CN102659337A - Composite Portland cement using green mud and basalt as mixed materials - Google Patents
Composite Portland cement using green mud and basalt as mixed materials Download PDFInfo
- Publication number
- CN102659337A CN102659337A CN2012101159340A CN201210115934A CN102659337A CN 102659337 A CN102659337 A CN 102659337A CN 2012101159340 A CN2012101159340 A CN 2012101159340A CN 201210115934 A CN201210115934 A CN 201210115934A CN 102659337 A CN102659337 A CN 102659337A
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- portland cement
- composite portland
- green mud
- basalt
- grinding
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/10—Production of cement, e.g. improving or optimising the production methods; Cement grinding
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- Treatment Of Sludge (AREA)
- Processing Of Solid Wastes (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The invention belongs to the filed of buildings and relates to a building material, in particular to composite Portland cement using green mud and a basalt as mixed materials. The composite Portland cement comprises the following preparation steps of dewatering and drying the green mud till the moisture content is less than 1 percent, crushing the basalt into broken stones of which the grain sizes are 50 millimeters, mixing and feeding the basalt broken stones, the green mud, gypsum, an activating agent and a cement clinker into grinding equipment for grinding till the specific surface area is 330 m<2>/kg-350 m<2>/kg, drying in the grinding process, so that the moisture content of ground powder is less than 0.5 percent, and grinding to obtain the composite Portland cement. The composite Portland cement has the benefits that the production process is simple, a large quantity of easily-available abandoned corner stones in a basalt quarry, the green mud and other industrial wastes are taken as the mixed materials, the cost is low, the early strength and the construction performance of the composite Portland cement are effectively improved, resources and energy resources are saved, the industrial production is facilitated, and the environment friendliness is facilitated, the energy is saved, and the emission is reduced.
Description
Technical field
The invention belongs to building field, relate to a kind of material of construction, specifically is a kind of composite Portland cement that uses green mud and Irish touchstone to make mixing material.
Background technology
Composite Portland cement (code name PC) is by the levigate hydraulic cementing materials of processing of mixing material, the proper amount of gypsum of Portland clinker, two or more regulation (composite Portland cement [abbreviation complex cement]); The total addition content of mixing material should be no more than 50% greater than 20% by mass percentage in the cement.The used blended material of composite Portland cement is to meet the granulated blast-furnace slag of GB203-2008 regulation at present; The pozzolana mixed material and the flyash that meets the GB1596-2005 regulation that meet the GB2847-1996 regulation; And the active addition of newly opening up according to the GB175-2007 appendix A; Do not meet cement additive and Wingdale, the sandstone of latent hydraulicity or the volcanical ash property of standard-required like iron-tion slag, refining ferrochrome slag isoreactivity mixing material and activity index; And the nonactive mixing material of newly opening up according to GB 175-2007 appendix A, like titanium slag etc.
Green mud is meant that caustic room alkali in the paper technology reclaims the waste that the back produces, if arbitrarily topple over, stacking or landfill, can cause great harm to environment: 1, take a large amount of soils; 2, polluted air; 3, pollute water system etc.Through retrieval, mix green mud and also do not see relevant report as the composite Portland cement mixing material.
Summary of the invention
The objective of the invention is to the deficiency of prior art and a kind of composite Portland cement is provided; With trade wastes such as the discarded corner building stones of measuring the flyash that is easy to get greatly, furnace bottom slag, basalt stone field and green muds is main mixing material; Cost is low, and production technique is simple, and the composite Portland cement of gained can satisfy composite Portland cement requirement in the GB 175-2007 general purpose portland cement standard; Can handle industrial residue in a large number; Help environment protection and energy-saving and emission-reduction, can improve the composite Portland cement early strength simultaneously, improve the workability of composite Portland cement.
