CN102677485A - Method for dyeing real silk with Juglandaceae vegetable dye - Google Patents
Method for dyeing real silk with Juglandaceae vegetable dye Download PDFInfo
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- CN102677485A CN102677485A CN2012101664782A CN201210166478A CN102677485A CN 102677485 A CN102677485 A CN 102677485A CN 2012101664782 A CN2012101664782 A CN 2012101664782A CN 201210166478 A CN201210166478 A CN 201210166478A CN 102677485 A CN102677485 A CN 102677485A
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Abstract
The invention discloses a method for dyeing real silk with a Juglandaceae vegetable dye, which is used for carrying out direct dyeing or pre-mordant dyeing on the real silk with the Juglandaceae vegetable dye. The direct dyeing process comprises the following steps: adding the Juglandaceae vegetable dye of which the mass is 10 percent to 50 percent of that of the real silk onto the real silk to carry out dyeing, wherein the bath ratio, i.e. the weight ratio of the real silk to dyeing liquor, is 1:1 to 1:150; carrying out dip dyeing for a certain time or slowly heating; then cooling at room temperature; and taking out the dyed real silk, washing the real silk with water and air-drying the real silk. According to the invention, the natural and nontoxic Juglandaceae vegetable dye is used for dyeing the real silk, so that not only the dyeing chromatograph of the Juglandaceae vegetable dye is improved, but also the application of a synthetic dye to the real silk is reduced, the technical basis is provided for developing the natural dye and meanwhile the basis is provided for really implementing the industrial large-scale production and the high efficient circulating utilization of the agricultural resources.
Description
Technical field
What the present invention relates to is the method in a kind of printing technology field, specifically is a kind of method of utilizing juglandaceae plant dyestuff dyeing silk.
Background technology
Synthesize along with banning use of of the continuous development of environmental protection health dyestuff theory, particularly implementation abroad is poisonous under the actively promoting of green movements such as dying, the vegetable colour of green health more and more receives people's attention.
Juglandaceae (Juglandaceae) plant is a section of Dicotyledoneae Hamamelidae Hamamelididae, fallen leaves or half evergreen or aiphyllium, and wherein various plants has the cultivation history in more than 2,000 year in this section.This section's plant timber is hard, is hardwood seeds preferably, can make implements, and most kinds are rich in tannin, is the raw material that extracts tannin, the general oil-containing of seed.The whole world has 9 to belong to 72 kinds, is interrupted being distributed in Eurasia and America, with SOUTHERN CHINA to South East Asia Mainland and southern US to Central America most species.Modern medicine study is thought, the phosphatide in the juglandaceae plant has the good health care effect to cranial nerve, and unrighted acid has the arteriosclerotic effect of control.Also contain the indispensable elements of human body such as zinc, manganese, chromium in the juglandaceae plant.According to data record both domestic and external, the leaf of part juglandaceae plant, branch, rascal or bark all have certain medical value, and have effects such as sterilization, sterilization, diuresis, nourishing, detoxifcation, desinsection.
Through existing technical literature retrieval is found; Publication number is the patent of invention of 102321983A; Provide " a kind of method of utilizing alkannin printing and dyeing real silk, this method comprises the steps: 1) preparation alkannin extract: light violet grass is cleaned, cuts off, dried, and the Asian puccoon that will dry then is according to mixing with 1: 10 proportioning of mass ratio of water; heated and boiled 2 hours, extracts to obtain required dye liquor; 2) preparation mordant: raw material is selected a kind of in ferric sulfate, aluminum sulfate, the nickelous sulfate for use, and sodium carbonate particle and water, and according to 1: 8: 150 Hybrid Heating of weight ratio, temperature is controlled at 65 ℃, and the time is 30 minutes, and room temperature cooling back is subsequent use; 3) dyeing: before silk drops into the alkannin dye liquor, carry out preliminary treatment with mordant; Also can in alkannin dye liquor dyeing course, add, also not only preliminary treatment but also in dyeing course, add, the mordant consumption is 1g/l～10g/l; Concrete dyeing is: the Asian puccoon dye liquor concentration is 3g/l～10g/l; Dyeing temperature is 65～85 ℃, and bath raio is 1: 30～50, and dyeing time is 40～90 minutes; 4) post processing: comprise cleaning, dehydration, make through mechanical finishing again.”
