150BS of high viscosity deep refining; Described base oil B is the synthetic base oil of ester class; Described oxidation inhibitor A is pentanoic; Described oxidation inhibitor B is phosphoric acid fourth octyl group zinc salt; Described rust-preventive agent A is benzotriazole; Rust-preventive agent B is alkenyl succinic acid; Described extreme pressure anti-wear additives A is tritolyl phosphate; Described extreme pressure anti-wear additives B is potassium borate; Described tackifier are low-molecular-weight polyisobutylene.
The preparation of greases method that is exclusively used in metallurgy industry sinter machine, specifically comprises the following steps:
(1) press formula rate the base oil B of 60% base oil A and 40% is dropped in saponification still, and be warmed up to 60-80 DEG C;
(2) stearylamine of formula rate, aniline, quadrol are put in saponification still and stirred with the mixture of step (1), churning time is 5-10 minute;
(3) by formula rate, the base oil B of 40% base oil A and 60% is put in oil groove, and be warmed up to 70-90 DEG C;
(4) MDI of formula rate is put in oil groove, mix with the mixture of step (3), fully stir until entirely molten;
(5) mixture of step (4) is driven in saponification still, the mixture stirring with step (2) mixes, slowly heat up, require to start temperature at 60-90 DEG C, stir 30-50 minute, then the 1.5-3 hour that at the uniform velocity heats up, stops heat supply when temperature is increased to 160-250 DEG C;
(6) mixture step (5) being stirred is transferred to and is in harmonious proportion in still, in the time that temperature drops to 110-140 DEG C, adds oxidation inhibitor A and tackifier, stirs;
(7), in the time that temperature drops to 80-110 DEG C, oxidation inhibitor B, rust-preventive agent A, rust-preventive agent B, extreme pressure anti-wear additives A, extreme pressure anti-wear additives B are joined and be in harmonious proportion in still, and stir;
(8), by the mixture circulation shear of step (7) after 30-60 minute, under 20-35MPa pressure, homogeneous, degassed, discharging, obtain product.
Embodiment bis-: a kind of lubricating grease that is exclusively used in metallurgy industry sinter machine, the weight percent of the each component of its constitutive material is: stearylamine 4%, aniline 3%, quadrol 1%, MDI 2.5%, base oil A 50%, base oil B 20%, oxidation inhibitor A 0.5%, oxidation inhibitor B2%, rust-preventive agent A 1%, rust-preventive agent B2%, extreme pressure anti-wear additives A 2%, extreme pressure anti-wear additives B 2%, tackifier 12.5%.
Wherein, described base oil A is the mineral oil 150BS of high viscosity deep refining; Described base oil B is the synthetic base oil of ester class; Described oxidation inhibitor A is pentanoic; Described oxidation inhibitor B is phosphoric acid fourth octyl group zinc salt; Described rust-preventive agent A is benzotriazole; Rust-preventive agent B is alkenyl succinic acid; Described extreme pressure anti-wear additives A is tritolyl phosphate; Described extreme pressure anti-wear additives B is potassium borate; Described tackifier are low-molecular-weight polyisobutylene.
The preparation of greases method that is exclusively used in metallurgy industry sinter machine, specifically comprises the following steps:
(1) press formula rate the base oil B of 60% base oil A and 40% is dropped in saponification still, and be warmed up to 60-80 DEG C;
(2) stearylamine of formula rate, aniline, quadrol are put in saponification still and stirred with the mixture of step (1), churning time is 5-10 minute;
(3) by formula rate, the base oil B of 40% base oil A and 60% is put in oil groove, and be warmed up to 70-90 DEG C;
(4) MDI of formula rate is put in oil groove, mix with the mixture of step (3), fully stir until entirely molten;
(5) mixture of step (4) is driven in saponification still, the mixture stirring with step (2) mixes, slowly heat up, require to start temperature at 60-90 DEG C, stir 30-50 minute, then the 1.5-3 hour that at the uniform velocity heats up, stops heat supply when temperature is increased to 160-250 DEG C;
(6) mixture step (5) being stirred is transferred to and is in harmonious proportion in still, in the time that temperature drops to 110-140 DEG C, adds oxidation inhibitor A and tackifier, stirs;
(7), in the time that temperature drops to 80-110 DEG C, oxidation inhibitor B, rust-preventive agent A, rust-preventive agent B, extreme pressure anti-wear additives A, extreme pressure anti-wear additives B are joined and be in harmonious proportion in still, and stir;
(8), by the mixture circulation shear of step (7) after 30-60 minute, under 20-35MPa pressure, homogeneous, degassed, discharging, obtain product.
Product Validation:
After testing, the indices of this product all reaches service requirements.
Claims (2)
1. one kind is exclusively used in the lubricating grease of metallurgy industry sinter machine, it is characterized in that: the weight percent of the each component of its constitutive material is: stearylamine 3-6%, aniline 2-5%, quadrol 1-3%, MDI 2 ~ 3%, base oil A 50 ~ 70%, base oil B 20 ~ 30%, oxidation inhibitor A 0.5 ~ 1%, oxidation inhibitor B2 ~ 4%, rust-preventive agent A 1 ~ 2%, rust-preventive agent B2 ~ 3%, extreme pressure anti-wear additives A 2 ~ 5%, extreme pressure anti-wear additives B 2 ~ 4%, tackifier 10 ~ 20%, described tackifier are low-molecular-weight polyisobutylene; Described base oil A is the mineral oil 150BS of high viscosity deep refining, described base oil B is the synthetic base oil of ester class, described oxidation inhibitor A is pentanoic, described rust-preventive agent A is benzotriazole, described rust-preventive agent B is alkenyl succinic acid, described extreme pressure anti-wear additives A is tritolyl phosphate, and described extreme pressure anti-wear additives B is potassium borate, and the weight percent sum of said components is 100%.