The technical scheme that the present invention adopted:
A kind of composite Portland cement that uses green mud and Irish touchstone to make mixing material; Be earlier green mud to be dehydrated water ratio less than 1%; The Irish touchstone mine tailing is broken into particle diameter less than 50 millimeters rubble, and send into milling equipment then to carry out grinding to specific surface area be 330m with basaltic broken stone, green mud, gypsum, acvator and after cement clinker mixes
2/ kg～350m
2/ kg; Carry out drying treatment in the grinding process and use abrasive dust material water ratio less than 0.5%; Go out mill and obtain composite Portland cement; Wherein in butt, each component percentage ratio meter by weight is respectively: basaltic broken stone 5%～35%, cement clinker 50%～75%, green mud 3%～15%, gypsum 3%～8%, acvator 0.5%～5%, various component weight percentage summations are one of percentage hundred.
Said acvator is the mixture of organic cpds and mineral compound; Wherein organic cpds comprises a kind of in trolamine, tri-isopropanolamine, sodium formiate, calcium formiate, lime acetate, sodium acetate or the potassium acetate or more than two kinds, and mineral compound comprises a kind of in water glass, potassium silicate, Calucium Silicate powder, sodium sulfate, vitriolate of tartar, ferric sulfate, ammonium sulfate, yellow soda ash, salt of wormwood, volatile salt or quicklime, the active silica or more than two kinds.
In acvator, by weight, the usage quantity of each component is in the organic cpds:
Trolamine or tri-isopropanolamine 0.02～0.1;
A kind of in sodium formiate, calcium formiate, lime acetate, sodium acetate or the potassium acetate or mix 0.2～3.0 more than two kinds;
The usage quantity of each component is in the mineral compound:
A kind of in water glass, potassium silicate, Calucium Silicate powder, sodium sulfate, vitriolate of tartar, ferric sulfate, ammonium sulfate, yellow soda ash, salt of wormwood, volatile salt or the quicklime or mix 0.2～3.0 more than two kinds;
Active silica 10.0～100.0.
Said milling equipment is one or both combinations in ball milling, vertical roller grinder, the vibration mill.
Among the present invention, can add blended material commonly used simultaneously at basaltic broken stone and green mud blended as required, by weight percentage, the add-on of blended material commonly used is below 35% of total material.Said blended material commonly used is meant a kind of or mixing in flyash or the furnace bottom slag.
Among the present invention, can in going out the abrasive dust material, add specific surface area as required is 400m
2/ kg～450m
2The GBFS of/kg, by weight percentage, the add-on of GBFS is below 20% of total material.
The Production Flow Chart of composite Portland cement provided by the present invention is: green mud is dehydrated handle water ratio less than 1% earlier; Irish touchstone corner building stones are broken into rubble below 50 millimeters; Press formula rate again and basaltic broken stone, green mud, gypsum, acvator are mixed (adding blended material [flyash and/or furnace bottom slag] commonly used as required) with cement clinker; Compound gets into grinding system and carries out grinding processing, and going out abrasive dust body fineness, to be controlled at specific surface area be 330m
2/ kg～350m
2/ kg; In grinding process; Adopt the fluidizing furnace heat air delivery to dry to advancing grind materials; For guaranteeing out that mill cement quality and storage and transportation normally need guarantee out mill cement water ratio less than 0.5% (preferably less than 0.3%), (can in going out the abrasive dust material, add specific surface area as required is 400m to go out to grind to obtain composite Portland cement
2/ kg～450m
2The GBFS of/kg).
Production technique of the present invention is simple, is mixing material with trade wastes such as the discarded corner building stones of measuring the basalt stone field that is easy to get greatly, green muds, and cost is low; The gained composite Portland cement can satisfy the requirement of composite Portland cement in the GB 175-2007 general purpose portland cement standard; Improve composite Portland cement early strength and workability effectively, economize on resources and the energy, help suitability for industrialized production; Can handle industrial residue in a large number, help environment protection and energy-saving and emission-reduction.
