CN102635171B - Preparation method of integral-type vacuum heat insulation and temperature preservation plate - Google Patents
Preparation method of integral-type vacuum heat insulation and temperature preservation plate Download PDFInfo
- Publication number
- CN102635171B CN102635171B CN201210136456.1A CN201210136456A CN102635171B CN 102635171 B CN102635171 B CN 102635171B CN 201210136456 A CN201210136456 A CN 201210136456A CN 102635171 B CN102635171 B CN 102635171B
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- plate
- core plate
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- thermal insulation
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A30/00—Adapting or protecting infrastructure or their operation
- Y02A30/24—Structural elements or technologies for improving thermal insulation
- Y02A30/242—Slab shaped vacuum insulation
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02B—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
- Y02B80/00—Architectural or constructional elements improving the thermal performance of buildings
- Y02B80/10—Insulation, e.g. vacuum or aerogel insulation
Abstract
The invention discloses a preparation method of an integral-type vacuum heat insulation and temperature preservation plate, and belongs to the technical field of an outer temperature preservation material for building outer walls. The technical scheme to be solved is that a preparation method of a vacuum heat insulation and temperature preservation plate which has a plate-type core material, has good integrity, is low in air leakage rate, and prevents cold and hot bridge is provided. According to the technical scheme, the preparation method comprises the following steps of: step one, manufacturing a core material plate; step two, loading the core material plate, and step three, vacuumizing and packaging. According to the invention, different from the prior art that the core material is in a powder shape, the plate provided by the invention has the advantages that an inorganic material is synthesized into the plate material, and a special bonding material is adopted for bonding the core material and the packaging layer together, thus the temperature preservation plate has the integrity; the core material plate is adopted and drilled for holding an air absorption agent, the quantity and position are distributed scientifically, and the long-lasting vacuum degree is ensured; and the air leakage rate is lowered by a dual-seal mode.
Description
Technical field
The preparation method of a kind of monolithic vacuum thermal insulation of the present invention plate belongs to external wall outer insulation material technology for building field.
Background technology
At present, for energy-saving material-vacuum thermal insulation plate of building inside and outside wall, leak rate is high, and surface finish is poor, maintenance usefulness is short, and after gas leakage, core separates formation " two skins " with vacuum bag, overlap edge easily produces the problems such as cold-heat bridge.In concrete engineering uses, return factory's ratio large, completion repair rate is high, and " the figure for shadow-play wall " that cold-heat bridge causes is obvious, and above these technological deficiencies and inadequate natural endowment, badly influence construction work progress and quality and heat preservation energy-saving effect.
Summary of the invention
The present invention, in order to overcome the deficiencies in the prior art, provides a kind of tabular core, the preparation method of the vacuum thermal insulation plate that good integrity, leak rate be low, avoid cold-heat bridge.
In order to solve the problems of the technologies described above, the technical solution used in the present invention is, a kind of preparation method of monolithic vacuum thermal insulation plate carries out according to following steps:
The first step, the making of core plate
A, by the raw material of core plate according to following weight portion proportioning: superfine fibre 70-55 part, poromerics 15-20 part, half closed pore granular material 8-18 part and cementing agent 3-10 part;
B, be 2:1 mix and blend pulping by weight by the raw material of described core plate and water, then extrusion modling, obtains moulding core plate;
C, described moulding core plate is dried to 5-8min at the temperature of 180 ℃-400 ℃, then by the moulding core plate cutting of oven dry and beat equably multiple through holes on the plate face of well cutting, obtain standard core plate;
Second step, loads core plate
To in the through hole of described standard core plate, dose getter, then apply fire prevention adhesives at two plate faces of the standard core plate of filling getter, then put into encapsulated layer and carry out extrusion bondedly, obtain core plate to be packaged;
The 3rd step, vacuumizes encapsulation
Described core plate to be packaged is vacuumized to 5-25min, and vacuum reaches 10
-2-10
-4kPa, then carries out heat sealing and second pulse extruding sealing successively, finally cuts and obtains standard warming plate.
Described superfine fibre is mineral wool, or mineral wool; Described poromerics is silica; Described half closed pore granular material is perlite; Described cementing agent is starch and ripe rubber powder, and the weight part ratio of starch and ripe rubber powder is 1:2.
Described fire prevention adhesive is cloud stone glue for building or environment-friendly type chlorobutyl benzene-free fire-retarded universal glue for building.
Described standard core plate freeze-thaw resistance is more than or equal to 0.1MPa, and impact strength is not less than 2.0J.
