CN102719866A - Cleaning and activating complex agent before plating of stainless steel parts and production process of cleaning and activating complex agent - Google Patents

Cleaning and activating complex agent before plating of stainless steel parts and production process of cleaning and activating complex agent Download PDF

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Publication number
CN102719866A
CN102719866A CN2012101910382A CN201210191038A CN102719866A CN 102719866 A CN102719866 A CN 102719866A CN 2012101910382 A CN2012101910382 A CN 2012101910382A CN 201210191038 A CN201210191038 A CN 201210191038A CN 102719866 A CN102719866 A CN 102719866A
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China
Prior art keywords
weighing
solution
cleaning
add
stainless steel
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CN2012101910382A
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Chinese (zh)
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刘贯军
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Henan Institute of Science and Technology
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Henan Institute of Science and Technology
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Priority to CN2012101910382A priority Critical patent/CN102719866A/en
Publication of CN102719866A publication Critical patent/CN102719866A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a cleaning and activating complex agent before plating of stainless steel parts. The cleaning and activating complex agent comprises kerosene, concentrated hydrochloric acid, sodium tripolyphosphate, OP-10 emulsifiers, water glass and lauryl sodium sulfate. A production process of the cleaning and activating complex agent includes: (1) weighing the concentrated hydrochloric acid, and diluting the weighed concentrated hydrochloric acid by distilled water; (2) weighing the sodium tripolyphosphate, and adding the weighed sodium tripolyphosphate into the diluted hydrochloric acid obtained at the step (1); (3) weighing the water glass, and adding the weighed water glass into solution formed at the step (2); (4) weighing the OP-10 emulsifiers, and adding the weighed OP-10 emulsifiers into solution formed at the step (3); (5) weighing the lauryl sodium sulfate, and adding the weighed lauryl sodium sulfate into solution formed at the step (4); (6) weighing the kerosene, and adding the weighed kerosene into solution formed at the step (5); and (7) adding a proper amount of the distilled water into solution formed at the step (6) to enable the solution to be 1000ml so as to complete preparation. The cleaning and activating complex agent before plating of the stainless steel parts is convenient to process, good in use effects and capable of meeting the requirements on cleaning and activating of the stainless steel parts before plating.