Patent publication No. is China's invention application of 102153883A; This patent provide " a kind of woolen dyed technical field utilize the walnut plant as the preparation and the application of wool dye; through the broken end of walnut plant is extracted down after after the vacuum water-bath concentrates at 10-150 ℃; obtain walnut powdery concentrate, i.e. the walnut vegetable colour.The present invention utilizes the plant walnut plant of Nantural non-toxic to be used for woolen dyed; For reducing the use of synthetic dyestuffs; The exploitation natural dye provides technical basis, simultaneously, also for the real efficient recycling of large-scale industrialization production and agricultural resource that realizes foundation is provided.”
Further in the retrieval, do not find to utilize the application report of juglandaceae plant dyestuff dyeing silk.
Summary of the invention
The object of the invention is to disclose a kind of method of utilizing juglandaceae plant dyestuff dyeing silk.The present invention is used for silk dyeing with the juglandaceae plant dyestuff of Nantural non-toxic; The dyeing spectrum of juglandaceae plant dyestuff is increased; And for reducing the use of synthetic dyestuffs on real silk; The exploitation natural dye provides technical basis, simultaneously, also for the real efficient recycling of large-scale industrialization production and agricultural resource that realizes foundation is provided.
The present invention realizes that through following technical scheme the present invention adopts dyeing silk on the different mordant dyeing method from juglandaceae plant, to extract the natural dye of preparation, draws the Color of different colour systems.
The present invention mainly utilizes the juglandaceae plant dyestuff that real silk is carried out direct dyeing or preparatory mordant dyeing look.
Described direct dyeing is meant: through with 10%-50% (with the ratio of real silk quality; W/W) juglandaceae plant dyestuff dyes on being added to and carrying out on the real silk, and bath raio is (part by weight of real silk and dye liquor) 1:1-1:150, contaminates a period of time; Perhaps slowly heating; The real silk that dyed is taken out in room temperature cooling then, and washing is dried.
Described preparatory mordant dyeing look is meant: real silk immersed in the water, lets its abundant wetting back take out, water is extracted, and for use.With mordant is that (with the ratio of real silk quality, W/W), bath raio (part by weight of real silk and dye liquor) is 1:1-1:80 to 10%-30%, and 15-100 ℃ of heating down cooled off under the room temperature then; (with the ratio of real silk quality, juglandaceae plant dyestuff W/W) dyes on being added to and carrying out on the real silk, and bath raio is (part by weight of real silk and dye liquor) 1:1-1:150, slowly heats, and the real silk that dyed is taken out in room temperature cooling then, and washing is dried with 10%-50%.
Slow heating in the described direct dyeing is meant: temperature heats 10-360min down at 10-100 ℃.
Slow heating in the described preparatory mordant dyeing look is meant: temperature heats 10-240min down at 15-100 ℃.
In the described preparatory mordant dyeing look 15-100 ℃ heating down, heat time heating time wie20-480min.
Said room temperature cool time is 1 hour.
Described mordant solution is alum, copper sulphate or ferrous sulfate.
The gained real silk was pale brown look when application juglandaceae plant dyestuff carried out direct dyeing to real silk, and when using the method for preparatory mordant dyeing look, the real silk of different mordant gained is a different colours, can obtain sundown, olive-green, brown.
The present invention utilizes juglandaceae plant to dye, and has plant resources and enriches, and is nontoxic, easy artificial growth, and dyefastness is good simultaneously, and dye-uptake is high, even dyeing, color and luster is soft, nature, the processing of use environmental protection mordant can also increase chromatogram; Simultaneously, the present invention also provides the most simple and effective dyeing, utilizes minimum cost to create the highest economy and society and is worth, and has really realized pollution-free, high environmental protection, low power consuming, and has made agricultural resource obtain maximized recycle.
The specific embodiment
Elaborate in the face of embodiments of the invention down, present embodiment provided detailed embodiment and concrete operating process, but protection scope of the present invention is not limited to following embodiment being to implement under the prerequisite with technical scheme of the present invention.
Embodiment 1
After collecting the juglandaceae plant fermentation, dry, pulverize the back and cross 40 mesh sieves, take by weighing the 200g vegetable material and add 35% ethanolic solution; Wherein the weight ratio of juglandaceae plant raw material and solvent is 1:15, solidliquid mixture is placed under 60 ℃ of conditions of indoor temperature mix, and natural dye 24h is extracted in lixiviate; Cross then and filter dye solution; 40 ℃ decompression is concentrated down with the stock staining solution that extracts, and obtains juglandaceae plant powdery concentrate, i.e. the juglandaceae plant dyestuff.