Embodiment
Below in conjunction with embodiment, specific embodiments of the invention describes in further detail.Following examples are used to explain the present invention, but are not used for limiting scope of the present invention.
Embodiment one
Produce the PC32.5R composite Portland cement
The chemical ingredients such as the table 1 of Irish touchstone, flyash, furnace bottom slag, GBFS and green mud:
The chemical ingredients of each component of table 1 (mass percent)
Produce the proportioning such as the table 2 of each component of PC32.5R composite Portland cement:
Table 2 unit: kg
Wherein acvator is formed (by weight) as follows:
Trolamine 0.05kg, water glass 1kg, salt of wormwood 0.5kg.
Production technique is following:
Press table 2 proportioning, earlier with green mud dehydrate to water ratio less than 1%, subsequent use, again Irish touchstone is broken into rubble below 50 millimeters, subsequent use.Go into milling system and carry out grinding processing basaltic broken stone (below 50 millimeters) and green mud (dry), flyash, gypsum, cement clinker, activator mix are laggard, going out the abrasive dust material, to be controlled at specific surface area be 330m
2/ kg is to 350m
2/ kg in grinding process, adopts the fluidizing furnace heat air delivery to dry advancing grind materials, simultaneously for guaranteeing out that mill cement quality and storage and transportation normally need guarantee out abrasive dust material water ratio less than 0.3%, goes out mill and obtains composite Portland cement PC 32.5R.
Embodiment two
The chemical constitution of Irish touchstone, flyash, furnace bottom slag, GBFS and green mud, acvator composition, production technique are with embodiment one.
Produce the proportioning such as the table 3 of each component of PC32.5R composite Portland cement:
Table 3 unit: kg
Embodiment three
The chemical constitution of Irish touchstone, flyash, furnace bottom slag, GBFS and green mud, production technique are with embodiment one.
Acvator is formed (by weight) as follows:
Tri-isopropanolamine 0.05kg, water glass 1kg, active silica 10kg.
Produce the proportioning such as the table 4 of each component of PC32.5R composite Portland cement:
Table 4 unit: kg
Embodiment four
The chemical constitution of Irish touchstone, flyash, furnace bottom slag, GBFS and green mud is with embodiment one.Acvator is formed with embodiment three.
Produce the proportioning such as the table 5 of each component of PC32.5R composite Portland cement:
Table 5 unit: kg
Production technique is following:
Press table 5 proportioning, earlier with green mud dehydrate to water ratio less than 1%, subsequent use, again Irish touchstone is broken into rubble below 50 millimeters, subsequent use.Go into milling system and carry out grinding processing basaltic broken stone (below 50 millimeters) and green mud (dry), gypsum, cement clinker, activator mix are laggard, going out the abrasive dust material, to be controlled at specific surface area be 330m
2/ kg is to 350m
2/ kg; In grinding process; Adopt the fluidizing furnace heat air delivery to dry advancing grind materials, simultaneously for guaranteeing out that mill cement quality and storage and transportation normally need guarantee out abrasive dust material water ratio less than 0.3%, (specific surface area is 400m after mixer adds the S95 GBFS to go out mill
2/ kg is to 450m
2/ kg), obtain composite Portland cement PC 32.5R.
Embodiment five
Produce the PC42.5R composite Portland cement
The chemical ingredients such as the table 6 of Irish touchstone, flyash, furnace bottom slag, GBFS and green mud, cement clinker:
The chemical ingredients of each component of table 6 (mass percent)
Acvator is formed (by weight) as follows:
Trolamine 0.05kg, calcium formiate 0.5kg, water glass 1kg.
Produce the proportioning such as the table 7 of each component of PC42.5R composite Portland cement:
Table 7 unit: kg
Production technique is with embodiment four.
Embodiment six
The chemical constitution of Irish touchstone, flyash, furnace bottom slag, GBFS and green mud, acvator composition, production technique are with embodiment five.