The through-hole diameter of described standard core plate is 3-4mm.
Second step loads in core plate at two plate faces of the standard core plate of described filling getter and applies after fire prevention adhesives, then puts into encapsulated layer and carry out extrusion bondedly, and adhesion strength is greater than 0.1MPa.
The beneficial effect that the present invention compared with prior art has is: the warming plate that the present invention makes is except possessing the excellent properties of prior art vacuum heat-insulating plate, made up that the leak rate that prior art and product exist is high, after poor flatness, gas leakage core loose, sink and " two skins " and product thin and thick differs, length not etc., the size defect and the inadequate natural endowment that are not inconsistent.Improve the globality of warming plate, guarantee that warming plate has good energy-saving heat preserving effect, greatly reduce the leak rate in production, transportation and the work progress of warming plate, saved production, application and cost of transportation, make specification, size standard, the standard more of product.The present invention adopts inorganic material to synthesize a kind of sheet material, and mode that to substitute prior art core be powdery has improved planeness and the specification standards of warming plate; Utilize the equally distributed hemispherical projections of plate face of core plate, improve the adhesion strength of warming plate; Adopt a kind of special binder material that core and encapsulated layer are bonded as one, make warming plate there is globality; Adopt core twist drill hole to place getter, science quantity allotted and position, guarantee lasting vacuum; Adopt two sealing modes to reduce leak rate; Adopt special strip warming plate to fill the overlap edge of warming plate, thereby solve the problem of prior art because of the cold-heat bridge formation " figure for shadow-play wall " of overlap edge generation.
The specific embodiment
Below in conjunction with specific embodiment, the invention will be further described.
Overall vacuum heat insulating thermal preserving board prepared by the present invention, comprise encapsulated layer and core plate, its final structure is: core plate is between two-layer encapsulated layer, the connection that is fused of the surrounding of two-layer encapsulated layer, on the plate face of core plate, be evenly provided with multiple through holes, plate face surface uniform is distributed with multiple hemispherical projections of rectangular array, through hole is positioned in the middle of adjacent four hemispherical projections, getter is filled in through hole, on two plate faces of core plate, be coated with adhesive, encapsulated layer and core plate surface are linked into an integrated entity.
The high 2-4mm of hemispherical projections, the adjacent spaces 10mm of the plate face surface distributed of core plate.The plate face of core plate can be also smooth plate face.
In preparation method's second step, will in the through hole of standard core plate, dose getter, then apply fire prevention adhesives at two plate faces of the standard core plate of filling getter, then put into encapsulated layer and carry out extrusion bondedly, obtain core plate to be packaged; Wherein the bond area of the standard core plate of encapsulated layer and filling getter, between 85-90 part, leaves space for getter plays a role.
Embodiment 1
A preparation method for monolithic vacuum thermal insulation plate, carries out according to following steps:
The first step, the making of core plate
A, by the raw material of core plate according to following weight portion proportioning: 5 parts of 70 parts of superfine fibres, 15 parts of poromerics, 10 parts of half closed pore granular materials and cementing agents;
B, be 2:1 mix and blend pulping by weight by the raw material of described core plate and water, then extrusion modling, obtains moulding core plate;
C, described moulding core plate is dried to 5min at the temperature of 400 ℃, then by the moulding core plate cutting of oven dry and beat equably the through hole that multiple diameters are 4mm on the plate face of well cutting, obtain standard core plate; Standard core plate freeze-thaw resistance is more than or equal to 0.1MPa, and impact strength is not less than 2.0J;
Second step, loads core plate
To in the through hole of described standard core plate, dose getter, then apply fire prevention adhesives at two plate faces of the standard core plate of filling getter, then put into encapsulated layer and carry out extrusion bondedly, adhesion strength is greater than 0.1MPa, obtains core plate to be packaged;
The 3rd step, vacuumizes encapsulation
Described core plate to be packaged is vacuumized to 25min, and vacuum reaches 10
-2-10
-4kPa, then carries out heat sealing and second pulse extruding sealing successively, finally cuts and obtains standard warming plate.
Superfine fibre is mineral wool; Poromerics is silica; Half closed pore granular material is perlite; Cementing agent is starch and ripe rubber powder, and the weight part ratio of starch and ripe rubber powder is 1:2.
Fire prevention adhesive is cloud stone glue for building.