Embodiment 2
Get real silk and add the clear water rinsing, bleed off cleaning fluid, extract.(with the ratio of real silk quality, juglandaceae plant dyestuff W/W) dyes on being added to and carrying out on the real silk, is that 1:50 adds water by bath raio, and temperature was at room temperature cooled off 1 hour after taking out then at 50 ℃ of heating 80min down, and washing is dried, and the gained real silk is pale brown look with 30%.
Present embodiment uses the juglandaceae plant dyestuff directly real silk to be dyeed, and the gained color is pale brown look, even dyeing; COLOR FASTNESS is good; Do not exist synthetic dyestuffs to the pollution of environment with to the harm of human body, can be used for the cleaner production of textile industry, but large-scale industrial production.
Embodiment 3
Get real silk and add the clear water rinsing, bleed off cleaning fluid, extract.Add water by the 1:20 bath raio, (with the ratio of real silk quality, alum W/W) boils 30min to put into 30% after the heating; Tapping after room temperature cooling at least one hour then, (with the ratio of real silk quality, juglandaceae plant dyestuff W/W) dyes on being added to and carrying out on the real silk with 30% after the real silk flushing; By bath raio is that 1:10 adds water, and temperature heats 10min down at 90 ℃, at room temperature cools off 1 hour after taking out then; Washing is dried, and the gained real silk is a sundown.
Present embodiment uses the juglandaceae plant dyestuff under the condition of alum as mordant, real silk to be dyeed; The gained color is a sundown; Even dyeing, COLOR FASTNESS is good, does not exist synthetic dyestuffs to the pollution of environment with to the harm of human body; Can be used for the cleaner production of textile industry, but large-scale industrial production.
Embodiment 4
Get real silk and add the clear water rinsing, bleed off cleaning fluid, extract.Add water by the 1:20 bath raio, (with the ratio of real silk quality, copper sulphate W/W) boils 60min to put into 20% after the heating; Tapping after room temperature cooling at least one hour then, (with the ratio of real silk quality, juglandaceae plant dyestuff W/W) dyes on being added to and carrying out on the real silk with 30% after the real silk flushing; By bath raio is that 1:90 adds water, and temperature heats 15min down at 60 ℃, at room temperature cools off 1 hour after taking out then; Washing is dried, and the gained real silk is an olive-green.
Present embodiment uses the juglandaceae plant dyestuff under the condition of mantoquita as mordant, real silk to be dyeed; The gained color is an olive-green; Even dyeing, COLOR FASTNESS is good, does not exist synthetic dyestuffs to the pollution of environment with to the harm of human body; Can be used for the cleaner production of textile industry, but large-scale industrial production.
Embodiment 5
Get real silk and add the clear water rinsing, bleed off cleaning fluid, extract.Add water by the 1:20 bath raio, (with the ratio of real silk quality, ferrous sulfate W/W) boils 80min to put into 10% after the heating; Tapping after room temperature cooling at least one hour then, (with the ratio of real silk quality, juglandaceae plant dyestuff W/W) dyes on being added to and carrying out on the real silk with 40% after the real silk flushing; By bath raio is that 1:90 adds water, and temperature heats 240min down at 90 ℃, at room temperature cools off 1 hour after taking out then; Washing is dried, and the gained real silk is a brown.
Present embodiment uses the juglandaceae plant dyestuff under the condition of metal ferrous salt as mordant, real silk to be dyeed; The gained color is a brown; Even dyeing, COLOR FASTNESS is good, does not exist synthetic dyestuffs to the pollution of environment with to the harm of human body; Can be used for the cleaner production of textile industry, but large-scale industrial production.
The sample that the present invention is last after dying detects through Shanghai Textile Industry Technology Supervision Institute, and testing result is judged to be each item dyeing index according to standard GB 18401-2003 and all meets standard, and is as shown in the table.
Although content of the present invention has been done detailed introduction through above-mentioned preferred embodiment, will be appreciated that above-mentioned description should not be considered to limitation of the present invention.After those skilled in the art have read foregoing, for multiple modification of the present invention with to substitute all will be conspicuous.Therefore, protection scope of the present invention should be limited appended claim.