2. a kind of preparation of greases method that is exclusively used in metallurgy industry sinter machine as claimed in claim 1, is characterized in that: described preparation method, specifically comprises the following steps:
(1) press formula rate the base oil B of 60% base oil A and 40% is dropped in saponification still, and be warmed up to 60-80 DEG C;
(2) stearylamine of formula rate, aniline, quadrol are put in saponification still and stirred with the mixture of step (1), churning time is 5-10 minute;
(3) by formula rate, the base oil B of 40% base oil A and 60% is put in oil groove, and be warmed up to 70-90 DEG C;
(4) MDI of formula rate is put in oil groove, mix with the mixture of step (3), fully stir until entirely molten;
(5) mixture of step (4) is driven in saponification still, the mixture stirring with step (2) mixes, slowly heat up, require to start temperature at 60-90 DEG C, stir 30-50 minute, then the 1.5-3 hour that at the uniform velocity heats up, stops heat supply when temperature is increased to 160-250 DEG C;
(6) mixture step (5) being stirred is transferred to and is in harmonious proportion in still, in the time that temperature drops to 110-140 DEG C, adds oxidation inhibitor A and tackifier, stirs;
(7), in the time that temperature drops to 80-110 DEG C, oxidation inhibitor B, rust-preventive agent A, rust-preventive agent B, extreme pressure anti-wear additives A, extreme pressure anti-wear additives B are joined and be in harmonious proportion in still, and stir;
(8), by the mixture circulation shear of step (7) after 30-60 minute, under 20-35MPa pressure, homogeneous, degassed, discharging, obtain product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210214194.6A CN102746930B (en) | 2012-06-27 | 2012-06-27 | Grease used specially for sintering machine in metallurgical industry and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210214194.6A CN102746930B (en) | 2012-06-27 | 2012-06-27 | Grease used specially for sintering machine in metallurgical industry and preparation method thereof |
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| CN102746930A CN102746930A (en) | 2012-10-24 |
| CN102746930B true CN102746930B (en) | 2014-12-10 |
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| CN103497814B (en) * | 2013-09-02 | 2015-07-01 | 安庆市中天石油化工有限公司 | Lubricating grease specially used in high-temperature kiln car, and preparation method thereof |
| CN105087106A (en) * | 2015-08-11 | 2015-11-25 | 新乡市恒星化工有限责任公司 | Lubricating grease special for blast-furnace equipment and preparation method thereof |
| CN105861125A (en) * | 2016-04-19 | 2016-08-17 | 天津海航石油能源科技有限公司 | Anti-corrosion lubricating grease for unbonded prestressed ribs and preparation method of anti-corrosion lubricating grease |
| JP6841547B2 (en) * | 2017-01-18 | 2021-03-10 | 出光興産株式会社 | Grease composition and its manufacturing method |
| CN107760425A (en) * | 2017-11-15 | 2018-03-06 | 郑州市欧普士科技有限公司 | A kind of long-life bearing lubricating grease and preparation method thereof |
| CN109762629A (en) * | 2018-12-19 | 2019-05-17 | 无锡飞天润滑油科技股份有限公司 | A kind of sintering machine slide way packing grease and preparation method thereof |
| CN111057609A (en) * | 2019-12-10 | 2020-04-24 | 融润化工科技有限公司 | High dropping point extreme pressure drilling tool thread grease |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101693851A (en) * | 2009-09-30 | 2010-04-14 | 中国石油化工股份有限公司 | Synthetic high-temperature lubricating grease and production method thereof |
| CN102311850A (en) * | 2011-08-04 | 2012-01-11 | 安庆市中天石油化工有限公司 | Grease specially used for heavy-load open-type gear and preparation method thereof |
| CN102417847A (en) * | 2011-10-17 | 2012-04-18 | 中国石油化工股份有限公司 | Lubricating grease composition |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6667281B2 (en) * | 2000-10-06 | 2003-12-23 | Nippon Oil Corporation | Grease composition |
-
2012
- 2012-06-27 CN CN201210214194.6A patent/CN102746930B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101693851A (en) * | 2009-09-30 | 2010-04-14 | 中国石油化工股份有限公司 | Synthetic high-temperature lubricating grease and production method thereof |
| CN102311850A (en) * | 2011-08-04 | 2012-01-11 | 安庆市中天石油化工有限公司 | Grease specially used for heavy-load open-type gear and preparation method thereof |
| CN102417847A (en) * | 2011-10-17 | 2012-04-18 | 中国石油化工股份有限公司 | Lubricating grease composition |
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| Publication number | Publication date |
|---|---|
| CN102746930A (en) | 2012-10-24 |
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Address after: 246521 Susong Economic Development Zone, Anhui, Anqing Patentee after: ANHUI ZHONG TIAN PETROCHEMICAL Co.,Ltd. Address before: 246521 Susong County Industrial Park, Anhui, Anqing Patentee before: ANQING ZHONGTIAN PETROLEUM CHEMICAL INDUSTRY Co.,Ltd. |
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Denomination of invention: A lubricating grease specially used for sintering machine in metallurgical industry and its preparation method Effective date of registration: 20200729 Granted publication date: 20141210 Pledgee: Susong sub branch of China Construction Bank Corp. Pledgor: ANHUI ZHONG TIAN PETROCHEMICAL Co.,Ltd. Registration number: Y2020980004498 |
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Denomination of invention: A lubricating grease specially used for sintering machine in metallurgical industry and its preparation method Effective date of registration: 20220930 Granted publication date: 20141210 Pledgee: Susong sub branch of China Construction Bank Corp. Pledgor: ANHUI ZHONG TIAN PETROCHEMICAL Co.,Ltd. Registration number: Y2022980017334 |