Embodiment 2
A preparation method for monolithic vacuum thermal insulation plate, carries out according to following steps:
The first step, the making of core plate
A, by the raw material of core plate according to following weight portion proportioning: 10 parts of 55 parts of superfine fibres, 20 parts of poromerics, 15 parts of half closed pore granular materials and cementing agents;
B, be 2:1 mix and blend pulping by weight by the raw material of described core plate and water, then extrusion modling, obtains moulding core plate;
C, described moulding core plate is dried to 8min at the temperature of 150 ℃, then by the moulding core plate cutting of oven dry and beat equably the through hole that multiple diameters are 3mm on the plate face of well cutting, obtain standard core plate; Standard core plate freeze-thaw resistance is more than or equal to 0.1MPa, and impact strength is not less than 2.0J;
Second step, loads core plate
To in the through hole of described standard core plate, dose getter, then apply fire prevention adhesives at two plate faces of the standard core plate of filling getter, then put into encapsulated layer and carry out extrusion bondedly, adhesion strength is greater than 0.1MPa, obtains core plate to be packaged;
The 3rd step, vacuumizes encapsulation
Described core plate to be packaged is vacuumized to 20min, and vacuum reaches 10
-2-10
-4kPa, then carries out heat sealing and second pulse extruding sealing successively, finally cuts and obtains standard warming plate.
Superfine fibre is mineral wool; Poromerics is silica; Half closed pore granular material is perlite; Cementing agent is starch and ripe rubber powder, and the weight part ratio of starch and ripe rubber powder is 1:2.
Fire prevention adhesive is environment-friendly type chlorobutyl benzene-free fire-retarded universal glue for building.
Embodiment 3
A preparation method for monolithic vacuum thermal insulation plate, carries out according to following steps:
The first step, the making of core plate
A, by the raw material of core plate according to following weight portion proportioning: 7 parts of 60 parts of superfine fibres, 15 parts of poromerics, 18 parts of half closed pore granular materials and cementing agents;
B, be 2:1 mix and blend pulping by weight by the raw material of described core plate and water, then extrusion modling, obtains moulding core plate;
C, described moulding core plate is dried to 6min at the temperature of 300 ℃, then by the moulding core plate cutting of oven dry and beat equably the through hole that multiple diameters are 4mm on the plate face of well cutting, obtain standard core plate; Standard core plate freeze-thaw resistance is more than or equal to 0.1MPa, and impact strength is not less than 2.0J;
Second step, loads core plate
To in the through hole of described standard core plate, dose getter, then apply fire prevention adhesives at two plate faces of the standard core plate of filling getter, then put into encapsulated layer and carry out extrusion bondedly, adhesion strength is greater than 0.1MPa, obtains core plate to be packaged;
The 3rd step, vacuumizes encapsulation
Described core plate to be packaged is vacuumized to 10min, and vacuum reaches 10
-2-10
-4kPa, then carries out heat sealing and second pulse extruding sealing successively, finally cuts and obtains standard warming plate.
Superfine fibre is mineral wool; Poromerics is silica; Half closed pore granular material is perlite; Cementing agent is starch and ripe rubber powder, and the weight part ratio of starch and ripe rubber powder is 1:2.
Fire prevention adhesive is cloud stone glue for building.
Embodiment 4
A preparation method for monolithic vacuum thermal insulation plate, carries out according to following steps:
The first step, the making of core plate
A, by the raw material of core plate according to following weight portion proportioning: 5 parts of 65 parts of superfine fibres, 18 parts of poromerics, 12 parts of half closed pore granular materials and cementing agents;
B, be 2:1 mix and blend pulping by weight by the raw material of described core plate and water, then extrusion modling, obtains moulding core plate;
C, described moulding core plate is dried to 7min at the temperature of 350 ℃, then by the moulding core plate cutting of oven dry and beat equably the through hole that multiple diameters are 3mm on the plate face of well cutting, obtain standard core plate; Standard core plate freeze-thaw resistance is more than or equal to 0.1MPa, and impact strength is not less than 2.0J;
Second step, loads core plate
To in the through hole of described standard core plate, dose getter, then apply fire prevention adhesives at two plate faces of the standard core plate of filling getter, then put into encapsulated layer and carry out extrusion bondedly, adhesion strength is greater than 0.1MPa, obtains core plate to be packaged;
The 3rd step, vacuumizes encapsulation
Described core plate to be packaged is vacuumized to 15min, and vacuum reaches 10
-2-10
-4kPa, then carries out heat sealing and second pulse extruding sealing successively, finally cuts and obtains standard warming plate.