Description

Clean activation recombiner and production technique thereof before a kind of stainless steel part plating
Technical field:
The present invention relates to the stainless steel part plating process, particularly a kind of being applicable to cleaned before the stainless steel part plating, cleaned the activation recombiner before the plating of activatory stainless steel part.
Background technology:
At present, for anti-corrosion, wear resisting property and the aesthetic that further improves Stainless Steel Products, to carry out the chemical nickel plating processing particularly stainless steel stretched of Stainless Steel Products as the thermos cup etc.Oil removing, rust cleaning and activation are that metallochemistry plates indispensable pre-treating technology; And oil removing, rust cleaning and activatory reagent are a lot; With triplicity also having together, but all low because of processing efficiency, discharge not environmental protection, clean reasons such as cost height, its result of use is not satisfactory; And then influence stainless steel stretched coating effect, bring a lot of inconvenience for stainless steel stretched processing.
Summary of the invention:
Clean activation recombiner and production technique thereof before the purpose of this invention is to provide the good stainless steel part plating of a kind of result of use.
Technical scheme of the present invention is; Clean the activation recombiner before a kind of stainless steel part plating, it is characterized in that: in every liter of solution that configures, contain: kerosene 50-200g/L, concentrated hydrochloric acid 50-200g/L; Tripoly phosphate sodium STPP 50-200g/L; OP-10 emulsifying agent 20-60g/L, water glass 10-80g/L, sodium lauryl sulphate 10-50g/L.Said concentrated hydrochloric acid is industrial concentrated hydrochloric acid.The production technique of cleaning the activation recombiner before the plating of a kind of stainless steel part is characterized in that: (1) with taking by weighing concentrated hydrochloric acid 50-200g, and use the 200ml distilled water diluting; (2) take by weighing tripoly phosphate sodium STPP 50-200g, add in (1) Hydrogen chloride in step, be stirred to dissolving with glass stick; (3) take by weighing water glass 10-80g, add in the solution of (2) step formation, be stirred to dissolving with glass stick; (4) take by weighing OP-10 emulsifying agent 20-60g, add in the solution of (3) step formation, be stirred to dissolving with glass stick; (5) take by weighing sodium lauryl sulphate 10-50g, add in the solution of (4) step formation, be stirred to dissolving with glass stick; (6) take by weighing kerosene 50-200g, add in the solution of (5) step formation, be stirred to dissolving with glass stick; (7) add in the solution of an amount of zero(ppm) water to (6) step formation, make this solution become 1000ml, accomplish preparation.
The present invention is easy to process, and result of use is better, can satisfy the preceding needs of living that clean of stainless steel part plating.
Embodiment:
Describe embodiment in detail:
Embodiment one:
(1), and uses the 200ml distilled water diluting with taking by weighing industrial concentrated hydrochloric acid 50g; (2) take by weighing tripoly phosphate sodium STPP 200g, add in (1) Hydrogen chloride in step, be stirred to dissolving with glass stick; (3) take by weighing water glass 10g, add in the solution of (2) step formation, be stirred to dissolving with glass stick; (4) take by weighing OP-10 emulsifying agent 20g, add in the solution of (3) step formation, be stirred to dissolving with glass stick; (5) take by weighing sodium lauryl sulphate 50g, add in the solution of (4) step formation, be stirred to dissolving with glass stick; (6) take by weighing kerosene 100g, add in the solution of (5) step formation, be stirred to dissolving with glass stick; (7) add in the solution of an amount of zero(ppm) water to (6) step formation, make this solution become 1000ml, accomplish preparation.
Embodiment two:
(1), and uses the 200ml distilled water diluting with taking by weighing industrial concentrated hydrochloric acid 100g; (2) take by weighing tripoly phosphate sodium STPP 50g, add in (1) Hydrogen chloride in step, be stirred to dissolving with glass stick; (3) take by weighing water glass 80g, add in the solution of (2) step formation, be stirred to dissolving with glass stick; (4) take by weighing OP-10 emulsifying agent 60g, add in the solution of (3) step formation, be stirred to dissolving with glass stick; (5) take by weighing sodium lauryl sulphate 10g, add in the solution of (4) step formation, be stirred to dissolving with glass stick; (6) take by weighing kerosene 50g, add in the solution of (5) step formation, be stirred to dissolving with glass stick; (7) add in the solution of an amount of zero(ppm) water to (6) step formation, make this solution become 1000ml, accomplish preparation.
Embodiment three:
(1), and uses the 200ml distilled water diluting with taking by weighing concentrated hydrochloric acid 200g; (2) take by weighing tripoly phosphate sodium STPP 100g, add in (1) Hydrogen chloride in step, be stirred to dissolving with glass stick; (3) take by weighing water glass 30g, add in the solution of (2) step formation, be stirred to dissolving with glass stick; (4) take by weighing OP-10 emulsifying agent 40g, add in the solution of (3) step formation, be stirred to dissolving with glass stick; (5) take by weighing sodium lauryl sulphate 40g, add in the solution of (4) step formation, be stirred to dissolving with glass stick; (6) take by weighing kerosene 200g, add in the solution of (5) step formation, be stirred to dissolving with glass stick; (7) add in the solution of an amount of zero(ppm) water to (6) step formation, make this solution become 1000ml, accomplish preparation.
Embodiment four:
(1), and uses the 200ml distilled water diluting with taking by weighing concentrated hydrochloric acid 120g; (2) take by weighing tripoly phosphate sodium STPP 140g, add in (1) Hydrogen chloride in step, be stirred to dissolving with glass stick; (3) take by weighing water glass 70g, add in the solution of (2) step formation, be stirred to dissolving with glass stick; (4) take by weighing OP-10 emulsifying agent 35g, add in the solution of (3) step formation, be stirred to dissolving with glass stick; (5) take by weighing sodium lauryl sulphate 25g, add in the solution of (4) step formation, be stirred to dissolving with glass stick; (6) take by weighing kerosene 150g, add in the solution of (5) step formation, be stirred to dissolving with glass stick; (7) add in the solution of an amount of zero(ppm) water to (6) step formation, make this solution become 1000ml, accomplish preparation.
  