Produce the proportioning such as the table 8 of each component of PC42.5R composite Portland cement:
Table 8 unit: kg
Embodiment seven
The chemical constitution of Irish touchstone, flyash, furnace bottom slag, GBFS and green mud, acvator composition, production technique are with embodiment five.
Produce the proportioning such as the table 9 of each component of PC42.5R composite Portland cement:
Table 9 unit: kg
Embodiment eight
The chemical constitution of Irish touchstone, flyash, furnace bottom slag, GBFS and green mud, acvator composition, production technique are with embodiment five.
Produce the proportioning such as the table 10 of each component of PC42.5R composite Portland cement:
Table 10 unit: kg
Detect:
With embodiment of the invention prepared composite silicate cement, detect various performances such as table 11 according to the standard of GB/T17671-1999.
Table 11
Table 11 is the result show; Use green mud and Irish touchstone to do the composite Portland cement 3 days of mixing material and the requirement that 28 days bending and compressive strength meet composite Portland cement in the GB 175-2007 general purpose portland cement standard fully, can satisfy PC42.5R and PC32.5R index.
The above only is a preferred implementation of the present invention; Should be pointed out that for those skilled in the art, under the prerequisite that does not break away from know-why of the present invention; Can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (4)
1. composite Portland cement that uses green mud and Irish touchstone to make mixing material; It is characterized in that earlier green mud being dehydrated water ratio less than 1%; The Irish touchstone mine tailing is broken into particle diameter less than 50 millimeters rubble, and send into milling equipment then to carry out grinding to specific surface area be 330m with basaltic broken stone, green mud, gypsum, acvator and after cement clinker mixes
2/ kg～350m
2/ kg; Carry out drying treatment in the grinding process and use abrasive dust material water ratio less than 0.5%; Go out mill and obtain composite Portland cement; Wherein in butt, each component percentage ratio meter by weight is respectively: basaltic broken stone 5%～35%, cement clinker 50%～75%, green mud 3%～15%, gypsum 3%～8%, acvator 0.5%～5%, and various component weight percentage summations are one of percentage hundred; Said acvator is that organic cpds and mineral compound are with arbitrary proportion blended mixture; Wherein organic cpds comprises a kind of in trolamine, tri-isopropanolamine, sodium formiate, calcium formiate, lime acetate, sodium acetate or the potassium acetate or more than two kinds, and mineral compound comprises a kind of in water glass, potassium silicate, Calucium Silicate powder, sodium sulfate, vitriolate of tartar, ferric sulfate, ammonium sulfate, yellow soda ash, salt of wormwood, volatile salt or quicklime, the active silica or more than two kinds;
In acvator, by weight, the usage quantity of each component is in the organic cpds:
Trolamine or tri-isopropanolamine 0.02～0.1;
A kind of in sodium formiate, calcium formiate, lime acetate, sodium acetate or the potassium acetate or mix 0.2～3.0 more than two kinds;
The usage quantity of each component is in the mineral compound:
A kind of in water glass, potassium silicate, Calucium Silicate powder, sodium sulfate, vitriolate of tartar, ferric sulfate, ammonium sulfate, yellow soda ash, salt of wormwood, volatile salt or the quicklime or mix 0.2～3.0 more than two kinds;
Active silica 10.0～100.0.
2. composite Portland cement according to claim 1 is characterized in that: said milling equipment is one or both combinations in ball milling, vertical roller grinder, the vibration mill.
3. composite Portland cement according to claim 1 is characterized in that: add blended material commonly used simultaneously at basaltic broken stone and green mud blended, by weight percentage, the add-on of blended material commonly used is below 35% of total material; Said blended material commonly used is meant a kind of or mixing in flyash or the furnace bottom slag.