Claims (5)
1. a method of utilizing juglandaceae plant dyestuff dyeing silk is characterized in that utilizing the juglandaceae plant dyestuff that real silk is carried out direct dyeing or preparatory mordant dyeing look, wherein:
Described direct dyeing is meant: be added to through the juglandaceae plant dyestuff with real silk quality 10%-50% and dye on carrying out on the real silk, bath raio is that the part by weight of real silk and dye liquor is 1:1-1:150, contaminates a period of time; Perhaps slowly heating; The real silk that dyed is taken out in room temperature cooling then, and washing is dried;
Described preparatory mordant dyeing look is meant: real silk immersed in the water, lets its abundant wetting back take out, water is extracted, and for use; Get the mordant of real silk quality 10%-30%, bath raio is that the part by weight of real silk and dye liquor is 1:1-1:80, and 15-100 ℃ of heating down cooled off under the room temperature then; The juglandaceae plant dyestuff of the 10%-50% of real silk quality is added to dyes on carrying out on the real silk, bath raio is to be that the part by weight of real silk and dye liquor is 1:1-1:150, slowly heating, and the real silk that dyed is taken out in room temperature cooling then, and washing is dried.
2. the method for utilizing juglandaceae plant dyestuff dyeing silk according to claim 1 is characterized in that: the slow heating in the described direct dyeing is meant: temperature heats 10-360min down at 10-100 ℃.
3. the method for utilizing juglandaceae plant dyestuff dyeing silk according to claim 1 is characterized in that: the slow heating in the described preparatory mordant dyeing look is meant: heat 10-240min down at 15-100 ℃.
4. the method for utilizing juglandaceae plant dyestuff dyeing silk according to claim 1 is characterized in that: in the described preparatory mordant dyeing look 15-100 ℃ heating down, heat time heating time wie20-480min.
5. the method for utilizing juglandaceae plant dyestuff dyeing silk according to claim 1 is characterized in that: said room temperature cool time is 1 hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2012101664782A CN102677485A (en) | 2012-05-24 | 2012-05-24 | Method for dyeing real silk with Juglandaceae vegetable dye |
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| CN2012101664782A CN102677485A (en) | 2012-05-24 | 2012-05-24 | Method for dyeing real silk with Juglandaceae vegetable dye |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103334290A (en) * | 2013-04-23 | 2013-10-02 | 太仓市其盛化纤厂 | Silk fabric dyeing method |
| CN103669030A (en) * | 2013-11-28 | 2014-03-26 | 湖州立方塑木新材料有限公司 | Walnut skin printing and dyeing technology |
| CN103757942A (en) * | 2014-01-03 | 2014-04-30 | 蒋立宪 | Method for harmless dyeing of school uniform fabric |
| CN107805955A (en) * | 2017-11-15 | 2018-03-16 | 南通大学 | A kind of diaphragma juglandis dyeing method |
| CN110747661A (en) * | 2018-07-24 | 2020-02-04 | 广东印象派服装有限公司 | Dyeing method of mulberry silk |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1912011A (en) * | 2005-08-11 | 2007-02-14 | 青岛海联植物科技研究所 | Method for extracting matural dye from external skin of walnut |
| CN102153883A (en) * | 2011-03-02 | 2011-08-17 | 上海交通大学 | Preparation and application of wool dye prepared by walnut plant |
| CN102321983A (en) * | 2011-08-10 | 2012-01-18 | 无锡市联盛印染有限公司 | Silk dyeing and finishing method using shikonin derivatives |
-
2012
- 2012-05-24 CN CN2012101664782A patent/CN102677485A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1912011A (en) * | 2005-08-11 | 2007-02-14 | 青岛海联植物科技研究所 | Method for extracting matural dye from external skin of walnut |
| CN102153883A (en) * | 2011-03-02 | 2011-08-17 | 上海交通大学 | Preparation and application of wool dye prepared by walnut plant |
| CN102321983A (en) * | 2011-08-10 | 2012-01-18 | 无锡市联盛印染有限公司 | Silk dyeing and finishing method using shikonin derivatives |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103334290A (en) * | 2013-04-23 | 2013-10-02 | 太仓市其盛化纤厂 | Silk fabric dyeing method |
| CN103669030A (en) * | 2013-11-28 | 2014-03-26 | 湖州立方塑木新材料有限公司 | Walnut skin printing and dyeing technology |
| CN103757942A (en) * | 2014-01-03 | 2014-04-30 | 蒋立宪 | Method for harmless dyeing of school uniform fabric |
| CN107805955A (en) * | 2017-11-15 | 2018-03-16 | 南通大学 | A kind of diaphragma juglandis dyeing method |
| CN110747661A (en) * | 2018-07-24 | 2020-02-04 | 广东印象派服装有限公司 | Dyeing method of mulberry silk |
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Application publication date: 20120919 |