Experimental example:
Use compound formula preparation 2000ml recombiner solution of the present invention; Put into the stainless steel thermos cup after the drawn that is coated with full drawing oil also welds; And clean the ultrasonic cleaner normal temperature that the beaker of splendid attire recombiner solution and thermos cup is put into 40KHz after 1 minute (if therebetween suitably turning workpieces better effects if) and take out, in clear water, rinse (about 0.5 minute) well after, put into chemical plating fluid; Begin to take place electroless plating reaction after half a minute approximately, the coating effect is comparatively desirable.
Tooling cost of the present invention is lower, and the discharging compliance with environmental protection requirements is better to the plating pre-treatment effect of stainless steel part.

Claims (3)

1. clean the activation recombiner before a stainless steel part plating; It is characterized in that: in every liter of solution that configures, contain: kerosene 50-200g/L; Concentrated hydrochloric acid 50-200g/L, tripoly phosphate sodium STPP 50-200g/L, OP-10 emulsifying agent 20-60g/L; Water glass 10-80g/L, sodium lauryl sulphate 10-50g/L.
2. clean the activation recombiner before a kind of stainless steel part plating as claimed in claim 1, it is characterized in that: said concentrated hydrochloric acid is industrial concentrated hydrochloric acid.
3. the production technique of cleaning the activation recombiner before the stainless steel part plating is characterized in that: (1) with taking by weighing concentrated hydrochloric acid 50-200g, and use the 200ml distilled water diluting; (2) take by weighing tripoly phosphate sodium STPP 50-200g, add in (1) Hydrogen chloride in step, be stirred to dissolving with glass stick; (3) take by weighing water glass 10-80g, add in the solution of (2) step formation, be stirred to dissolving with glass stick; (4) take by weighing OP-10 emulsifying agent 20-60g, add in the solution of (3) step formation, be stirred to dissolving with glass stick; (5) take by weighing sodium lauryl sulphate 10-50g, add in the solution of (4) step formation, be stirred to dissolving with glass stick; (6) take by weighing kerosene 50-200g, add in the solution of (5) step formation, be stirred to dissolving with glass stick; (7) add in the solution of an amount of zero(ppm) water to (6) step formation, make this solution become 1000ml, accomplish preparation.
CN2012101910382A 2012-06-12 2012-06-12 Cleaning and activating complex agent before plating of stainless steel parts and production process of cleaning and activating complex agent Pending CN102719866A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109748267A (en) * 2019-02-21 2019-05-14 苏州市安派精密电子有限公司 A kind of graphene thermal component preparation method based on multiple tracks cleaning
CN113622007A (en) * 2021-09-08 2021-11-09 苏州市安派精密电子有限公司 Preparation method of high-flexibility graphite or graphene heat dissipation component

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA903647A (en) * 1972-06-27 Burden Peter Cleaning composition and process
CN1034589A (en) * 1988-01-30 1989-08-09 高占祥 The preparation and the application thereof of low temperature rust cleaning liquid fast
CN101225522A (en) * 2008-02-15 2008-07-23 重庆大学 Metal deoiling cleaning agent and deoiling method thereof
CN102021589A (en) * 2010-12-18 2011-04-20 江苏德美科技有限公司 Acidic normal temperature degreasing agent and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA903647A (en) * 1972-06-27 Burden Peter Cleaning composition and process
CN1034589A (en) * 1988-01-30 1989-08-09 高占祥 The preparation and the application thereof of low temperature rust cleaning liquid fast
CN101225522A (en) * 2008-02-15 2008-07-23 重庆大学 Metal deoiling cleaning agent and deoiling method thereof
CN102021589A (en) * 2010-12-18 2011-04-20 江苏德美科技有限公司 Acidic normal temperature degreasing agent and preparation method thereof

Non-Patent Citations (4)

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Title
余存烨: "表面活性剂在化学清洗中的应用", 《石油化工腐蚀与防护》 *
姜力强等: "盐酸酸洗液防蚀抑雾剂的研究", 《 腐蚀科学与防护技术》 *
张安富: "盐酸介质中表面活性剂对碳钢缓蚀作用的研究", 《表面技术》 *
王文忠: "浅谈表面活性剂与金属水基脱脂清洗", 《电镀与环保》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109748267A (en) * 2019-02-21 2019-05-14 苏州市安派精密电子有限公司 A kind of graphene thermal component preparation method based on multiple tracks cleaning
CN113622007A (en) * 2021-09-08 2021-11-09 苏州市安派精密电子有限公司 Preparation method of high-flexibility graphite or graphene heat dissipation component

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Application publication date: 20121010