4. composite Portland cement according to claim 1 is characterized in that: in going out the abrasive dust material, adding specific surface area is 400m
2/ kg～450m
2The GBFS of/kg, by weight percentage, the add-on of GBFS is below 20% of total material.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210115934.0A CN102659337B (en) | 2012-04-20 | 2012-04-20 | Composite Portland cement using green mud and basalt as mixed materials |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210115934.0A CN102659337B (en) | 2012-04-20 | 2012-04-20 | Composite Portland cement using green mud and basalt as mixed materials |
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| CN102659337A true CN102659337A (en) | 2012-09-12 |
| CN102659337B CN102659337B (en) | 2014-01-01 |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104230291A (en) * | 2014-08-27 | 2014-12-24 | 郑旭 | Modified basalt reinforced gypsum |
| CN104496255A (en) * | 2014-11-28 | 2015-04-08 | 苏笮斌 | TK-JH mineral interface active material, and preparation method and application method thereof |
| CN104496246A (en) * | 2014-12-24 | 2015-04-08 | 熊敏 | Cement concrete building solid phase filler surfactant and manufacturing and use methods thereof |
| CN105800974A (en) * | 2016-02-26 | 2016-07-27 | 华润水泥技术研发有限公司 | Composite silicate P.C32.5R cement and application thereof in decoration |
| CN105884222A (en) * | 2016-04-08 | 2016-08-24 | 赞皇济槐矿粉建材有限公司 | Composite cement made from basalt and preparation method of composite cement |
| CN104844111B (en) * | 2015-04-30 | 2016-08-24 | 谭云松 | A kind of admixture and concrete prepared therefrom |
| CN107098610A (en) * | 2017-05-17 | 2017-08-29 | 洛阳宏昌水泥有限公司 | A kind of cement ingredient of utilization bottom slag |
| US11981860B2 (en) | 2021-04-30 | 2024-05-14 | União Brasileira De Educação E Assistência—Mantenedora Da Pucrs | Hydraulic cement composition, process and use |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104230291A (en) * | 2014-08-27 | 2014-12-24 | 郑旭 | Modified basalt reinforced gypsum |
| CN104230291B (en) * | 2014-08-27 | 2016-03-23 | 郑旭 | Modification basalt strengthens gypsum |
| CN104496255A (en) * | 2014-11-28 | 2015-04-08 | 苏笮斌 | TK-JH mineral interface active material, and preparation method and application method thereof |
| CN104496255B (en) * | 2014-11-28 | 2017-01-18 | 苏笮斌 | Mineral interface active material, and preparation method and application method thereof |
| CN104496246A (en) * | 2014-12-24 | 2015-04-08 | 熊敏 | Cement concrete building solid phase filler surfactant and manufacturing and use methods thereof |
| CN104844111B (en) * | 2015-04-30 | 2016-08-24 | 谭云松 | A kind of admixture and concrete prepared therefrom |
| CN105800974A (en) * | 2016-02-26 | 2016-07-27 | 华润水泥技术研发有限公司 | Composite silicate P.C32.5R cement and application thereof in decoration |
| CN105800974B (en) * | 2016-02-26 | 2018-07-20 | 华润水泥技术研发有限公司 | A kind of composition silicate P.C32.5R cement and its application in finishing |
| CN105884222A (en) * | 2016-04-08 | 2016-08-24 | 赞皇济槐矿粉建材有限公司 | Composite cement made from basalt and preparation method of composite cement |
| CN105884222B (en) * | 2016-04-08 | 2018-06-12 | 赞皇济槐矿粉建材有限公司 | A kind of complex cement using basalt as material and preparation method thereof |
| CN107098610A (en) * | 2017-05-17 | 2017-08-29 | 洛阳宏昌水泥有限公司 | A kind of cement ingredient of utilization bottom slag |
| US11981860B2 (en) | 2021-04-30 | 2024-05-14 | União Brasileira De Educação E Assistência—Mantenedora Da Pucrs | Hydraulic cement composition, process and use |
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| Publication number | Publication date |
|---|---|
| CN102659337B (en) | 2014-01-01 |
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