Superfine fibre is mineral wool; Poromerics is silica; Half closed pore granular material is perlite; Cementing agent is starch and ripe rubber powder, and the weight part ratio of starch and ripe rubber powder is 1:2.
Fire prevention adhesive is environment-friendly type chlorobutyl benzene-free fire-retarded universal glue for building.
The present invention can summarize with other the concrete form without prejudice to spirit of the present invention or principal character.Therefore, no matter from that, above-mentioned embodiment of the present invention all can only think explanation of the present invention can not limit invention, claims have been pointed out scope of the present invention, and scope of the present invention is not pointed out in above-mentioned explanation, therefore, any variation in implication and the scope suitable with claims of the present invention, all should think to be included in the scope of claims.
Claims (6)
1. a preparation method for monolithic vacuum thermal insulation plate, is characterized in that carrying out according to following steps:
The first step, the making of core plate
A, by the raw material of core plate according to following weight portion proportioning: superfine fibre 70-55 part, poromerics 15-20 part, half closed pore granular material 8-18 part and cementing agent 3-10 part; Described superfine fibre is mineral wool or mineral wool, and described poromerics is silica, and described half closed pore granular material is perlite;
B, be 2:1 mix and blend pulping by weight by the raw material of described core plate and water, then extrusion modling, obtains moulding core plate;
C, described moulding core plate is dried to 5-8min at the temperature of 180 ℃-400 ℃, then by the moulding core plate cutting of oven dry and beat equably multiple through holes on the plate face of well cutting, obtain standard core plate;
Second step, loads core plate
To in the through hole of described standard core plate, dose getter, then apply fire prevention adhesives at two plate faces of the standard core plate of filling getter, then put into encapsulated layer and carry out extrusion bondedly, obtain core plate to be packaged;
The 3rd step, vacuumizes encapsulation
Described core plate to be packaged is vacuumized to 5-25min, and vacuum reaches 10
-2-10
-4kPa, then carries out heat sealing and second pulse extruding sealing successively, finally cuts and obtains standard warming plate.
2. the preparation method of a kind of monolithic vacuum thermal insulation plate according to claim 1, is characterized in that described cementing agent is starch and ripe rubber powder, and the weight part ratio of starch and ripe rubber powder is 1:2.
3. the preparation method of a kind of monolithic vacuum thermal insulation plate according to claim 1, is characterized in that described fire prevention adhesive is cloud stone glue for building or environment-friendly type chlorobutyl benzene-free fire-retarded universal glue for building.
4. the preparation method of a kind of monolithic vacuum thermal insulation plate according to claim 1, is characterized in that described standard core plate freeze-thaw resistance is more than or equal to 0.1MPa, and impact strength is not less than 2.0J.
5. the preparation method of a kind of monolithic vacuum thermal insulation plate according to claim 1, the through-hole diameter that it is characterized in that described standard core plate is 3-4mm.
6. the preparation method of a kind of monolithic vacuum thermal insulation plate according to claim 1, it is characterized in that second step loads in core plate at two plate faces of the standard core plate of described filling getter applies after fire prevention adhesives, put into encapsulated layer again and carry out extrusion bondedly, adhesion strength is greater than 0.1MPa.
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Cited By (1)
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DE102015008157A1 (en) * | 2014-11-27 | 2016-06-02 | Liebherr-Hausgeräte Lienz Gmbh | Vakuumdämmkörper |
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CN103206027B (en) * | 2013-04-24 | 2015-11-25 | 王明堂 | A kind of light-weight building vacuum heat-insulation plate |
CN104373763A (en) * | 2013-08-12 | 2015-02-25 | 苏州维艾普新材料股份有限公司 | Vacuum insulation panel produced from core material of porous structure and production method of vacuum insulation panel |
CN103968586B (en) * | 2014-05-15 | 2015-06-10 | 青岛科瑞新型环保材料有限公司 | STP Core-film integral insulating board |
CN108277656B (en) * | 2018-01-12 | 2020-05-19 | 江苏巨盈节能环保科技有限公司 | Vacuum insulation panel prepared from industrial solid waste and preparation method |
CN108251913A (en) * | 2018-01-12 | 2018-07-06 | 江苏巨盈节能环保科技有限公司 | A kind of ultra-fine inorganic fibre spray coating heat preservation material and preparation method thereof |
CN108678200A (en) * | 2018-05-22 | 2018-10-19 | 江苏大利节能科技股份有限公司 | A kind of vacuum heat-insulating plate and preparation method thereof applied to building exterior wall heat preserving |
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